GB1262401A - Benefication of ilmenite - Google Patents
Benefication of ilmeniteInfo
- Publication number
- GB1262401A GB1262401A GB07691/70A GB1769170A GB1262401A GB 1262401 A GB1262401 A GB 1262401A GB 07691/70 A GB07691/70 A GB 07691/70A GB 1769170 A GB1769170 A GB 1769170A GB 1262401 A GB1262401 A GB 1262401A
- Authority
- GB
- United Kingdom
- Prior art keywords
- leach liquor
- ilmenite
- hcl
- leaching
- content
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- YDZQQRWRVYGNER-UHFFFAOYSA-N iron;titanium;trihydrate Chemical compound O.O.O.[Ti].[Fe] YDZQQRWRVYGNER-UHFFFAOYSA-N 0.000 title abstract 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 7
- 238000002386 leaching Methods 0.000 abstract 4
- 239000000203 mixture Substances 0.000 abstract 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 abstract 2
- 229910052595 hematite Inorganic materials 0.000 abstract 2
- 239000011019 hematite Substances 0.000 abstract 2
- SZVJSHCCFOBDDC-UHFFFAOYSA-N iron(II,III) oxide Inorganic materials O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 abstract 1
- 239000000571 coke Substances 0.000 abstract 1
- 239000000567 combustion gas Substances 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- 229910052742 iron Inorganic materials 0.000 abstract 1
- LIKBJVNGSGBSGK-UHFFFAOYSA-N iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Fe+3].[Fe+3] LIKBJVNGSGBSGK-UHFFFAOYSA-N 0.000 abstract 1
- 239000002893 slag Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1204—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 preliminary treatment of ores or scrap to eliminate non- titanium constituents, e.g. iron, without attacking the titanium constituent
- C22B34/1213—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 preliminary treatment of ores or scrap to eliminate non- titanium constituents, e.g. iron, without attacking the titanium constituent by wet processes, e.g. using leaching methods or flotation techniques
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Abstract
1,262,401. Benificiation of ilmenite; iron oxide. BENILITE CORP. 14 April, 1970 [15 Oct., 1969], No. 17691/70. Headings C1A and C1N. A titaniferous ore or slag, e.g. ilmenite, ilmenite magnetite, ilmenite-hematite, titaniferous magnetite, and titaniferous hematite, is benificiated 'by leaching it in a digester with hydrochloric acid leach liquor, the leaching liquor being heated during this process by feeding into the digester a vapour mixture formed by distilling an azeotropic mixture of HCl -and -water, by which means the HCl content of the leach liquor is simultaneously replenished. The leaching may be .conducted at a pressure of 20-50 p.s.i.g. and a temperature of 108 to 145 C., and the HCl content of the leach liquor may be recovered and reused in the process either as leach liquor or as the source of the vapour mixture. The preferred HCl concentration of the leach liquor is 20% by wt., and the leaching may be performed in two counter current stages. Depending on the ferrie/ferrous content of the ore, it may first be subjected to a reducing step, e.g. with coke at 815 to 1090 C. The iron content of the used leach liquor may be obtained as the oxide by hydrolysis of the chloride at high temperatures, e.g. 260-500 C., by direct contact with combustion gases. This simultaneously regenerates the HCl leach liquor.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US86654869A | 1969-10-15 | 1969-10-15 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1262401A true GB1262401A (en) | 1972-02-02 |
Family
ID=25347844
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB07691/70A Expired GB1262401A (en) | 1969-10-15 | 1970-04-14 | Benefication of ilmenite |
Country Status (12)
| Country | Link |
|---|---|
| JP (1) | JPS558572B1 (en) |
| CY (1) | CY748A (en) |
| DE (1) | DE2004878C3 (en) |
| FR (1) | FR2065775A5 (en) |
| GB (1) | GB1262401A (en) |
| IE (1) | IE34646B1 (en) |
| IL (1) | IL35038A (en) |
| MY (1) | MY7300089A (en) |
| NO (1) | NO130392B (en) |
| PL (1) | PL81917B1 (en) |
| SE (1) | SE370414B (en) |
| ZA (1) | ZA706712B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7008602B2 (en) | 2002-04-19 | 2006-03-07 | Millennium Inorganic Chemicals, Inc. | Beneficiation of titaniferous ore with sulfuric acid |
| CN103917670A (en) * | 2011-11-08 | 2014-07-09 | 奥图泰有限公司 | Method for leaching a sulphidic metal concentrate |
| CN109179496A (en) * | 2018-09-18 | 2019-01-11 | 攀枝花中达钛业科技有限公司 | High-grade titanium dioxide and preparation method thereof |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2428003A1 (en) * | 1978-06-09 | 1980-01-04 | Uop Inc | Recovery of high purity titanium from ilmenite - by formation of tri:chloride and subsequent crystallisation from aq. soln. |
| KR101323754B1 (en) * | 2013-04-29 | 2013-10-31 | 한국지질자원연구원 | Recovery of acid and platinum group metals from leaching solution of waste catalyst |
-
1970
- 1970-02-03 DE DE2004878A patent/DE2004878C3/en not_active Expired
- 1970-02-10 JP JP1140170A patent/JPS558572B1/ja active Pending
- 1970-02-10 FR FR7004697A patent/FR2065775A5/fr not_active Expired
- 1970-04-14 GB GB07691/70A patent/GB1262401A/en not_active Expired
- 1970-07-28 SE SE7010344A patent/SE370414B/xx unknown
- 1970-08-02 IL IL35038A patent/IL35038A/en unknown
- 1970-08-24 NO NO03214/70A patent/NO130392B/no unknown
- 1970-10-01 IE IE1267/70A patent/IE34646B1/en unknown
- 1970-10-02 ZA ZA706712A patent/ZA706712B/en unknown
- 1970-10-14 PL PL1970143907A patent/PL81917B1/pl unknown
-
1973
- 1973-12-30 MY MY89/73A patent/MY7300089A/en unknown
-
1974
- 1974-06-18 CY CY74874A patent/CY748A/en unknown
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7008602B2 (en) | 2002-04-19 | 2006-03-07 | Millennium Inorganic Chemicals, Inc. | Beneficiation of titaniferous ore with sulfuric acid |
| CN103917670A (en) * | 2011-11-08 | 2014-07-09 | 奥图泰有限公司 | Method for leaching a sulphidic metal concentrate |
| CN109179496A (en) * | 2018-09-18 | 2019-01-11 | 攀枝花中达钛业科技有限公司 | High-grade titanium dioxide and preparation method thereof |
| CN109179496B (en) * | 2018-09-18 | 2021-02-02 | 攀枝花中达钛业科技有限公司 | High grade titanium dioxide and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| PL81917B1 (en) | 1975-10-31 |
| IL35038A (en) | 1974-03-14 |
| DE2004878A1 (en) | 1971-05-06 |
| IE34646L (en) | 1971-04-15 |
| FR2065775A5 (en) | 1971-08-06 |
| DE2004878C3 (en) | 1975-09-18 |
| IE34646B1 (en) | 1975-07-09 |
| MY7300089A (en) | 1973-12-31 |
| IL35038A0 (en) | 1970-10-30 |
| SE370414B (en) | 1974-10-14 |
| ZA706712B (en) | 1971-12-29 |
| DE2004878B2 (en) | 1975-01-16 |
| NO130392B (en) | 1974-08-26 |
| CY748A (en) | 1974-06-18 |
| JPS558572B1 (en) | 1980-03-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee | ||
| 728C | Application made for restoration (sect. 28/1977) | ||
| 728R | Application refused (sect. 28/1977) [restoration of lapsed patent] |