GB1160765A - Process for the Preparation of Ruthenium Carbonyl - Google Patents

Process for the Preparation of Ruthenium Carbonyl

Info

Publication number
GB1160765A
GB1160765A GB3578866A GB3578866A GB1160765A GB 1160765 A GB1160765 A GB 1160765A GB 3578866 A GB3578866 A GB 3578866A GB 3578866 A GB3578866 A GB 3578866A GB 1160765 A GB1160765 A GB 1160765A
Authority
GB
United Kingdom
Prior art keywords
ruthenium
tri
enolizable
sodium
compound
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3578866A
Inventor
John Paton Candlin
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Imperial Chemical Industries Ltd
Original Assignee
Imperial Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Imperial Chemical Industries Ltd filed Critical Imperial Chemical Industries Ltd
Priority to GB3578866A priority Critical patent/GB1160765A/en
Publication of GB1160765A publication Critical patent/GB1160765A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G55/00—Compounds of ruthenium, rhodium, palladium, osmium, iridium, or platinum
    • C01G55/007—Compounds containing at least one carbonyl group

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1,160,765. Tri-ruthenium dodecacarbonyl. IMPERIAL CHEMICAL INDUSTRIES Ltd. 10 Aug., 1967 [10 Aug., 1966], No. 35788/66. Heading C1A. Tri-ruthenium dodecacarbonyl is made by reacting (i) an inorganic Ru salt (ii) an alkali metal or alkaline earth metal compound of an organic acid or an enolizable compound and (iii) a mixture of carbon monoxide and hydrogen in a solvent. Component (ii) may be replaced by the alkali metal or alkaline earth metal and a free organic acid or enolizable compound. The preferred Ru salt is ruthenium tri-chloride and the preferred solvents are methanol, ethanol and dimethyl formamide. The organic acids may be succinic, stearic, acetic, benzoic, and naphthenic acids, the enolizable compounds may be acetylacetone, methyl acetoacetate, and naphthols. Examples are given of the reaction of ruthenium chloride in methanol with (1) sodium acetyl-acetonate (2) sodium metal and acetyl acetone and (3) sodium naphthenate.
GB3578866A 1966-08-10 1966-08-10 Process for the Preparation of Ruthenium Carbonyl Expired GB1160765A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB3578866A GB1160765A (en) 1966-08-10 1966-08-10 Process for the Preparation of Ruthenium Carbonyl

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB3578866A GB1160765A (en) 1966-08-10 1966-08-10 Process for the Preparation of Ruthenium Carbonyl

Publications (1)

Publication Number Publication Date
GB1160765A true GB1160765A (en) 1969-08-06

Family

ID=10381563

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3578866A Expired GB1160765A (en) 1966-08-10 1966-08-10 Process for the Preparation of Ruthenium Carbonyl

Country Status (1)

Country Link
GB (1) GB1160765A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5531120B1 (en) * 2013-01-21 2014-06-25 田中貴金属工業株式会社 Method for producing dodecacarbonyltriruthenium
US9290841B2 (en) 2011-08-03 2016-03-22 Tanaka Kikinzoku Kogyo K.K. Organoruthenium compound for chemical vapor deposition raw material and production method for the organoruthenium compound

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9290841B2 (en) 2011-08-03 2016-03-22 Tanaka Kikinzoku Kogyo K.K. Organoruthenium compound for chemical vapor deposition raw material and production method for the organoruthenium compound
JP5531120B1 (en) * 2013-01-21 2014-06-25 田中貴金属工業株式会社 Method for producing dodecacarbonyltriruthenium
WO2014112613A1 (en) * 2013-01-21 2014-07-24 田中貴金属工業株式会社 Production method for dodecacarbonyl triruthenium
JP2014139111A (en) * 2013-01-21 2014-07-31 Tanaka Kikinzoku Kogyo Kk Method for manufacturing dodecacarbonyl triruthenium
US9266916B2 (en) 2013-01-21 2016-02-23 Tanaka Kikinzoku Kogyo K.K. Production method for dodecacarbonyl triruthenium

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Legal Events

Date Code Title Description
PS Patent sealed
PLNP Patent lapsed through nonpayment of renewal fees