GB1415723A - Preparation of olefinically unsaturated n,n-dialkylamides and their use - Google Patents
Preparation of olefinically unsaturated n,n-dialkylamides and their useInfo
- Publication number
- GB1415723A GB1415723A GB4129973A GB4129973A GB1415723A GB 1415723 A GB1415723 A GB 1415723A GB 4129973 A GB4129973 A GB 4129973A GB 4129973 A GB4129973 A GB 4129973A GB 1415723 A GB1415723 A GB 1415723A
- Authority
- GB
- United Kingdom
- Prior art keywords
- polyol
- beta
- cracking
- ester
- ether substituted
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000002360 preparation method Methods 0.000 title abstract 2
- 229920005862 polyol Polymers 0.000 abstract 5
- 150000003077 polyols Chemical class 0.000 abstract 5
- 238000007112 amidation reaction Methods 0.000 abstract 4
- 238000005336 cracking Methods 0.000 abstract 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 3
- 125000005250 alkyl acrylate group Chemical group 0.000 abstract 3
- 150000002148 esters Chemical class 0.000 abstract 3
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 abstract 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 2
- 230000002378 acidificating effect Effects 0.000 abstract 2
- 150000001408 amides Chemical class 0.000 abstract 2
- 150000001732 carboxylic acid derivatives Chemical class 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 239000007795 chemical reaction product Substances 0.000 abstract 2
- 229910004298 SiO 2 Inorganic materials 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 239000004411 aluminium Substances 0.000 abstract 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- 230000002862 amidating effect Effects 0.000 abstract 1
- 230000009435 amidation Effects 0.000 abstract 1
- 150000001733 carboxylic acid esters Chemical class 0.000 abstract 1
- 238000004523 catalytic cracking Methods 0.000 abstract 1
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 1
- 239000003112 inhibitor Substances 0.000 abstract 1
- 229910052742 iron Inorganic materials 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 abstract 1
- 150000002763 monocarboxylic acids Chemical class 0.000 abstract 1
- 229940088644 n,n-dimethylacrylamide Drugs 0.000 abstract 1
- YLGYACDQVQQZSW-UHFFFAOYSA-N n,n-dimethylprop-2-enamide Chemical compound CN(C)C(=O)C=C YLGYACDQVQQZSW-UHFFFAOYSA-N 0.000 abstract 1
- 238000006116 polymerization reaction Methods 0.000 abstract 1
- 238000004064 recycling Methods 0.000 abstract 1
- 239000003381 stabilizer Substances 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
- C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
- C07C233/02—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
- C07C15/02—Monocyclic hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
- C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
- C07C233/34—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by amino groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US285796A US3914303A (en) | 1972-09-01 | 1972-09-01 | Preparation of N,N-dialkylacylamides |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1415723A true GB1415723A (en) | 1975-11-26 |
Family
ID=23095725
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB4129973A Expired GB1415723A (en) | 1972-09-01 | 1973-09-03 | Preparation of olefinically unsaturated n,n-dialkylamides and their use |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3914303A (enExample) |
| JP (1) | JPS4966623A (enExample) |
| DE (1) | DE2344070C3 (enExample) |
| FR (2) | FR2334661A1 (enExample) |
| GB (1) | GB1415723A (enExample) |
| IT (1) | IT995233B (enExample) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106883136A (zh) * | 2017-03-17 | 2017-06-23 | 浙江联盛化学股份有限公司 | 3‑甲氧基‑n,n‑二甲基丙酰胺的合成方法 |
| CN106966923A (zh) * | 2017-03-17 | 2017-07-21 | 浙江联盛化学股份有限公司 | 一种3‑甲氧基‑n,n‑二甲基丙酰胺的合成方法 |
| CN115028545A (zh) * | 2022-05-30 | 2022-09-09 | 江苏万盛大伟化学有限公司 | 一种废水中苯酚萃取剂dw503的制备方法 |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2836520C2 (de) * | 1978-08-21 | 1984-03-22 | Chemische Fabrik Stockhausen GmbH, 4150 Krefeld | Verfahren zur Herstellung von alpha , beta -ungesättigten, N-substituierten Carbonsäureamiden |
| IN151693B (enExample) * | 1978-05-05 | 1983-07-02 | Stockhausen & Cie Chem Fab | |
| DE2967515D1 (en) * | 1978-12-27 | 1985-10-24 | Stockhausen Chem Fab Gmbh | Process for the preparation of alpha-beta unsaturated n-substituted carboxylic acid amides, alpha-beta unsaturated n-substituted carboxylic acid amides and their use for preparing ion exchangers |
| DE2918486C2 (de) * | 1979-05-08 | 1982-10-14 | Chemische Fabrik Stockhausen GmbH, 4150 Krefeld | Verfahren zur Herstellung von N-substituierten Acrylamiden |
| US4251461A (en) * | 1980-01-17 | 1981-02-17 | Texaco Development Corporation | Process for reducing acid impurity levels in N-(tertiaryaminoalkyl)acrylamide production |
| US4287363A (en) * | 1980-09-02 | 1981-09-01 | Texaco Inc. | Preparation of N-(alkylaminoalkyl)acrylamides |
| CA1322750C (en) * | 1987-12-17 | 1993-10-05 | Mitsui Toatsu Chemicals, Inc. | Preparation process of unsaturated carboxylic acid amide |
| US4959489A (en) * | 1989-10-02 | 1990-09-25 | Air Products And Chemicals, Inc. | Process for making an acrylamide containing a dialkyl acetal group |
| US5587515A (en) * | 1992-10-21 | 1996-12-24 | Kohjin Co., Ltd. | Method of manufacturing N-monosubstituted (meth)acrylamides |
| US20050027120A1 (en) * | 2003-06-02 | 2005-02-03 | Reactimex, S.A. De C.V. | Method for the synthesis of amides and related products from esters or ester-like compounds |
| KR101410256B1 (ko) * | 2007-02-20 | 2014-06-20 | 이데미쓰 고산 가부시키가이샤 | β-알콕시프로피온아미드류의 제조 방법 |
| JP5331469B2 (ja) * | 2008-12-10 | 2013-10-30 | 出光興産株式会社 | β−アルコキシプロピオンアミド類の製造方法 |
| JP5626838B2 (ja) * | 2010-02-17 | 2014-11-19 | Ｋｊケミカルズ株式会社 | 高品位なｎ（ｎ，ｎ）−モノ（ジ）アルキルアクリルアミドの製造方法 |
| JP5574099B2 (ja) | 2010-05-26 | 2014-08-20 | セイコーエプソン株式会社 | インクジェット捺染用インク組成物およびインクジェット捺染方法 |
| JP2011246571A (ja) * | 2010-05-26 | 2011-12-08 | Seiko Epson Corp | インクジェット記録用非水系インク組成物およびインクジェット記録方法 |
| JP5601075B2 (ja) * | 2010-08-04 | 2014-10-08 | 株式会社リコー | インクジェット用インク、並びにインクカートリッジ、インクジェット記録方法、インクジェット記録装置及びインク記録物 |
| JP5700195B2 (ja) | 2010-09-03 | 2015-04-15 | セイコーエプソン株式会社 | インクジェット記録用非水系インク組成物、インクセット、およびインクジェット記録方法 |
| JPWO2013153754A1 (ja) * | 2012-04-11 | 2015-12-17 | 出光興産株式会社 | β−アルコキシプロピオンアミド類の製造方法 |
| JPWO2015147046A1 (ja) * | 2014-03-28 | 2017-04-13 | 出光興産株式会社 | 抽出蒸留用の抽出溶剤、及びそれを用いた炭化水素類の分離方法 |
| CN117820156A (zh) * | 2023-12-04 | 2024-04-05 | 深圳市宝安区新材料研究院 | 一种烷氧基二甲基丙酰胺粗品的提纯方法 |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2128208A (en) * | 1937-02-27 | 1938-08-23 | Du Pont | Alkoxy derivatives of methacrylic acid esters and method of producing them |
| US2393000A (en) * | 1943-07-24 | 1946-01-15 | Wingfoot Corp | Process of preparing alkoxy propionyl compounds |
| US2534585A (en) * | 1948-04-15 | 1950-12-19 | American Cyanamid Co | Method of producing n-alkyl acrylamides |
| US2529838A (en) * | 1948-09-23 | 1950-11-14 | American Cyanamid Co | Preparation of n, n-dialkylacrylamides |
| US2562583A (en) * | 1948-12-29 | 1951-07-31 | Union Carbide & Carbon Corp | Process for making acrylonitriles |
| US2587209A (en) * | 1949-08-01 | 1952-02-26 | Union Carbide & Carbon Corp | Production of acrylamides |
| US2702822A (en) * | 1952-06-12 | 1955-02-22 | Hercules Powder Co Ltd | Production of unsaturated amides |
| US2719175A (en) * | 1952-11-01 | 1955-09-27 | Eastman Kodak Co | Vapor phase preparation of n-substituted acrylamides |
| US3288794A (en) * | 1962-09-12 | 1966-11-29 | C P Hall Company Of Illinois | Method of making amides of dimethylamine and piperazine |
-
1972
- 1972-09-01 US US285796A patent/US3914303A/en not_active Expired - Lifetime
-
1973
- 1973-08-27 IT IT28260/73A patent/IT995233B/it active
- 1973-08-31 JP JP48097419A patent/JPS4966623A/ja active Pending
- 1973-08-31 DE DE2344070A patent/DE2344070C3/de not_active Expired
- 1973-08-31 FR FR7331618A patent/FR2334661A1/fr active Granted
- 1973-09-03 GB GB4129973A patent/GB1415723A/en not_active Expired
-
1974
- 1974-06-06 FR FR7419623A patent/FR2224449B1/fr not_active Expired
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106883136A (zh) * | 2017-03-17 | 2017-06-23 | 浙江联盛化学股份有限公司 | 3‑甲氧基‑n,n‑二甲基丙酰胺的合成方法 |
| CN106966923A (zh) * | 2017-03-17 | 2017-07-21 | 浙江联盛化学股份有限公司 | 一种3‑甲氧基‑n,n‑二甲基丙酰胺的合成方法 |
| CN106883136B (zh) * | 2017-03-17 | 2019-07-26 | 浙江联盛化学股份有限公司 | 3-甲氧基-n,n-二甲基丙酰胺的合成方法 |
| CN106966923B (zh) * | 2017-03-17 | 2019-07-26 | 浙江联盛化学股份有限公司 | 一种3-甲氧基-n,n-二甲基丙酰胺的合成方法 |
| CN115028545A (zh) * | 2022-05-30 | 2022-09-09 | 江苏万盛大伟化学有限公司 | 一种废水中苯酚萃取剂dw503的制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| IT995233B (it) | 1975-11-10 |
| FR2334661A1 (fr) | 1977-07-08 |
| FR2334661B1 (enExample) | 1978-05-12 |
| USB285796I5 (enExample) | 1975-01-28 |
| JPS4966623A (enExample) | 1974-06-27 |
| DE2344070B2 (de) | 1979-06-13 |
| FR2224449A1 (enExample) | 1974-10-31 |
| US3914303A (en) | 1975-10-21 |
| DE2344070C3 (de) | 1980-03-13 |
| DE2344070A1 (de) | 1974-03-14 |
| FR2224449B1 (enExample) | 1978-05-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |