GB1381730A - Process for the industrial manufacture of dinitrostilbene disulphonic acid - Google Patents

Process for the industrial manufacture of dinitrostilbene disulphonic acid

Info

Publication number
GB1381730A
GB1381730A GB5583871A GB5583871A GB1381730A GB 1381730 A GB1381730 A GB 1381730A GB 5583871 A GB5583871 A GB 5583871A GB 5583871 A GB5583871 A GB 5583871A GB 1381730 A GB1381730 A GB 1381730A
Authority
GB
United Kingdom
Prior art keywords
dinitrostilbene
disulphonic acid
industrial manufacture
acid
disulphonic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB5583871A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Clayton Aniline Co Ltd
Original Assignee
Clayton Aniline Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to BE792103D priority Critical patent/BE792103A/en
Application filed by Clayton Aniline Co Ltd filed Critical Clayton Aniline Co Ltd
Priority to GB5583871A priority patent/GB1381730A/en
Priority to JP47116713A priority patent/JPS4875553A/ja
Priority to CH1707772A priority patent/CH576954A5/xx
Priority to CA157,523A priority patent/CA983026A/en
Priority to FR7242281A priority patent/FR2164182A5/fr
Priority to IT5434872A priority patent/IT973782B/en
Priority to DE19722258530 priority patent/DE2258530A1/en
Priority to BR842372A priority patent/BR7208423D0/en
Priority to ES409127A priority patent/ES409127A1/en
Publication of GB1381730A publication Critical patent/GB1381730A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C07C303/22—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof from sulfonic acids, by reactions not involving the formation of sulfo or halosulfonyl groups; from sulfonic halides by reactions not involving the formation of halosulfonyl groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1381730 4,4<SP>1</SP>-Dinitrostilbene-2,2<SP>1</SP>-disulphonic acid CLAYTON ANILINE CO Ltd 15 Nov 1972 [1 Dec 1971] 55838/71 Heading C2C 4,41-Dinitrostilbene-2,2<SP>1</SP>-disulphonic acid is obtained by treating 4-nitrotoluene-2-sulphonic acid with liquid or gaseous halogen under alkaline conditions at a temperature below the boiling point of the reaction mixture, preferably at 80 to 90‹ C. The process may be carried out continuously. Examples are given which illustrate the process.
GB5583871A 1971-12-01 1971-12-01 Process for the industrial manufacture of dinitrostilbene disulphonic acid Expired GB1381730A (en)

Priority Applications (10)

Application Number Priority Date Filing Date Title
BE792103D BE792103A (en) 1971-12-01 NEW MANUFACTURING PROCESS FOR DINITROSTILBENE DISULPHONIC ACID ON AN INDUSTRIAL SCALE
GB5583871A GB1381730A (en) 1971-12-01 1971-12-01 Process for the industrial manufacture of dinitrostilbene disulphonic acid
JP47116713A JPS4875553A (en) 1971-12-01 1972-11-22
CH1707772A CH576954A5 (en) 1971-12-01 1972-11-23
CA157,523A CA983026A (en) 1971-12-01 1972-11-27 Process for the industrial manufacture of dinitrostilbene disulphonic acid
FR7242281A FR2164182A5 (en) 1971-12-01 1972-11-28
IT5434872A IT973782B (en) 1971-12-01 1972-11-29 PROCEDURE FOR PRODUCING ACID 4 4 DINITROSTILBEN 2 2 DISULFURNICO
DE19722258530 DE2258530A1 (en) 1971-12-01 1972-11-29 PROCESS FOR THE PREPARATION OF 4.4'DINITROSTILBEN-2.2'-DISULPHONIC ACID
BR842372A BR7208423D0 (en) 1971-12-01 1972-11-30 PROCESS FOR OBTAINING 4 4 'DINITROSTYLBENE 2 2' DISSULPHONIC ACID
ES409127A ES409127A1 (en) 1971-12-01 1972-11-30 Process for the industrial manufacture of dinitrostilbene disulphonic acid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB5583871A GB1381730A (en) 1971-12-01 1971-12-01 Process for the industrial manufacture of dinitrostilbene disulphonic acid

Publications (1)

Publication Number Publication Date
GB1381730A true GB1381730A (en) 1975-01-29

Family

ID=10475023

Family Applications (1)

Application Number Title Priority Date Filing Date
GB5583871A Expired GB1381730A (en) 1971-12-01 1971-12-01 Process for the industrial manufacture of dinitrostilbene disulphonic acid

Country Status (10)

Country Link
JP (1) JPS4875553A (en)
BE (1) BE792103A (en)
BR (1) BR7208423D0 (en)
CA (1) CA983026A (en)
CH (1) CH576954A5 (en)
DE (1) DE2258530A1 (en)
ES (1) ES409127A1 (en)
FR (1) FR2164182A5 (en)
GB (1) GB1381730A (en)
IT (1) IT973782B (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4680146A (en) * 1985-05-31 1987-07-14 Bayer Aktiengesellschaft Process for the preparation of 4,4'-dinitrostilbene-2,2'-disulphonic acid salts
US5808141A (en) * 1993-09-08 1998-09-15 Bayer Aktiengesellschaft Process for preparing 4,4'-dinitrostilbene-2,2'-disulphonic acid
CN106146357A (en) * 2015-04-14 2016-11-23 上海合丽亚日化技术有限公司 A kind of preparation method of DSD acid
CN107417581A (en) * 2017-08-15 2017-12-01 连云港莱亚化学有限公司 A kind of method of aqueous phase pressurization synthesis DSD acid oxidation intermediates

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2916912A1 (en) * 1979-04-26 1980-11-06 Bayer Ag METHOD FOR PRODUCING 4-NITROTOLUOL-2-SULPHONIC ACID
ATE3974T1 (en) * 1979-06-08 1983-07-15 Ciba-Geigy Ag PROCESS FOR THE PREPARATION OF 4,4'-DINITROSTILBENE-2,2'-DISULPHONIC ACID AND THEIR SALTS AND THEIR USE.
EP0305648B1 (en) * 1987-08-12 1990-03-28 Ciba-Geigy Ag Process for the preparation of 4,4'-dinitrostilbene-2,2'-disulfonic acid

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4680146A (en) * 1985-05-31 1987-07-14 Bayer Aktiengesellschaft Process for the preparation of 4,4'-dinitrostilbene-2,2'-disulphonic acid salts
US5808141A (en) * 1993-09-08 1998-09-15 Bayer Aktiengesellschaft Process for preparing 4,4'-dinitrostilbene-2,2'-disulphonic acid
CN106146357A (en) * 2015-04-14 2016-11-23 上海合丽亚日化技术有限公司 A kind of preparation method of DSD acid
CN106146357B (en) * 2015-04-14 2017-12-26 上海合丽亚日化技术有限公司 A kind of preparation method of DSD acid
CN107417581A (en) * 2017-08-15 2017-12-01 连云港莱亚化学有限公司 A kind of method of aqueous phase pressurization synthesis DSD acid oxidation intermediates

Also Published As

Publication number Publication date
BE792103A (en) 1973-05-30
CH576954A5 (en) 1976-06-30
ES409127A1 (en) 1975-11-16
CA983026A (en) 1976-02-03
JPS4875553A (en) 1973-10-11
FR2164182A5 (en) 1973-07-27
IT973782B (en) 1974-06-10
DE2258530A1 (en) 1973-06-07
BR7208423D0 (en) 1973-08-23

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Legal Events

Date Code Title Description
PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee