GB1032379A - Production of dimethylolglyoxalmonourcine - Google Patents

Production of dimethylolglyoxalmonourcine

Info

Publication number
GB1032379A
GB1032379A GB1511465A GB1511465A GB1032379A GB 1032379 A GB1032379 A GB 1032379A GB 1511465 A GB1511465 A GB 1511465A GB 1511465 A GB1511465 A GB 1511465A GB 1032379 A GB1032379 A GB 1032379A
Authority
GB
United Kingdom
Prior art keywords
glyoxal
aqueous solution
formaldehyde
reacting
dimethylolglyoxalmonourcine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB1511465A
Inventor
Harro Petersen
Hans Joachim Grasshoff
Hans Brandris
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Badische Anilin and Sodafabrik AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE, Badische Anilin and Sodafabrik AG filed Critical BASF SE
Publication of GB1032379A publication Critical patent/GB1032379A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/04—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
    • C07D233/28—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D233/30—Oxygen or sulfur atoms
    • C07D233/40—Two or more oxygen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

Dimethylolglyoxalmonoureine is made by reacting urea with an equimolar amount of glyoxal in an aqueous medium at pH of 3.8 to 4.2 at 25-60 DEG C. and reacting the intermediate thus obtained, without isolation, with two molar equivalents of formaldehyde at a pH of 7 to 7.5 at 25-60 DEG C. As glyoxal in aqueous solution shows an acid reaction it is usually necessary to adjust the pH at both stages with an alkaline reagent, preferably sodium carbonate or sodium hydrogen carbonate. The glyoxal is preferably used as a 40% by wt. aqueous solution and the formaldehyde as a 30-40% by wt. aqueous solution.
GB1511465A 1964-04-11 1965-04-09 Production of dimethylolglyoxalmonourcine Expired GB1032379A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEB76291A DE1266307B (en) 1964-04-11 1964-04-11 Process for the preparation of dimethylolglyoxalmonourein

Publications (1)

Publication Number Publication Date
GB1032379A true GB1032379A (en) 1966-06-08

Family

ID=6979013

Family Applications (1)

Application Number Title Priority Date Filing Date
GB1511465A Expired GB1032379A (en) 1964-04-11 1965-04-09 Production of dimethylolglyoxalmonourcine

Country Status (2)

Country Link
DE (1) DE1266307B (en)
GB (1) GB1032379A (en)

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1010099A (en) * 1948-04-26 1952-06-13 Bozel Maletra Water-soluble condensation products for textile finishing
FR1060331A (en) * 1951-08-02 1954-04-01 Basf Ag Process for obtaining ureins from ethanedial
DE910475C (en) * 1951-08-17 1954-05-03 Basf Ag Process for the production of nitrogen-containing condensation products

Also Published As

Publication number Publication date
DE1266307B (en) 1968-04-18

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