GB327996A - Process for the manufacture of organic stibinic acids and salts thereof - Google Patents
Process for the manufacture of organic stibinic acids and salts thereofInfo
- Publication number
- GB327996A GB327996A GB142629A GB142629A GB327996A GB 327996 A GB327996 A GB 327996A GB 142629 A GB142629 A GB 142629A GB 142629 A GB142629 A GB 142629A GB 327996 A GB327996 A GB 327996A
- Authority
- GB
- United Kingdom
- Prior art keywords
- chloro
- carbamino
- salts
- prepared
- stibinic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000003839 salts Chemical class 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- MWZAMPYHMUSARJ-UHFFFAOYSA-M stibinic acid Chemical class O[SbH2]=O MWZAMPYHMUSARJ-UHFFFAOYSA-M 0.000 title 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 abstract 1
- 125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 abstract 1
- 150000007513 acids Chemical class 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 150000001463 antimony compounds Chemical class 0.000 abstract 1
- 229910000410 antimony oxide Inorganic materials 0.000 abstract 1
- 239000002585 base Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- XLJMAIOERFSOGZ-UHFFFAOYSA-M cyanate Chemical compound [O-]C#N XLJMAIOERFSOGZ-UHFFFAOYSA-M 0.000 abstract 1
- 235000011187 glycerol Nutrition 0.000 abstract 1
- 150000007529 inorganic bases Chemical class 0.000 abstract 1
- 229910052757 nitrogen Inorganic materials 0.000 abstract 1
- 150000007530 organic bases Chemical class 0.000 abstract 1
- VTRUBDSFZJNXHI-UHFFFAOYSA-N oxoantimony Chemical compound [Sb]=O VTRUBDSFZJNXHI-UHFFFAOYSA-N 0.000 abstract 1
- 229940072033 potash Drugs 0.000 abstract 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 abstract 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 abstract 1
- 235000015320 potassium carbonate Nutrition 0.000 abstract 1
- 230000001225 therapeutic effect Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/90—Antimony compounds
- C07F9/92—Aromatic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
327,996. Carpmael, A., (I. G. Farbenindustrie Akt.-Ges.). Jan. 15, 1929. Organo-stibinic acids are prepared by diazotizing an o-, m-, or pcarbamino-arylamine and treating with an antimony compound in known manner. The products, in the form of their salts with organic or inorganic bases, possess therapeutic properties. According to the example, p-carbaminophenylstibinic acid is obtained by treating diazotized 4-carbamino-1-aminobanzene with a solution of antimony oxide in hydrochloric acid, preferably in the presence of glycerine (see Specitication 244,746); its salts with potash or other alkalies and nitrogen bases are described. In the same way, 2-chloro-4-carbaminophenyl-1- stibinic acid is prepared from 2-chloro-4-carbamino-1-aminobenzene and converted into its potassium salt. 2-Chloro-4-carbamino-1-aminobenzene is prepared by treatment of 2-chloro-4-aminoacetanilide with a cyanate and splitting off the acetyl group from the resulting carbamino compound.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB142629A GB327996A (en) | 1929-01-15 | 1929-01-15 | Process for the manufacture of organic stibinic acids and salts thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB142629A GB327996A (en) | 1929-01-15 | 1929-01-15 | Process for the manufacture of organic stibinic acids and salts thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB327996A true GB327996A (en) | 1930-04-15 |
Family
ID=9721812
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB142629A Expired GB327996A (en) | 1929-01-15 | 1929-01-15 | Process for the manufacture of organic stibinic acids and salts thereof |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB327996A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2488268A (en) * | 1945-10-06 | 1949-11-15 | Squibb & Sons Inc | Methods of preparing urea-(stibanilic acid) reaction products |
-
1929
- 1929-01-15 GB GB142629A patent/GB327996A/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2488268A (en) * | 1945-10-06 | 1949-11-15 | Squibb & Sons Inc | Methods of preparing urea-(stibanilic acid) reaction products |
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