FR867145A - Perfectionnements à la fabrication des esters nitriques - Google Patents
Perfectionnements à la fabrication des esters nitriquesInfo
- Publication number
- FR867145A FR867145A FR867145DA FR867145A FR 867145 A FR867145 A FR 867145A FR 867145D A FR867145D A FR 867145DA FR 867145 A FR867145 A FR 867145A
- Authority
- FR
- France
- Prior art keywords
- alcohol
- amyl
- nitric acid
- water
- nitrate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000002148 esters Chemical class 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- -1 Alkyl nitrates Chemical class 0.000 abstract 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 4
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 3
- 229910017604 nitric acid Inorganic materials 0.000 abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 3
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 abstract 2
- 239000004202 carbamide Substances 0.000 abstract 2
- 230000032050 esterification Effects 0.000 abstract 2
- 238000005886 esterification reaction Methods 0.000 abstract 2
- 125000000740 n-pentyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- 229910002651 NO3 Inorganic materials 0.000 abstract 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 abstract 1
- 238000009825 accumulation Methods 0.000 abstract 1
- 150000001298 alcohols Chemical class 0.000 abstract 1
- 238000010533 azeotropic distillation Methods 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 239000003153 chemical reaction reagent Substances 0.000 abstract 1
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 abstract 1
- 239000003085 diluting agent Substances 0.000 abstract 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 abstract 1
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 abstract 1
- 125000001972 isopentyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])C([H])([H])* 0.000 abstract 1
- GAPFWGOSHOCNBM-UHFFFAOYSA-N isopropyl nitrate Chemical compound CC(C)O[N+]([O-])=O GAPFWGOSHOCNBM-UHFFFAOYSA-N 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- LRMHVVPPGGOAJQ-UHFFFAOYSA-N methyl nitrate Chemical compound CO[N+]([O-])=O LRMHVVPPGGOAJQ-UHFFFAOYSA-N 0.000 abstract 1
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 abstract 1
- 125000001280 n-hexyl group Chemical group C(CCCCC)* 0.000 abstract 1
- TXQBMQNFXYOIPT-UHFFFAOYSA-N octyl nitrate Chemical group CCCCCCCCO[N+]([O-])=O TXQBMQNFXYOIPT-UHFFFAOYSA-N 0.000 abstract 1
- 239000012071 phase Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/02—Preparation of esters of nitric acid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C203/00—Esters of nitric or nitrous acid
- C07C203/02—Esters of nitric acid
- C07C203/04—Esters of nitric acid having nitrate groups bound to acyclic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C203/00—Esters of nitric or nitrous acid
- C07C203/02—Esters of nitric acid
- C07C203/08—Esters of nitric acid having nitrate groups bound to carbon atoms of rings other than six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Applications Claiming Priority (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US225908A US2294849A (en) | 1938-08-20 | 1938-08-20 | Manufacture of nitric acid esters |
| GB5722/40A GB540050A (en) | 1938-08-20 | 1940-03-29 | Improvements in or relating to manufacture of nitric acid esters |
| NL97876A NL65504C (enrdf_load_stackoverflow) | 1938-08-20 | 1940-05-06 | |
| FR867145T | 1940-05-15 | ||
| CH237619T | 1940-05-24 | ||
| BE440425T | 1941-01-30 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| FR867145A true FR867145A (fr) | 1941-10-02 |
Family
ID=9801395
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR867145D Expired FR867145A (fr) | 1938-08-20 | 1940-05-15 | Perfectionnements à la fabrication des esters nitriques |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US2294849A (enrdf_load_stackoverflow) |
| BE (1) | BE440425A (enrdf_load_stackoverflow) |
| CH (1) | CH237619A (enrdf_load_stackoverflow) |
| FR (1) | FR867145A (enrdf_load_stackoverflow) |
| GB (1) | GB540050A (enrdf_load_stackoverflow) |
| NL (1) | NL65504C (enrdf_load_stackoverflow) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE504749A (enrdf_load_stackoverflow) * | 1950-07-24 | |||
| US2750415A (en) * | 1952-07-25 | 1956-06-12 | Du Pont | Separation and oxidation of cyclohexyl nitrate and related compounds |
| US2768964A (en) * | 1953-05-27 | 1956-10-30 | Du Pont | Production of alkyl nitrates |
| US2977384A (en) * | 1953-07-10 | 1961-03-28 | Ici Ltd | Production of alkyl nitrates |
| BE534134A (enrdf_load_stackoverflow) * | 1953-09-16 | 1900-01-01 | ||
| DE1046007B (de) * | 1954-07-02 | 1958-12-11 | Nynaes Petroleum Ab | Verfahren zur Herstellung von Isopropylnitrat |
| US2736742A (en) * | 1954-07-08 | 1956-02-28 | Nitroglycerin Ab | Method of processing acid nitrated organic products |
| US3409620A (en) * | 1967-02-06 | 1968-11-05 | Mario Biazzi Sa Dr Ing | Continuous manufacture in vacuum of nitric esters and/or organic nitro compounds |
| DE2820890C2 (de) * | 1978-05-12 | 1986-09-25 | Josef Meissner GmbH & Co, 5000 Köln | Verfahren zur kontinuierlichen Herstellung von Salpetersäureestern mehrwertiger Alkohole |
| US5162568A (en) * | 1983-11-21 | 1992-11-10 | E. I. Du Pont De Nemours And Company | Nitration of alkanols |
| US4536190A (en) * | 1984-04-02 | 1985-08-20 | Ethyl Corporation | Cetane improver composition |
| NL8802276A (nl) * | 1988-09-15 | 1990-04-02 | Cedona Pharm Bv | Geneesmiddel met relaxerende werking, dat als aktieve stof een nitraatester bevat. |
| ITMI20022410A1 (it) * | 2002-11-14 | 2004-05-15 | Dinamite Dipharma S P A | Procedimento per la nitrazione di alcandioli. |
| CN102557953B (zh) * | 2011-12-29 | 2013-11-06 | 北京理工大学 | 一种制备c4～c10烷基直链烃一元醇硝酸酯的方法 |
| JP7664247B2 (ja) | 2019-11-28 | 2025-04-17 | ペトロレオ ブラジレイロ ソシエダ アノニマ － ペトロブラス | ディーゼル用セタン価向上剤としてのグリセロール及びエタノールのエーテルの硝酸エステル及びその製造方法 |
| CN113651698B (zh) * | 2021-08-17 | 2024-01-12 | 西安万德能源化学股份有限公司 | 一种提高硝酸异丙酯合成后废酸安定性的处理方法 |
-
1938
- 1938-08-20 US US225908A patent/US2294849A/en not_active Expired - Lifetime
-
1940
- 1940-03-29 GB GB5722/40A patent/GB540050A/en not_active Expired
- 1940-05-06 NL NL97876A patent/NL65504C/xx active
- 1940-05-15 FR FR867145D patent/FR867145A/fr not_active Expired
- 1940-05-24 CH CH237619D patent/CH237619A/de unknown
-
1941
- 1941-01-30 BE BE440425D patent/BE440425A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| NL65504C (enrdf_load_stackoverflow) | 1950-04-15 |
| BE440425A (enrdf_load_stackoverflow) | 1941-02-28 |
| CH237619A (de) | 1945-05-15 |
| US2294849A (en) | 1942-09-01 |
| GB540050A (en) | 1941-10-03 |
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