GB1279720A - Improvements in or relating to the formation of gaseous products for analysis - Google Patents

Improvements in or relating to the formation of gaseous products for analysis

Info

Publication number
GB1279720A
GB1279720A GB63427/69A GB6342769A GB1279720A GB 1279720 A GB1279720 A GB 1279720A GB 63427/69 A GB63427/69 A GB 63427/69A GB 6342769 A GB6342769 A GB 6342769A GB 1279720 A GB1279720 A GB 1279720A
Authority
GB
United Kingdom
Prior art keywords
analysis
tube
combustion
introduced via
crucible
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB63427/69A
Inventor
Walter Koch
Helmut Lemm
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of GB1279720A publication Critical patent/GB1279720A/en
Expired legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N7/00—Analysing materials by measuring the pressure or volume of a gas or vapour
    • G01N7/14—Analysing materials by measuring the pressure or volume of a gas or vapour by allowing the material to emit a gas or vapour, e.g. water vapour, and measuring a pressure or volume difference
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/20—Metals
    • G01N33/202—Constituents thereof
    • G01N33/2022—Non-metallic constituents
    • G01N33/2025—Gaseous constituents
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/02—Devices for withdrawing samples
    • G01N1/22—Devices for withdrawing samples in the gaseous state

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Immunology (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)

Abstract

1279720 Combustion analysis W KOCH and H LEMM 31 Dec 1969 [12 March 1969] 63427/69 Heading B1X Combustion apparatus used in gaseous analysis comprises a crucible I heated in a lower portion by, e.g. a resistor 2, and cooled in an upper portion by a cooling jacket 3. Material for analysis is introduced via tube 5 and heated whereupon any gaseous products are removed via an exit 7 in a headpiece 4 by means of a pump (not shown) and a scavenging stream of oxygen introduced via a tube 6 which also seals the filling tube 5 to air. Savenging gas may also be introduced via tube 8. The products are conveyed to, e.g. an infra red or mass spectrometer, or a gas chromatograph. A known weight of sample may be introduced. Electrodes 10, 11 of an electrostatic precipitator prevent deposition of any metallic dust on the upper cooler part of the crucible 1. The combustion and analysis may be computorised for automatic procedure. Particular application is in the analysis of carbon and sulphur and total hydrogen.
GB63427/69A 1969-03-12 1969-12-31 Improvements in or relating to the formation of gaseous products for analysis Expired GB1279720A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19691912526 DE1912526A1 (en) 1969-03-12 1969-03-12 Method and device for the formation of gaseous analysis products by heating the sample material

Publications (1)

Publication Number Publication Date
GB1279720A true GB1279720A (en) 1972-06-28

Family

ID=5727890

Family Applications (1)

Application Number Title Priority Date Filing Date
GB63427/69A Expired GB1279720A (en) 1969-03-12 1969-12-31 Improvements in or relating to the formation of gaseous products for analysis

Country Status (3)

Country Link
US (1) US3694157A (en)
DE (1) DE1912526A1 (en)
GB (1) GB1279720A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4525328A (en) * 1982-03-05 1985-06-25 Leco Corporation Carbon, hydrogen, and nitrogen analyzer
US4573910A (en) * 1982-03-05 1986-03-04 Leco Corporation Carbon, hydrogen, and nitrogen analyzer
US4622009A (en) * 1982-03-05 1986-11-11 Leco Corporation Carbon, hydrogen, and nitrogen analyzer

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4282183A (en) * 1978-11-09 1981-08-04 Leco Corporation Combustion system
FR2472748A1 (en) * 1979-12-27 1981-07-03 Mo I Stali I Splavov Metallurgical slag hydrogen content measurement - involves lengthy melting in sealed furnace to ensure complete hydrogen extraction
US4680167A (en) * 1983-02-09 1987-07-14 Alcor, Inc. Controlled atmosphere oven
US4568426A (en) * 1983-02-09 1986-02-04 Alcor, Inc. Controlled atmosphere oven
FR2560529B1 (en) * 1984-03-02 1986-11-07 Rhone Poulenc Rech APPARATUS FOR WET CHEMICAL REACTION OF VARIOUS PRODUCTS
FR2560686B1 (en) * 1984-03-05 1986-11-07 Rhone Poulenc Rech MINERALIZATION APPARATUS FOR INDIVIDUAL AUTOMATIC PROCESSING OF SAMPLES OF PRODUCTS PLACED IN CONTAINERS
US4824790A (en) * 1986-10-17 1989-04-25 Advanced Fuel Research, Inc. System and method for thermogravimetric analysis
FR2683044A1 (en) * 1991-10-29 1993-04-30 Unirec Method and device for analysing, by fractionated thermal decomposition, at least one inclusional component of a body
DE4312100C2 (en) * 1993-04-08 1995-05-11 Mannesmann Ag Catalytic reactor
GB2445184B (en) * 2006-12-29 2009-05-06 Thermo Fisher Scientific Inc Combustion analyser sample introduction apparatus and method
US8181504B2 (en) * 2009-02-18 2012-05-22 Factory Mutual Insurance Company Smoke evaluating device and related method
US10935524B2 (en) * 2017-07-27 2021-03-02 CEM Corporation, Lucidity Division Gas chromatograph device with inductively heated column and method of use thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4525328A (en) * 1982-03-05 1985-06-25 Leco Corporation Carbon, hydrogen, and nitrogen analyzer
US4573910A (en) * 1982-03-05 1986-03-04 Leco Corporation Carbon, hydrogen, and nitrogen analyzer
US4622009A (en) * 1982-03-05 1986-11-11 Leco Corporation Carbon, hydrogen, and nitrogen analyzer

Also Published As

Publication number Publication date
DE1912526A1 (en) 1970-10-01
US3694157A (en) 1972-09-26

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PLNP Patent lapsed through nonpayment of renewal fees