GB1268530A - Method of and apparatus for modulated sample feed in the spectrochemical analysis of solution - Google Patents
Method of and apparatus for modulated sample feed in the spectrochemical analysis of solutionInfo
- Publication number
- GB1268530A GB1268530A GB60992/69A GB6099269A GB1268530A GB 1268530 A GB1268530 A GB 1268530A GB 60992/69 A GB60992/69 A GB 60992/69A GB 6099269 A GB6099269 A GB 6099269A GB 1268530 A GB1268530 A GB 1268530A
- Authority
- GB
- United Kingdom
- Prior art keywords
- solution
- tube
- vaporiser
- fed
- vessel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/71—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light thermally excited
- G01N21/714—Sample nebulisers for flame burners or plasma burners
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/22—Devices for withdrawing samples in the gaseous state
Landscapes
- Health & Medical Sciences (AREA)
- Physics & Mathematics (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Plasma & Fusion (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
Abstract
1,268,530. Sample feeder. CARL-ZEISSSTIFTUNG [trading as CARL ZEISS]. 15 Dec., 1969 [20 Dec., 1968], No. 60992/69. Heading B1X. [Also in Division G2] In the spectrochemical analysis of a solution, a vaporiser-burner combination 1 is fed with a modulated sample of the solution 6. The solution passes from a vessel 5 through a capillary tube 4, a flexible capillary hose 3 and capillary tube 2 to the vaporiser 1. A member 7 slidably supported at 9 is connected to a rod 10 pivotally secured to a drive disc 11 which rotates to produce a reciprocating motion in the direction of arrow 12. This causes the formation within tube 4 of individual liquid columns separated by columns of air. Vessel 5 can be adjusted to allow for the drop in liquid level. The end of tube 4 can be made to remain in the solution 6 during a reciprocating cycle or be lifted above the liquid level. In a second embodiment, Fig. 2 (not shown), three solutions in a divided vessel (14) are successively fed to the vaporiser 1 through the tube 4 which is simultaneously rotated and lifted by a rod (18) and disc (19) driven by a motor (22). In a third embodiment, Fig. 4 (not shown), two solutions (43), (44) are alternately fed through respective flexible tubes (37), (38) to the vaporiser 1. In a fourth embodiment, Fig. 3 (not shown), the solution is fed under pressure by a piston (26) through a tube (23) which is reciprocated.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19681815958 DE1815958B1 (en) | 1968-12-20 | 1968-12-20 | Device for the modulated supply of a sample liquid to a spectroscopic light source, e.g. a flame |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1268530A true GB1268530A (en) | 1972-03-29 |
Family
ID=5716877
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB60992/69A Expired GB1268530A (en) | 1968-12-20 | 1969-12-15 | Method of and apparatus for modulated sample feed in the spectrochemical analysis of solution |
Country Status (3)
Country | Link |
---|---|
US (1) | US3625614A (en) |
DE (1) | DE1815958B1 (en) |
GB (1) | GB1268530A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3927768A1 (en) * | 1989-08-23 | 1991-02-28 | Perkin Elmer Corp | METHOD FOR DETERMINING CONCENTRATION BY MEANS OF ATOMEMISSION SPECTROSCOPY |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3740154A (en) * | 1971-10-28 | 1973-06-19 | Itt | Modulated composition flame photometer |
US4269507A (en) * | 1979-10-04 | 1981-05-26 | Aerochem Research Laboratories, Inc. | Method and apparatus for pulverizing solid materials with a grindstone and injecting particles thereof into a flame for analysis |
DE2944113A1 (en) * | 1979-10-31 | 1981-05-14 | Arno Dipl.-Phys. Dr. 7900 Ulm Müller | METHOD AND DEVICE FOR THE QUANTITATIVE ABSOLUTE DETERMINATION OF OPTICALLY ACTIVE SUBSTANCES |
BG33390A1 (en) * | 1980-11-12 | 1983-02-15 | Futekov | Apparatus for impulse dosing of liquid microsamples in atomicabsorbing spectrophotometer flame |
US4494871A (en) * | 1981-11-18 | 1985-01-22 | Nauchno-Proizvodstveno Predpriyatie "Balkan" | Device for pulse dosage of liquid microsamples into the flame of atom absorption spectrophotometer |
DE3531276A1 (en) * | 1985-09-02 | 1987-03-05 | Bodenseewerk Perkin Elmer Co | METHOD AND DEVICE FOR DETERMINING THE ZERO LINE IN ATOMIC ABSORPTION SPECTROMETERS |
IL95617A0 (en) * | 1990-09-09 | 1991-06-30 | Aviv Amirav | Pulsed flame detector method and apparatus |
JP2513082B2 (en) * | 1991-03-30 | 1996-07-03 | 株式会社島津製作所 | Atomic absorption spectrometer |
EP1672674A1 (en) * | 2004-12-17 | 2006-06-21 | Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V. | Method and system for high-throughput mass-analysis |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3469438A (en) * | 1967-04-12 | 1969-09-30 | Perkin Elmer Corp | Automatically controlled multiple sampling measurement system |
-
1968
- 1968-12-20 DE DE19681815958 patent/DE1815958B1/en active Pending
-
1969
- 1969-12-15 GB GB60992/69A patent/GB1268530A/en not_active Expired
- 1969-12-18 US US886098A patent/US3625614A/en not_active Expired - Lifetime
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3927768A1 (en) * | 1989-08-23 | 1991-02-28 | Perkin Elmer Corp | METHOD FOR DETERMINING CONCENTRATION BY MEANS OF ATOMEMISSION SPECTROSCOPY |
Also Published As
Publication number | Publication date |
---|---|
DE1815958B1 (en) | 1970-06-18 |
US3625614A (en) | 1971-12-07 |
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