FR3091283B1 - Purification d’hydroperoxyde d’alkyle par distillation en presence de methanol et d’eau - Google Patents
Purification d’hydroperoxyde d’alkyle par distillation en presence de methanol et d’eau Download PDFInfo
- Publication number
- FR3091283B1 FR3091283B1 FR1874176A FR1874176A FR3091283B1 FR 3091283 B1 FR3091283 B1 FR 3091283B1 FR 1874176 A FR1874176 A FR 1874176A FR 1874176 A FR1874176 A FR 1874176A FR 3091283 B1 FR3091283 B1 FR 3091283B1
- Authority
- FR
- France
- Prior art keywords
- water
- distillation
- methanol
- purification
- alkyl hydroperoxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 title abstract 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title abstract 4
- 238000004821 distillation Methods 0.000 title abstract 3
- 238000000746 purification Methods 0.000 title abstract 3
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 title abstract 2
- -1 alkyl hydroperoxide Chemical compound 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 150000002978 peroxides Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
- C07C407/003—Separation; Purification; Stabilisation; Use of additives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURIFICATION D’HYDROPEROXYDE D’ALKYLE PAR DISTILLATION EN PRESENCE DE METHANOL ET D’EAU L’invention concerne un procédé de purification d’un hydroperoxyde d’alkyle de son peroxyde de dialkyle, comprenant une étape de distillation en présence de méthanol et d’eau.
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR1874176A FR3091283B1 (fr) | 2018-12-26 | 2018-12-26 | Purification d’hydroperoxyde d’alkyle par distillation en presence de methanol et d’eau |
PCT/FR2019/053243 WO2020136335A1 (fr) | 2018-12-26 | 2019-12-20 | Purification d'hydroperoxyde d'alkyle par distillation en presence de methanol et d'eau |
EP19848899.1A EP3902782A1 (fr) | 2018-12-26 | 2019-12-20 | Purification d'hydroperoxyde d'alkyle par distillation en presence de methanol et d'eau |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR1874176A FR3091283B1 (fr) | 2018-12-26 | 2018-12-26 | Purification d’hydroperoxyde d’alkyle par distillation en presence de methanol et d’eau |
Publications (2)
Publication Number | Publication Date |
---|---|
FR3091283A1 FR3091283A1 (fr) | 2020-07-03 |
FR3091283B1 true FR3091283B1 (fr) | 2021-06-25 |
Family
ID=66776499
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR1874176A Active FR3091283B1 (fr) | 2018-12-26 | 2018-12-26 | Purification d’hydroperoxyde d’alkyle par distillation en presence de methanol et d’eau |
Country Status (3)
Country | Link |
---|---|
EP (1) | EP3902782A1 (fr) |
FR (1) | FR3091283B1 (fr) |
WO (1) | WO2020136335A1 (fr) |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2430864A (en) * | 1945-01-30 | 1947-11-18 | Union Oil Co | Hydrocarbon peroxides |
GB816200A (en) * | 1957-02-28 | 1959-07-08 | Bataafsche Petroleum | Process for the separation of diisopropyl benzene dihydroperoxides |
FR1506296A (fr) * | 1966-03-11 | 1967-12-22 | Charbonnages De France | Procédé d'oxydation en continu de composés organiques |
US3449217A (en) * | 1968-01-05 | 1969-06-10 | Halcon International Inc | Process of buffering a neutralized t-butyl hydroperoxide during distillation |
DE2916572A1 (de) | 1979-04-24 | 1980-11-13 | Peroxid Chemie Gmbh | Verfahren zur destillativen trennung von tert.-alkylhydroperoxiden und di- tert.-alkylperoxiden |
CN107501152B (zh) * | 2017-08-16 | 2019-09-20 | 中山大学惠州研究院 | 一种叔丁基过氧化氢的分离方法 |
-
2018
- 2018-12-26 FR FR1874176A patent/FR3091283B1/fr active Active
-
2019
- 2019-12-20 EP EP19848899.1A patent/EP3902782A1/fr active Pending
- 2019-12-20 WO PCT/FR2019/053243 patent/WO2020136335A1/fr unknown
Also Published As
Publication number | Publication date |
---|---|
WO2020136335A1 (fr) | 2020-07-02 |
EP3902782A1 (fr) | 2021-11-03 |
FR3091283A1 (fr) | 2020-07-03 |
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Legal Events
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PLFP | Fee payment |
Year of fee payment: 2 |
|
PLSC | Publication of the preliminary search report |
Effective date: 20200703 |
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PLFP | Fee payment |
Year of fee payment: 3 |
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PLFP | Fee payment |
Year of fee payment: 4 |
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PLFP | Fee payment |
Year of fee payment: 5 |
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PLFP | Fee payment |
Year of fee payment: 6 |