GB1189934A - A process for the preparation of a Zeolite-Based Catalyst - Google Patents
A process for the preparation of a Zeolite-Based CatalystInfo
- Publication number
- GB1189934A GB1189934A GB3951268A GB3951268A GB1189934A GB 1189934 A GB1189934 A GB 1189934A GB 3951268 A GB3951268 A GB 3951268A GB 3951268 A GB3951268 A GB 3951268A GB 1189934 A GB1189934 A GB 1189934A
- Authority
- GB
- United Kingdom
- Prior art keywords
- zeolitic material
- nickel
- tungsten
- cobalt
- molybdenum
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003054 catalyst Substances 0.000 title abstract 10
- 238000000034 method Methods 0.000 title abstract 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 abstract 24
- 239000000463 material Substances 0.000 abstract 16
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 14
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 14
- 229910052759 nickel Inorganic materials 0.000 abstract 12
- 238000011282 treatment Methods 0.000 abstract 11
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 abstract 11
- 229910052721 tungsten Inorganic materials 0.000 abstract 11
- 239000010937 tungsten Substances 0.000 abstract 11
- 239000010941 cobalt Substances 0.000 abstract 10
- 229910017052 cobalt Inorganic materials 0.000 abstract 10
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 abstract 10
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 abstract 9
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 9
- 229910052751 metal Inorganic materials 0.000 abstract 9
- 239000002184 metal Substances 0.000 abstract 9
- 229910052750 molybdenum Inorganic materials 0.000 abstract 9
- 239000011733 molybdenum Substances 0.000 abstract 9
- 239000002585 base Substances 0.000 abstract 8
- 238000001354 calcination Methods 0.000 abstract 8
- 239000000203 mixture Substances 0.000 abstract 8
- 239000000243 solution Substances 0.000 abstract 8
- 239000010457 zeolite Substances 0.000 abstract 8
- 229910021536 Zeolite Inorganic materials 0.000 abstract 7
- 150000001875 compounds Chemical class 0.000 abstract 7
- 229910052742 iron Inorganic materials 0.000 abstract 7
- 229910052757 nitrogen Inorganic materials 0.000 abstract 7
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 abstract 6
- 229910052783 alkali metal Inorganic materials 0.000 abstract 6
- 150000001340 alkali metals Chemical class 0.000 abstract 6
- 239000007864 aqueous solution Substances 0.000 abstract 6
- 230000008021 deposition Effects 0.000 abstract 6
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 6
- 238000010438 heat treatment Methods 0.000 abstract 5
- 150000003839 salts Chemical class 0.000 abstract 5
- 150000002739 metals Chemical class 0.000 abstract 4
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 abstract 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 3
- 150000003863 ammonium salts Chemical class 0.000 abstract 3
- 239000011230 binding agent Substances 0.000 abstract 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 abstract 2
- 229910018072 Al 2 O 3 Inorganic materials 0.000 abstract 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- BDAGIHXWWSANSR-UHFFFAOYSA-M Formate Chemical compound [O-]C=O BDAGIHXWWSANSR-UHFFFAOYSA-M 0.000 abstract 2
- 229910002651 NO3 Inorganic materials 0.000 abstract 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- 150000003973 alkyl amines Chemical class 0.000 abstract 2
- 239000004927 clay Substances 0.000 abstract 2
- 229930195733 hydrocarbon Natural products 0.000 abstract 2
- 150000002430 hydrocarbons Chemical class 0.000 abstract 2
- 239000001257 hydrogen Substances 0.000 abstract 2
- 229910052739 hydrogen Inorganic materials 0.000 abstract 2
- 229910021645 metal ion Inorganic materials 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 abstract 1
- KUCWUAFNGCMZDB-UHFFFAOYSA-N 2-amino-3-nitrophenol Chemical compound NC1=C(O)C=CC=C1[N+]([O-])=O KUCWUAFNGCMZDB-UHFFFAOYSA-N 0.000 abstract 1
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 abstract 1
- 239000004215 Carbon black (E152) Substances 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 abstract 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- OKIZCWYLBDKLSU-UHFFFAOYSA-M N,N,N-Trimethylmethanaminium chloride Chemical compound [Cl-].C[N+](C)(C)C OKIZCWYLBDKLSU-UHFFFAOYSA-M 0.000 abstract 1
- -1 N-substituted ammonium Chemical class 0.000 abstract 1
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 abstract 1
- NPYPAHLBTDXSSS-UHFFFAOYSA-N Potassium ion Chemical compound [K+] NPYPAHLBTDXSSS-UHFFFAOYSA-N 0.000 abstract 1
- 229910004298 SiO 2 Inorganic materials 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 abstract 1
- 229910000272 alkali metal oxide Inorganic materials 0.000 abstract 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 abstract 1
- 150000001342 alkaline earth metals Chemical class 0.000 abstract 1
- 229910000323 aluminium silicate Inorganic materials 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical compound [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 abstract 1
- 239000011609 ammonium molybdate Substances 0.000 abstract 1
- 229940010552 ammonium molybdate Drugs 0.000 abstract 1
- 235000018660 ammonium molybdate Nutrition 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 239000000440 bentonite Substances 0.000 abstract 1
- 229910000278 bentonite Inorganic materials 0.000 abstract 1
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 abstract 1
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 abstract 1
- 229910001424 calcium ion Inorganic materials 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 238000004517 catalytic hydrocracking Methods 0.000 abstract 1
- 239000000470 constituent Substances 0.000 abstract 1
- 238000005336 cracking Methods 0.000 abstract 1
- 230000002950 deficient Effects 0.000 abstract 1
- 230000000694 effects Effects 0.000 abstract 1
- 239000012013 faujasite Substances 0.000 abstract 1
- 239000008246 gaseous mixture Substances 0.000 abstract 1
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract 1
- 238000005342 ion exchange Methods 0.000 abstract 1
- 239000011707 mineral Substances 0.000 abstract 1
- 235000010755 mineral Nutrition 0.000 abstract 1
- VLAPMBHFAWRUQP-UHFFFAOYSA-L molybdic acid Chemical compound O[Mo](O)(=O)=O VLAPMBHFAWRUQP-UHFFFAOYSA-L 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- 150000007524 organic acids Chemical class 0.000 abstract 1
- 125000001477 organic nitrogen group Chemical group 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 239000008188 pellet Substances 0.000 abstract 1
- 229910001414 potassium ion Inorganic materials 0.000 abstract 1
- 239000000843 powder Substances 0.000 abstract 1
- 230000008929 regeneration Effects 0.000 abstract 1
- 238000011069 regeneration method Methods 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 229910001415 sodium ion Inorganic materials 0.000 abstract 1
- 229910021653 sulphate ion Inorganic materials 0.000 abstract 1
- KJFVITRRNTVAPC-UHFFFAOYSA-L tetramethylazanium;sulfate Chemical compound C[N+](C)(C)C.C[N+](C)(C)C.[O-]S([O-])(=O)=O KJFVITRRNTVAPC-UHFFFAOYSA-L 0.000 abstract 1
- 229960004418 trolamine Drugs 0.000 abstract 1
- CMPGARWFYBADJI-UHFFFAOYSA-L tungstic acid Chemical compound O[W](O)(=O)=O CMPGARWFYBADJI-UHFFFAOYSA-L 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/076—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof containing arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
Landscapes
- Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Catalysts (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB3951268A GB1189934A (en) | 1968-08-19 | 1968-08-19 | A process for the preparation of a Zeolite-Based Catalyst |
| NL6912516A NL161994B (nl) | 1968-08-19 | 1969-08-18 | Werkwijze voor de bereiding van een op zeoliet gebaseerde katalysator met een laag alkalimetaal- gehalte. |
| FR6928217A FR2015902A1 (en) | 1968-08-19 | 1969-08-18 | Low sodium content zeolite based hydroforming - catalysts |
| JP6498669A JPS4822590B1 (enrdf_load_stackoverflow) | 1968-08-19 | 1969-08-18 | |
| BE737585D BE737585A (enrdf_load_stackoverflow) | 1968-08-19 | 1969-08-18 | |
| DE19691941947 DE1941947C3 (de) | 1968-08-19 | 1969-08-18 | Verfahren zur Herstellung eines Katalysators auf Zeolithbasis und seine Verwendung beim Hydrokracken von Kohlenwasserstoffölen |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB3951268A GB1189934A (en) | 1968-08-19 | 1968-08-19 | A process for the preparation of a Zeolite-Based Catalyst |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1189934A true GB1189934A (en) | 1970-04-29 |
Family
ID=10409970
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3951268A Expired GB1189934A (en) | 1968-08-19 | 1968-08-19 | A process for the preparation of a Zeolite-Based Catalyst |
Country Status (6)
| Country | Link |
|---|---|
| JP (1) | JPS4822590B1 (enrdf_load_stackoverflow) |
| BE (1) | BE737585A (enrdf_load_stackoverflow) |
| DE (1) | DE1941947C3 (enrdf_load_stackoverflow) |
| FR (1) | FR2015902A1 (enrdf_load_stackoverflow) |
| GB (1) | GB1189934A (enrdf_load_stackoverflow) |
| NL (1) | NL161994B (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2358485A1 (de) * | 1973-11-23 | 1975-05-28 | Union Oil Co | Hydrothermalstabile, ammoniakstabile y-zeolith-zusammensetzung und deren verwendung |
| DE2366533C2 (de) * | 1973-11-23 | 1986-05-15 | Union Oil Co. Of California, Los Angeles, Calif. | Verfahren zur Herstellung eines hochtemperaturbeständigen, ammoniakstabilen Y-Zeoliths und dessen Verwendung |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS50122281U (enrdf_load_stackoverflow) * | 1974-03-20 | 1975-10-06 | ||
| JPS52109884U (enrdf_load_stackoverflow) * | 1976-02-17 | 1977-08-20 | ||
| FR2994394B1 (fr) * | 2012-08-09 | 2015-08-21 | Eurecat Sa | Procede de passivation par un compose azote d'un catalyseur zeolitique, en particulier d'un catalyseur d'hydrocraquage |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2510189A (en) * | 1948-02-16 | 1950-06-06 | Union Oil Co | Supported catalyst and preparation thereof |
| NL68368C (enrdf_load_stackoverflow) * | 1949-03-31 | |||
| US2967159A (en) * | 1957-05-22 | 1961-01-03 | Exxon Research Engineering Co | Hydrodesulfurization catalyst and method of preparing same |
| US2983670A (en) * | 1958-06-02 | 1961-05-09 | Union Oil Co | Hydrocracking process and catalyst |
| US3293192A (en) * | 1965-08-23 | 1966-12-20 | Grace W R & Co | Zeolite z-14us and method of preparation thereof |
| US3392108A (en) * | 1967-03-13 | 1968-07-09 | Exxon Research Engineering Co | Process for preparing mixed nonnoble metal catalyst compositions and processes utilizing same |
| US3354077A (en) * | 1966-03-30 | 1967-11-21 | Union Oil Co | Stabilized zeolites and use thereof for hydrocarbon conversions |
| US3394074A (en) * | 1967-04-03 | 1968-07-23 | Exxon Research Engineering Co | Single reactor hydrocracking process with mixed nonnoble metal catalyst for full boiling raw feed |
-
1968
- 1968-08-19 GB GB3951268A patent/GB1189934A/en not_active Expired
-
1969
- 1969-08-18 DE DE19691941947 patent/DE1941947C3/de not_active Expired
- 1969-08-18 BE BE737585D patent/BE737585A/xx not_active IP Right Cessation
- 1969-08-18 NL NL6912516A patent/NL161994B/xx not_active IP Right Cessation
- 1969-08-18 JP JP6498669A patent/JPS4822590B1/ja active Pending
- 1969-08-18 FR FR6928217A patent/FR2015902A1/fr not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2358485A1 (de) * | 1973-11-23 | 1975-05-28 | Union Oil Co | Hydrothermalstabile, ammoniakstabile y-zeolith-zusammensetzung und deren verwendung |
| DE2366533C2 (de) * | 1973-11-23 | 1986-05-15 | Union Oil Co. Of California, Los Angeles, Calif. | Verfahren zur Herstellung eines hochtemperaturbeständigen, ammoniakstabilen Y-Zeoliths und dessen Verwendung |
Also Published As
| Publication number | Publication date |
|---|---|
| NL6912516A (enrdf_load_stackoverflow) | 1970-02-23 |
| JPS4822590B1 (enrdf_load_stackoverflow) | 1973-07-06 |
| DE1941947C3 (de) | 1983-02-10 |
| DE1941947B2 (de) | 1977-12-08 |
| DE1941947A1 (de) | 1970-02-26 |
| FR2015902A1 (en) | 1970-04-30 |
| NL161994B (nl) | 1979-11-15 |
| BE737585A (enrdf_load_stackoverflow) | 1970-02-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PE20 | Patent expired after termination of 20 years |