GB1097947A - Improvements in and relating to the manufacture of aluminium chloride - Google Patents

Improvements in and relating to the manufacture of aluminium chloride

Info

Publication number
GB1097947A
GB1097947A GB977765A GB977765A GB1097947A GB 1097947 A GB1097947 A GB 1097947A GB 977765 A GB977765 A GB 977765A GB 977765 A GB977765 A GB 977765A GB 1097947 A GB1097947 A GB 1097947A
Authority
GB
United Kingdom
Prior art keywords
ticl4
liquid
alcl3
aluminium chloride
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB977765A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
American Potash and Chemical Corp
Original Assignee
American Potash and Chemical Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by American Potash and Chemical Corp filed Critical American Potash and Chemical Corp
Publication of GB1097947A publication Critical patent/GB1097947A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/48—Halides, with or without other cations besides aluminium
    • C01F7/56—Chlorides
    • C01F7/58—Preparation of anhydrous aluminium chloride
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/48—Halides, with or without other cations besides aluminium
    • C01F7/56—Chlorides
    • C01F7/58—Preparation of anhydrous aluminium chloride
    • C01F7/60—Preparation of anhydrous aluminium chloride from oxygen-containing aluminium compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

Aluminium chloride is produced by contacting a mixture of aluminium particles and liquid TiCl4 at 120-150 DEG C. with chlorine, either by passing gaseous Cl2 up through the mixture or using liquid Cl2 mixed with the TiCl4. When the temperature is above the b.pt. of TiCl4, 136 degrees, superatmospheric pressure is applied to prevent boiling. Al pellets and hot TiCl4 are introduced into a steam, water or oil jacketed reaction vessel of glass, steel, Ni, or alloy, and Cl2 is bubbled through or introduced in TiCl4, while liquid TiCl4 + AlCl3 is withdraw at the top. The reaction is carried out under reflux. Pure AlCl3 may be recovered from its solution in TiCl4 or the mixed halides may be oxidized in the vapour phase to produce TiO2 containing alumina.
GB977765A 1964-03-06 1965-03-08 Improvements in and relating to the manufacture of aluminium chloride Expired GB1097947A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US34990664A 1964-03-06 1964-03-06

Publications (1)

Publication Number Publication Date
GB1097947A true GB1097947A (en) 1968-01-03

Family

ID=23374471

Family Applications (1)

Application Number Title Priority Date Filing Date
GB977765A Expired GB1097947A (en) 1964-03-06 1965-03-08 Improvements in and relating to the manufacture of aluminium chloride

Country Status (5)

Country Link
BE (1) BE660709A (en)
DE (1) DE1592058A1 (en)
FR (1) FR1429587A (en)
GB (1) GB1097947A (en)
NL (1) NL6502864A (en)

Also Published As

Publication number Publication date
NL6502864A (en) 1965-09-07
FR1429587A (en) 1966-02-25
DE1592058A1 (en) 1971-02-11
BE660709A (en) 1965-07-01

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