GB1393034A - Process for the preparation of phosphonic acid dihalides - Google Patents
Process for the preparation of phosphonic acid dihalidesInfo
- Publication number
- GB1393034A GB1393034A GB2756472A GB2756472A GB1393034A GB 1393034 A GB1393034 A GB 1393034A GB 2756472 A GB2756472 A GB 2756472A GB 2756472 A GB2756472 A GB 2756472A GB 1393034 A GB1393034 A GB 1393034A
- Authority
- GB
- United Kingdom
- Prior art keywords
- phosphonic acid
- acid
- atoms
- formula
- ester
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical compound OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 title abstract 5
- 238000000034 method Methods 0.000 title abstract 2
- 125000004432 carbon atom Chemical group C* 0.000 abstract 4
- 125000006564 (C4-C8) cycloalkyl group Chemical group 0.000 abstract 2
- KCKMCFYLQPTGGE-UHFFFAOYSA-N ClCCOP(OCCCl)=O.ClCC Chemical compound ClCCOP(OCCCl)=O.ClCC KCKMCFYLQPTGGE-UHFFFAOYSA-N 0.000 abstract 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- 125000000217 alkyl group Chemical group 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 125000004437 phosphorous atom Chemical group 0.000 abstract 2
- 229910052698 phosphorus Inorganic materials 0.000 abstract 2
- 239000011574 phosphorus Substances 0.000 abstract 2
- -1 pyrophosphonic acid ester Chemical class 0.000 abstract 2
- 150000003839 salts Chemical class 0.000 abstract 2
- 239000007858 starting material Substances 0.000 abstract 2
- 125000004641 (C1-C12) haloalkyl group Chemical group 0.000 abstract 1
- MLSZIADXWDYFKM-UHFFFAOYSA-N 1-dichlorophosphorylethene Chemical compound ClP(Cl)(=O)C=C MLSZIADXWDYFKM-UHFFFAOYSA-N 0.000 abstract 1
- 239000004135 Bone phosphate Substances 0.000 abstract 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 1
- ZVNOEZHWBDKVHV-UHFFFAOYSA-N Cl[PH3]Cl Chemical class Cl[PH3]Cl ZVNOEZHWBDKVHV-UHFFFAOYSA-N 0.000 abstract 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 abstract 1
- ZBVOEVQTNYNNMY-UHFFFAOYSA-N O=P1=CCCC1 Chemical class O=P1=CCCC1 ZBVOEVQTNYNNMY-UHFFFAOYSA-N 0.000 abstract 1
- 125000003342 alkenyl group Chemical group 0.000 abstract 1
- 125000005037 alkyl phenyl group Chemical group 0.000 abstract 1
- 125000002947 alkylene group Chemical group 0.000 abstract 1
- 150000001408 amides Chemical class 0.000 abstract 1
- 150000001412 amines Chemical class 0.000 abstract 1
- 125000003277 amino group Chemical group 0.000 abstract 1
- 125000001246 bromo group Chemical group Br* 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 125000004093 cyano group Chemical group *C#N 0.000 abstract 1
- XQRLCLUYWUNEEH-UHFFFAOYSA-N diphosphonic acid Chemical compound OP(=O)OP(O)=O XQRLCLUYWUNEEH-UHFFFAOYSA-N 0.000 abstract 1
- 150000004820 halides Chemical class 0.000 abstract 1
- 229910052736 halogen Inorganic materials 0.000 abstract 1
- 150000002367 halogens Chemical class 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 150000002391 heterocyclic compounds Chemical class 0.000 abstract 1
- 238000011065 in-situ storage Methods 0.000 abstract 1
- 125000004433 nitrogen atom Chemical group N* 0.000 abstract 1
- MPQXHAGKBWFSNV-UHFFFAOYSA-N oxidophosphanium Chemical class [PH3]=O MPQXHAGKBWFSNV-UHFFFAOYSA-N 0.000 abstract 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 abstract 1
- 150000003003 phosphines Chemical class 0.000 abstract 1
- 150000004714 phosphonium salts Chemical class 0.000 abstract 1
- FAIAAWCVCHQXDN-UHFFFAOYSA-N phosphorus trichloride Chemical compound ClP(Cl)Cl FAIAAWCVCHQXDN-UHFFFAOYSA-N 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 125000001453 quaternary ammonium group Chemical group 0.000 abstract 1
- 125000001424 substituent group Chemical group 0.000 abstract 1
- LMBFAGIMSUYTBN-MPZNNTNKSA-N teixobactin Chemical compound C([C@H](C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H](CCC(N)=O)C(=O)N[C@H]([C@@H](C)CC)C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H]1C(N[C@@H](C)C(=O)N[C@@H](C[C@@H]2NC(=N)NC2)C(=O)N[C@H](C(=O)O[C@H]1C)[C@@H](C)CC)=O)NC)C1=CC=CC=C1 LMBFAGIMSUYTBN-MPZNNTNKSA-N 0.000 abstract 1
- LUVCTYHBTXSAMX-UHFFFAOYSA-N tris(2-chloroethyl) phosphite Chemical compound ClCCOP(OCCCl)OCCCl LUVCTYHBTXSAMX-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/42—Halides thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712129584 DE2129584C3 (de) | 1971-06-15 | 1971-06-15 | Verfahren zur Herstellung von Phosphonsäuredihalogeniden |
| DE19712132962 DE2132962C3 (de) | 1971-07-02 | 1971-07-02 | Verfahren zur Herstellung von 2-Chloräthanphosphonsäuredichlorid |
| DE19722215314 DE2215314C3 (de) | 1972-03-29 | 1972-03-29 | Verfahren zur Herstellung von 2-Chloräthanphosphonsäuredichlorid |
| DE19722216565 DE2216565C3 (de) | 1972-04-06 | 1972-04-06 | Verfahren zur Herstellung von Phosphonsäuredihalogeniden |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1393034A true GB1393034A (en) | 1975-05-07 |
Family
ID=27431264
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2756472A Expired GB1393034A (en) | 1971-06-15 | 1972-06-13 | Process for the preparation of phosphonic acid dihalides |
Country Status (12)
| Country | Link |
|---|---|
| JP (1) | JPS5652025B2 (xx) |
| AT (1) | AT317251B (xx) |
| BE (1) | BE784923A (xx) |
| CA (1) | CA969194A (xx) |
| CH (1) | CH583743A5 (xx) |
| CS (1) | CS166044B2 (xx) |
| DD (1) | DD99383A5 (xx) |
| FR (1) | FR2141962B1 (xx) |
| GB (1) | GB1393034A (xx) |
| IL (1) | IL39681A (xx) |
| IT (1) | IT956531B (xx) |
| NL (1) | NL7207872A (xx) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3972923A (en) * | 1971-06-15 | 1976-08-03 | Hoechst Aktiengesellschaft | Process for the preparation of phosphonic acid dihalides |
| DE2259454C3 (de) * | 1972-12-05 | 1980-10-23 | Hoechst Ag, 6000 Frankfurt | Verfahren zur Herstellung von Halogenmethanphosphonsäuredihalogenid |
| DE2357676C2 (de) * | 1973-11-19 | 1982-02-04 | Hoechst Ag, 6000 Frankfurt | Verfahren zur Herstellung von 2-Halogenäthanphosphonsäuredihalogenid und Vinylphosphonsäuredihalogenid |
| DE3033614A1 (de) * | 1980-09-06 | 1982-04-29 | Hoechst Ag, 6000 Frankfurt | Verfahren zur herstellung von vinylphosphonsaeuredichlorid und 2-chlorethanphosphonsaeuredichlorid |
| DE3541627A1 (de) * | 1985-11-26 | 1987-05-27 | Hoechst Ag | Verfahren zur herstellung von phosphonsaeuredichloriden |
| DE3629579A1 (de) * | 1986-08-30 | 1988-03-03 | Hoechst Ag | Verfahren zur herstellung von 2-chlorethanphosphonsaeuredichlorid |
| DE3629578A1 (de) * | 1986-08-30 | 1988-03-03 | Hoechst Ag | Verfahren zur herstellung von vinylphosphonsaeuredichlorid |
| DE3641100A1 (de) * | 1986-12-02 | 1988-06-09 | Hoechst Ag | Verfahren zur herstellung von 2-chlorethanphosphonsaeuredichlorid |
-
1972
- 1972-06-06 CS CS3904A patent/CS166044B2/cs unknown
- 1972-06-08 DD DD163590A patent/DD99383A5/xx unknown
- 1972-06-09 NL NL7207872A patent/NL7207872A/xx not_active Application Discontinuation
- 1972-06-12 CH CH872272A patent/CH583743A5/xx not_active IP Right Cessation
- 1972-06-13 AT AT506472A patent/AT317251B/de not_active IP Right Cessation
- 1972-06-13 IT IT25626/72A patent/IT956531B/it active
- 1972-06-13 GB GB2756472A patent/GB1393034A/en not_active Expired
- 1972-06-13 IL IL39681A patent/IL39681A/xx unknown
- 1972-06-14 CA CA144,666A patent/CA969194A/en not_active Expired
- 1972-06-14 JP JP5870972A patent/JPS5652025B2/ja not_active Expired
- 1972-06-15 BE BE784923A patent/BE784923A/xx unknown
- 1972-06-15 FR FR7221600A patent/FR2141962B1/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| AT317251B (de) | 1974-08-26 |
| IT956531B (it) | 1973-10-10 |
| JPS4872126A (xx) | 1973-09-29 |
| DD99383A5 (xx) | 1973-08-05 |
| CA969194A (en) | 1975-06-10 |
| FR2141962A1 (xx) | 1973-01-26 |
| FR2141962B1 (xx) | 1977-12-23 |
| CH583743A5 (xx) | 1977-01-14 |
| BE784923A (fr) | 1972-12-15 |
| IL39681A0 (en) | 1972-08-30 |
| NL7207872A (xx) | 1972-12-19 |
| CS166044B2 (xx) | 1976-01-29 |
| JPS5652025B2 (xx) | 1981-12-09 |
| IL39681A (en) | 1975-11-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PE20 | Patent expired after termination of 20 years |