GB1089707A - Method for preparation of adiponitrile - Google Patents
Method for preparation of adiponitrileInfo
- Publication number
- GB1089707A GB1089707A GB33107/66A GB3310766A GB1089707A GB 1089707 A GB1089707 A GB 1089707A GB 33107/66 A GB33107/66 A GB 33107/66A GB 3310766 A GB3310766 A GB 3310766A GB 1089707 A GB1089707 A GB 1089707A
- Authority
- GB
- United Kingdom
- Prior art keywords
- phosphate
- adiponitrile
- salt
- preparation
- triethyldecyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- BTGRAWJCKBQKAO-UHFFFAOYSA-N adiponitrile Chemical compound N#CCCCCC#N BTGRAWJCKBQKAO-UHFFFAOYSA-N 0.000 title abstract 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 abstract 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 abstract 2
- VKYKSIONXSXAKP-UHFFFAOYSA-N hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 abstract 2
- NCRYTHRTIYJFKL-UHFFFAOYSA-K 1-methylpyridin-1-ium phosphate Chemical compound P(=O)([O-])([O-])[O-].C[N+]1=CC=CC=C1.C[N+]1=CC=CC=C1.C[N+]1=CC=CC=C1 NCRYTHRTIYJFKL-UHFFFAOYSA-K 0.000 abstract 1
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 abstract 1
- 239000004254 Ammonium phosphate Substances 0.000 abstract 1
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 abstract 1
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 abstract 1
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical class C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 229910000148 ammonium phosphate Inorganic materials 0.000 abstract 1
- 235000019289 ammonium phosphates Nutrition 0.000 abstract 1
- RDHPKYGYEGBMSE-UHFFFAOYSA-N bromoethane Chemical compound CCBr RDHPKYGYEGBMSE-UHFFFAOYSA-N 0.000 abstract 1
- 229910052681 coesite Inorganic materials 0.000 abstract 1
- 229910052906 cristobalite Inorganic materials 0.000 abstract 1
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 abstract 1
- 238000005868 electrolysis reaction Methods 0.000 abstract 1
- 239000008151 electrolyte solution Substances 0.000 abstract 1
- 235000010299 hexamethylene tetramine Nutrition 0.000 abstract 1
- 239000004312 hexamethylene tetramine Substances 0.000 abstract 1
- 229910000403 monosodium phosphate Inorganic materials 0.000 abstract 1
- 235000019799 monosodium phosphate Nutrition 0.000 abstract 1
- 230000007935 neutral effect Effects 0.000 abstract 1
- 150000007519 polyprotic acids Polymers 0.000 abstract 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 239000000377 silicon dioxide Substances 0.000 abstract 1
- 235000012239 silicon dioxide Nutrition 0.000 abstract 1
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 abstract 1
- 239000001488 sodium phosphate Substances 0.000 abstract 1
- 229910052682 stishovite Inorganic materials 0.000 abstract 1
- 229910021653 sulphate ion Inorganic materials 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
- 229910052905 tridymite Inorganic materials 0.000 abstract 1
- -1 triethyldecyl Chemical group 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B3/00—Electrolytic production of organic compounds
- C25B3/20—Processes
- C25B3/29—Coupling reactions
- C25B3/295—Coupling reactions hydrodimerisation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1019640A SU253767A1 (ru) | 1965-07-23 | Способ получения адипонитрила |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1089707A true GB1089707A (en) | 1967-11-08 |
Family
ID=20438688
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB33107/66A Expired GB1089707A (en) | 1965-07-23 | 1966-07-22 | Method for preparation of adiponitrile |
Country Status (5)
| Country | Link |
|---|---|
| BE (1) | BE684436A (enrdf_load_stackoverflow) |
| DE (1) | DE1593582A1 (enrdf_load_stackoverflow) |
| GB (1) | GB1089707A (enrdf_load_stackoverflow) |
| LU (1) | LU51624A1 (enrdf_load_stackoverflow) |
| NL (1) | NL156684B (enrdf_load_stackoverflow) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4230541A (en) * | 1979-09-21 | 1980-10-28 | Monsanto Company | Pretreatment of cathodes in electrohydrodimerization of acrylonitrile |
| US4250001A (en) * | 1979-06-19 | 1981-02-10 | Monsanto Company | Pretreatment of cathodes in electrohydrodimerization of acrylonitrile |
| US4306949A (en) | 1979-12-19 | 1981-12-22 | Monsanto Company | Electrohydrodimerization process |
-
1966
- 1966-07-20 BE BE684436D patent/BE684436A/xx not_active IP Right Cessation
- 1966-07-22 DE DE19661593582 patent/DE1593582A1/de active Pending
- 1966-07-22 GB GB33107/66A patent/GB1089707A/en not_active Expired
- 1966-07-22 LU LU51624A patent/LU51624A1/xx unknown
- 1966-07-22 NL NL6610378.A patent/NL156684B/xx not_active IP Right Cessation
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4250001A (en) * | 1979-06-19 | 1981-02-10 | Monsanto Company | Pretreatment of cathodes in electrohydrodimerization of acrylonitrile |
| US4230541A (en) * | 1979-09-21 | 1980-10-28 | Monsanto Company | Pretreatment of cathodes in electrohydrodimerization of acrylonitrile |
| US4306949A (en) | 1979-12-19 | 1981-12-22 | Monsanto Company | Electrohydrodimerization process |
Also Published As
| Publication number | Publication date |
|---|---|
| BE684436A (enrdf_load_stackoverflow) | 1967-01-03 |
| DE1593582A1 (enrdf_load_stackoverflow) | 1971-05-06 |
| LU51624A1 (enrdf_load_stackoverflow) | 1966-09-22 |
| NL6610378A (enrdf_load_stackoverflow) | 1967-01-24 |
| NL156684B (nl) | 1978-05-16 |
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