FR3091280B1 - Purification d’hydroperoxyde d’alkyle par distillation extractive - Google Patents

Purification d’hydroperoxyde d’alkyle par distillation extractive Download PDF

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Publication number
FR3091280B1
FR3091280B1 FR1874177A FR1874177A FR3091280B1 FR 3091280 B1 FR3091280 B1 FR 3091280B1 FR 1874177 A FR1874177 A FR 1874177A FR 1874177 A FR1874177 A FR 1874177A FR 3091280 B1 FR3091280 B1 FR 3091280B1
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FR
France
Prior art keywords
purification
alkyl hydroperoxide
extractive distillation
distillation
hydroperoxide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1874177A
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English (en)
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FR3091280A1 (fr
Inventor
Hemelryck Bruno Van
Serge Hub
Philippe Maj
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Arkema France SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arkema France SA filed Critical Arkema France SA
Priority to FR1874177A priority Critical patent/FR3091280B1/fr
Priority to CN201980042744.0A priority patent/CN112351968A/zh
Priority to US17/417,409 priority patent/US20220073456A1/en
Priority to EP19849029.4A priority patent/EP3902784A1/fr
Priority to PCT/FR2019/053259 priority patent/WO2020136337A1/fr
Publication of FR3091280A1 publication Critical patent/FR3091280A1/fr
Application granted granted Critical
Publication of FR3091280B1 publication Critical patent/FR3091280B1/fr
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00—Preparation of peroxy compounds
    • C07C407/003—Separation; Purification; Stabilisation; Use of additives
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40—Extractive distillation

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

PURIFICATION D’HYDROPEROXYDE D’ALKYLE PAR DISTILLATION EXTRACTIVE L’invention concerne un procédé de purification d’un hydroperoxyde d’alkyle de son peroxyde de dialkyle, comprenant une étape de distillation en présence d’alcool et d’eau suivie d’une extraction des condensats par un hydrocarbure ou un mélange d’hydrocarbures.
FR1874177A 2018-12-26 2018-12-26 Purification d’hydroperoxyde d’alkyle par distillation extractive Active FR3091280B1 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
FR1874177A FR3091280B1 (fr) 2018-12-26 2018-12-26 Purification d’hydroperoxyde d’alkyle par distillation extractive
CN201980042744.0A CN112351968A (zh) 2018-12-26 2019-12-20 通过萃取蒸馏将烷基氢过氧化物纯化
US17/417,409 US20220073456A1 (en) 2018-12-26 2019-12-20 Purification of alkyl hydroperoxide by extractive distillation
EP19849029.4A EP3902784A1 (fr) 2018-12-26 2019-12-20 Purification d'hydroperoxyde d'alkyle par distillation extractive
PCT/FR2019/053259 WO2020136337A1 (fr) 2018-12-26 2019-12-20 Purification d'hydroperoxyde d'alkyle par distillation extractive

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1874177A FR3091280B1 (fr) 2018-12-26 2018-12-26 Purification d’hydroperoxyde d’alkyle par distillation extractive

Publications (2)

Publication Number Publication Date
FR3091280A1 FR3091280A1 (fr) 2020-07-03
FR3091280B1 true FR3091280B1 (fr) 2021-06-25

Family

ID=66776500

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1874177A Active FR3091280B1 (fr) 2018-12-26 2018-12-26 Purification d’hydroperoxyde d’alkyle par distillation extractive

Country Status (5)

Country Link
US (1) US20220073456A1 (fr)
EP (1) EP3902784A1 (fr)
CN (1) CN112351968A (fr)
FR (1) FR3091280B1 (fr)
WO (1) WO2020136337A1 (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112300046A (zh) * 2020-11-27 2021-02-02 信汇科技有限公司 一种叔丁基过氧化氢的纯化方法以及叔丁醇的循环利用方法
CN115850143A (zh) * 2022-12-26 2023-03-28 兰州助剂厂有限责任公司 一种从叔丁基过氧化氢的中脱除轻组分的方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2383919A (en) * 1944-05-23 1945-08-28 Shell Dev Recovery of organic peroxides
DE2916572A1 (de) * 1979-04-24 1980-11-13 Peroxid Chemie Gmbh Verfahren zur destillativen trennung von tert.-alkylhydroperoxiden und di- tert.-alkylperoxiden
DE4232500A1 (de) * 1992-09-28 1994-03-31 Peroxid Chemie Gmbh Verfahren zum Herstellen von wasserarmen oder wasserfreien Lösungen von Alkylhydroperoxiden
DE102006032166B4 (de) * 2006-07-12 2018-08-02 Evonik Degussa Gmbh Verfahren zur Herstellung von Acylperoxiden
CN107501152B (zh) * 2017-08-16 2019-09-20 中山大学惠州研究院 一种叔丁基过氧化氢的分离方法

Also Published As

Publication number Publication date
EP3902784A1 (fr) 2021-11-03
WO2020136337A1 (fr) 2020-07-02
CN112351968A (zh) 2021-02-09
US20220073456A1 (en) 2022-03-10
FR3091280A1 (fr) 2020-07-03

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