GB1383583A - Continuous production of n,n-diacetylethylenediamine - Google Patents

Continuous production of n,n-diacetylethylenediamine

Info

Publication number
GB1383583A
GB1383583A GB1726172A GB1726172A GB1383583A GB 1383583 A GB1383583 A GB 1383583A GB 1726172 A GB1726172 A GB 1726172A GB 1726172 A GB1726172 A GB 1726172A GB 1383583 A GB1383583 A GB 1383583A
Authority
GB
United Kingdom
Prior art keywords
diacetylethylenediamine
april
continuous production
acetic acid
zones
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB1726172A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Badische Anilin and Sodafabrik AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE, Badische Anilin and Sodafabrik AG filed Critical BASF SE
Publication of GB1383583A publication Critical patent/GB1383583A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/34—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by amino groups
    • C07C233/35—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by amino groups with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom
    • C07C233/36—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by amino groups with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom having the carbon atom of the carboxamide group bound to a hydrogen atom or to a carbon atom of an acyclic saturated carbon skeleton

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1383583 N,N<SP>1</SP>-Diacetylethylenediamine BADISCHE ANILIN- & SODA-FABRIK AG 14 April 1972 [15 April 1971] 17261/72 Heading C2C N,N<SP>1</SP>-Diacetylethylenediamine is produced by continuously supplying ethylenediamine and acetic acid in a ratio by weight of from 1 : 2 to 1:3 to a melt of N.N<SP>1</SP>-diacetylethylenediamine at 140-215‹ C., continuously distilling off excess acetic acid and water and withdrawing N,N<SP>1</SP>-diacetylethylenediamine at the rate at which it is formed. The reaction may be carried out in 2-4 successive zones, or in a column in which individual trays are the different reaction zones.
GB1726172A 1971-04-15 1972-04-14 Continuous production of n,n-diacetylethylenediamine Expired GB1383583A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE2118282A DE2118282C3 (en) 1971-04-15 1971-04-15 Process for the continuous production of N.N'-diacetylethylenediamine

Publications (1)

Publication Number Publication Date
GB1383583A true GB1383583A (en) 1974-02-12

Family

ID=5804802

Family Applications (1)

Application Number Title Priority Date Filing Date
GB1726172A Expired GB1383583A (en) 1971-04-15 1972-04-14 Continuous production of n,n-diacetylethylenediamine

Country Status (9)

Country Link
AT (1) AT314492B (en)
BE (1) BE781995A (en)
CH (1) CH564520A5 (en)
DE (1) DE2118282C3 (en)
FR (1) FR2136341A5 (en)
GB (1) GB1383583A (en)
IT (1) IT954430B (en)
NL (1) NL7204898A (en)
SE (1) SE368198B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5661338A (en) * 1979-10-10 1981-05-26 Hoechst Ag Continuous manufacture of diacetylethylenediamine

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2828765A1 (en) * 1978-06-30 1980-01-10 Hoechst Ag METHOD FOR PRODUCING N, N'-DIACETYLETHYLENE DIAMINE
DE2832021A1 (en) * 1978-07-21 1980-01-31 Basf Ag METHOD FOR PRODUCING TETRAACETYLAETHYLENEDIAMIN
DE3021961A1 (en) * 1980-06-12 1981-12-24 Basf Ag, 6700 Ludwigshafen METHOD FOR PRODUCING N, N'-DIACETYLETHYLENE DIAMINE
DK12887A (en) * 1987-01-12 1988-07-13 Cheminova As PROCEDURE FOR THE PREPARATION OF N, N'-DIACETYLETHYLENDIAMINE

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5661338A (en) * 1979-10-10 1981-05-26 Hoechst Ag Continuous manufacture of diacetylethylenediamine
US4324911A (en) * 1979-10-10 1982-04-13 Hoechst Aktiengesellschaft Process for the continuous preparation of diacetyl ethylene diamine
JPH0141619B2 (en) * 1979-10-10 1989-09-06 Hoechst Ag

Also Published As

Publication number Publication date
CH564520A5 (en) 1975-07-31
DE2118282B2 (en) 1974-02-07
AT314492B (en) 1974-04-10
FR2136341A5 (en) 1972-12-22
DE2118282A1 (en) 1972-11-02
DE2118282C3 (en) 1974-10-03
NL7204898A (en) 1972-10-17
SE368198B (en) 1974-06-24
IT954430B (en) 1973-08-30
BE781995A (en) 1972-10-12

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PCNP Patent ceased through non-payment of renewal fee