GB1386166A - Process for preparing beta,delta-dioxocaproaldehyde dialkyl acetal - Google Patents
Process for preparing beta,delta-dioxocaproaldehyde dialkyl acetalInfo
- Publication number
- GB1386166A GB1386166A GB2457672A GB2457672A GB1386166A GB 1386166 A GB1386166 A GB 1386166A GB 2457672 A GB2457672 A GB 2457672A GB 2457672 A GB2457672 A GB 2457672A GB 1386166 A GB1386166 A GB 1386166A
- Authority
- GB
- United Kingdom
- Prior art keywords
- dioxocaproaldehyde
- alkyl
- delta
- dialkyl acetal
- preparing beta
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- NVBJELVUQIDITN-UHFFFAOYSA-N 3,5-dioxohexanal Chemical compound CC(=O)CC(=O)CC=O NVBJELVUQIDITN-UHFFFAOYSA-N 0.000 title 1
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 title 1
- 125000002777 acetyl group Chemical class [H]C([H])([H])C(*)=O 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- 125000000217 alkyl group Chemical group 0.000 abstract 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 2
- 150000001241 acetals Chemical class 0.000 abstract 2
- 239000000376 reactant Substances 0.000 abstract 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 1
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- 239000000159 acid neutralizing agent Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- BDAGIHXWWSANSR-UHFFFAOYSA-N formic acid Substances OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 abstract 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 abstract 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 239000011369 resultant mixture Substances 0.000 abstract 1
- 239000001117 sulphuric acid Substances 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/04—Saturated compounds containing keto groups bound to acyclic carbon atoms
- C07C49/175—Saturated compounds containing keto groups bound to acyclic carbon atoms containing ether groups, groups, groups, or groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/45—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation
- C07C45/455—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation with carboxylic acids or their derivatives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP46035981A JPS5114484B1 (enrdf_load_stackoverflow) | 1971-05-26 | 1971-05-26 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1386166A true GB1386166A (en) | 1975-03-05 |
Family
ID=12457047
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2457672A Expired GB1386166A (en) | 1971-05-26 | 1972-05-25 | Process for preparing beta,delta-dioxocaproaldehyde dialkyl acetal |
Country Status (8)
| Country | Link |
|---|---|
| JP (1) | JPS5114484B1 (enrdf_load_stackoverflow) |
| CA (1) | CA956325A (enrdf_load_stackoverflow) |
| CH (1) | CH538438A (enrdf_load_stackoverflow) |
| DE (1) | DE2225243A1 (enrdf_load_stackoverflow) |
| FR (1) | FR2139173B1 (enrdf_load_stackoverflow) |
| GB (1) | GB1386166A (enrdf_load_stackoverflow) |
| IT (1) | IT955938B (enrdf_load_stackoverflow) |
| NL (1) | NL7207200A (enrdf_load_stackoverflow) |
-
1971
- 1971-05-26 JP JP46035981A patent/JPS5114484B1/ja active Pending
-
1972
- 1972-05-24 DE DE19722225243 patent/DE2225243A1/de active Pending
- 1972-05-24 CH CH765772A patent/CH538438A/fr not_active IP Right Cessation
- 1972-05-25 GB GB2457672A patent/GB1386166A/en not_active Expired
- 1972-05-25 CA CA143,031A patent/CA956325A/en not_active Expired
- 1972-05-26 NL NL7207200A patent/NL7207200A/xx unknown
- 1972-05-26 FR FR7219001A patent/FR2139173B1/fr not_active Expired
- 1972-05-26 IT IT2495572A patent/IT955938B/it active
Also Published As
| Publication number | Publication date |
|---|---|
| CH538438A (fr) | 1973-06-30 |
| FR2139173A1 (enrdf_load_stackoverflow) | 1973-01-05 |
| IT955938B (it) | 1973-09-29 |
| JPS5114484B1 (enrdf_load_stackoverflow) | 1976-05-10 |
| CA956325A (en) | 1974-10-15 |
| NL7207200A (enrdf_load_stackoverflow) | 1972-11-28 |
| FR2139173B1 (enrdf_load_stackoverflow) | 1977-06-17 |
| DE2225243A1 (enrdf_load_stackoverflow) | 1972-12-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PCNP | Patent ceased through non-payment of renewal fee |