GB1005473A - Process for preparing a hydrophobic wet-precipitated silica - Google Patents

Process for preparing a hydrophobic wet-precipitated silica

Info

Publication number
GB1005473A
GB1005473A GB2018/64A GB201864A GB1005473A GB 1005473 A GB1005473 A GB 1005473A GB 2018/64 A GB2018/64 A GB 2018/64A GB 201864 A GB201864 A GB 201864A GB 1005473 A GB1005473 A GB 1005473A
Authority
GB
United Kingdom
Prior art keywords
silica
silane
suspension
preparing
precipitated silica
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2018/64A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Evonik Operations GmbH
Original Assignee
Degussa GmbH
Deutsche Gold und Silber Scheideanstalt
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Degussa GmbH, Deutsche Gold und Silber Scheideanstalt filed Critical Degussa GmbH
Publication of GB1005473A publication Critical patent/GB1005473A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/34—Silicon-containing compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/34—Silicon-containing compounds
    • C08K3/36—Silica
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • C09C1/309—Combinations of treatments provided for in groups C09C1/3009 - C09C1/3081
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/04—Physical treatment, e.g. grinding, treatment with ultrasonic vibrations
    • C09C3/043—Drying, calcination
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/12—Treatment with organosilicon compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/10—Solid density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/90—Other properties not specified above

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Composite Materials (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • General Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Physics & Mathematics (AREA)
  • Silicon Compounds (AREA)

Abstract

Hydrophobic silica is prepared by precipitating silica from alkali metal silicate solution with mineral acid, adding an organohalosilane to the suspension, filtering, washing and drying the precipitate, and heating at 300-400 DEG C. The silane may have 2 or 3 halogen atoms, preferably Cl, and the organic radicals may be saturated or unsaturated aliphatic, cycloaliphatic, or aromatic radicals containing up to 20 carbon atoms. Dimethyl dichlorosilane is exemplified. The silane, in amounts of 10-20% by weight of the dry silica before treatment, may be added with stirring at 50-90 DEG C. to a suspension at a pH of 5. The final heat treatment may be carried out in a muffle furnace or in a whirling or fluidized bed. The treated silica may be used as a filler for polychlorobutadiene.
GB2018/64A 1963-01-23 1964-01-16 Process for preparing a hydrophobic wet-precipitated silica Expired GB1005473A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DED40746A DE1172245B (en) 1963-01-23 1963-01-23 Process for the production of a hydrophobic wet precipitated silica

Publications (1)

Publication Number Publication Date
GB1005473A true GB1005473A (en) 1965-09-22

Family

ID=7045630

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2018/64A Expired GB1005473A (en) 1963-01-23 1964-01-16 Process for preparing a hydrophobic wet-precipitated silica

Country Status (7)

Country Link
AT (1) AT244302B (en)
BE (1) BE642816A (en)
CH (1) CH456551A (en)
DE (1) DE1172245B (en)
FR (1) FR1379435A (en)
GB (1) GB1005473A (en)
NL (1) NL129708C (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4839378A (en) * 1971-09-25 1973-06-09
US7811670B2 (en) 2005-08-26 2010-10-12 Ppg Industries Ohio, Inc. Coating compositions exhibiting corrosion resistance properties, related coated substrates, and methods

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1567449B1 (en) * 1965-12-10 1970-11-12 Degussa Process for the production of hydrophobic fine-grained powders and / or granules from water glass
DE2729244A1 (en) * 1977-06-29 1979-01-04 Degussa FELLING SILICIC ACID
DE10048616A1 (en) 2000-09-30 2002-04-11 Degussa Doped precipitated silica
DE10062449A1 (en) 2000-12-14 2002-06-20 Degussa Doped precipitated silica
US20120077918A1 (en) 2010-07-01 2012-03-29 Basf Se Mixtures containing effective materials and inorganic compounds with high surface area

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4839378A (en) * 1971-09-25 1973-06-09
US7811670B2 (en) 2005-08-26 2010-10-12 Ppg Industries Ohio, Inc. Coating compositions exhibiting corrosion resistance properties, related coated substrates, and methods
US8288000B2 (en) 2005-08-26 2012-10-16 Ppg Industries Ohio, Inc. Coating compositions exhibiting corrosion resistance properties, related coated substrates, and methods

Also Published As

Publication number Publication date
AT244302B (en) 1965-12-27
NL302524A (en) 1965-10-25
NL129708C (en) 1970-10-15
CH456551A (en) 1968-07-31
DE1172245B (en) 1964-06-18
BE642816A (en) 1964-05-15
FR1379435A (en) 1964-11-20

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