GB1404546A - Process for purifying commercial-grade phosphoric acid by extraction - Google Patents
Process for purifying commercial-grade phosphoric acid by extractionInfo
- Publication number
- GB1404546A GB1404546A GB2893573A GB2893573A GB1404546A GB 1404546 A GB1404546 A GB 1404546A GB 2893573 A GB2893573 A GB 2893573A GB 2893573 A GB2893573 A GB 2893573A GB 1404546 A GB1404546 A GB 1404546A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acid
- organic phase
- phase
- inorganic
- oetker
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title abstract 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 title 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 title 1
- 238000000605 extraction Methods 0.000 title 1
- 239000002253 acid Substances 0.000 abstract 5
- 239000012074 organic phase Substances 0.000 abstract 5
- 239000012071 phase Substances 0.000 abstract 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract 2
- 229910017053 inorganic salt Inorganic materials 0.000 abstract 2
- 239000003960 organic solvent Substances 0.000 abstract 2
- 238000000926 separation method Methods 0.000 abstract 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 abstract 1
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 abstract 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 1
- 229910019142 PO4 Inorganic materials 0.000 abstract 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical compound OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
- 150000001768 cations Chemical class 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 229910001853 inorganic hydroxide Inorganic materials 0.000 abstract 1
- 150000002500 ions Chemical class 0.000 abstract 1
- 150000002576 ketones Chemical class 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract 1
- 239000010452 phosphate Substances 0.000 abstract 1
- 235000021110 pickles Nutrition 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 229910021653 sulphate ion Inorganic materials 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
- C23G1/36—Regeneration of waste pickling liquors
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/46—Preparation involving solvent-solvent extraction
- C01B25/461—Preparation involving solvent-solvent extraction the phosphoric acid present in the medium obtained after reaction being first extracted from the liquid phase formed or separated then re-extracted as free acid by using water or as a phosphate by using a basic compound
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/46—Preparation involving solvent-solvent extraction
- C01B25/461—Preparation involving solvent-solvent extraction the phosphoric acid present in the medium obtained after reaction being first extracted from the liquid phase formed or separated then re-extracted as free acid by using water or as a phosphate by using a basic compound
- C01B25/462—Preparation involving solvent-solvent extraction the phosphoric acid present in the medium obtained after reaction being first extracted from the liquid phase formed or separated then re-extracted as free acid by using water or as a phosphate by using a basic compound the extracting agent being alcohol or a mixture of alcohols
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Analytical Chemistry (AREA)
- Inorganic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2229602 | 1972-06-19 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1404546A true GB1404546A (en) | 1975-09-03 |
Family
ID=5848004
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2893573A Expired GB1404546A (en) | 1972-06-19 | 1973-06-19 | Process for purifying commercial-grade phosphoric acid by extraction |
Country Status (9)
| Country | Link |
|---|---|
| JP (1) | JPS5310957B2 (enrdf_load_stackoverflow) |
| BE (1) | BE796996A (enrdf_load_stackoverflow) |
| DE (1) | DE2229602B1 (enrdf_load_stackoverflow) |
| FR (1) | FR2189316B1 (enrdf_load_stackoverflow) |
| GB (1) | GB1404546A (enrdf_load_stackoverflow) |
| IL (1) | IL42487A (enrdf_load_stackoverflow) |
| IT (1) | IT982777B (enrdf_load_stackoverflow) |
| NL (1) | NL173627C (enrdf_load_stackoverflow) |
| SE (1) | SE386148B (enrdf_load_stackoverflow) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2433307C3 (de) * | 1974-07-11 | 1984-03-22 | Chemische Fabrik Budenheim Rudolf A. Oetker, 6501 Budenheim | Verfahren zur Abtrennung eines Phosphorsäure-organisches Lösungsmittel-Wasser-Gemisches |
| DE2435789C3 (de) * | 1974-07-25 | 1984-06-20 | Hoechst Ag, 6230 Frankfurt | Verfahren zur Reinigung von Phosphorsäure mit Hilfe von 3-Methoxybutanol |
| DE2538720C2 (de) * | 1975-08-30 | 1982-11-18 | Giulini Chemie Gmbh, 6700 Ludwigshafen | Verfahren zur Reinigung von Naßverfahrensphosphorsäure |
| FR2447348A1 (fr) * | 1979-01-24 | 1980-08-22 | Rhone Poulenc Ind | Procede de purification d'un acide phosphorique impur |
| JPS55124490U (enrdf_load_stackoverflow) * | 1979-02-27 | 1980-09-03 | ||
| DE3328499A1 (de) * | 1983-08-06 | 1985-02-14 | Hoechst Ag, 6230 Frankfurt | Verfahren zur verminderung des fluorgehaltes einer nassverfahrensphosphorsaeure |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1531487A (fr) * | 1967-05-11 | 1968-07-05 | Pechiney Saint Gobain | Procédé continu perfectionné de purification de l'acide phosphorique par les solvants |
| DE2029564C3 (de) * | 1970-06-16 | 1978-06-22 | Giulini Chemie Gmbh, 6700 Ludwigshafen | Verfahren zur Herstellung von reinen Alkaliphosphaten aus Rohphosphorsäure |
-
1972
- 1972-06-19 DE DE2229602A patent/DE2229602B1/de active Pending
-
1973
- 1973-03-19 BE BE128972A patent/BE796996A/xx not_active IP Right Cessation
- 1973-03-29 NL NLAANVRAGE7304362,A patent/NL173627C/xx not_active IP Right Cessation
- 1973-04-16 IT IT23054/73A patent/IT982777B/it active
- 1973-05-04 SE SE7306294A patent/SE386148B/xx unknown
- 1973-06-12 IL IL42487A patent/IL42487A/en unknown
- 1973-06-19 JP JP6910873A patent/JPS5310957B2/ja not_active Expired
- 1973-06-19 FR FR7323032A patent/FR2189316B1/fr not_active Expired
- 1973-06-19 GB GB2893573A patent/GB1404546A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| FR2189316A1 (enrdf_load_stackoverflow) | 1974-01-25 |
| IL42487A (en) | 1977-02-28 |
| IL42487A0 (en) | 1973-08-29 |
| IT982777B (it) | 1974-10-21 |
| BE796996A (fr) | 1973-07-16 |
| FR2189316B1 (enrdf_load_stackoverflow) | 1978-07-21 |
| NL7304362A (enrdf_load_stackoverflow) | 1973-12-21 |
| DE2229602B1 (de) | 1973-09-27 |
| SE386148B (sv) | 1976-08-02 |
| NL173627C (nl) | 1984-02-16 |
| NL173627B (nl) | 1983-09-16 |
| JPS5310957B2 (enrdf_load_stackoverflow) | 1978-04-18 |
| JPS4963692A (enrdf_load_stackoverflow) | 1974-06-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |