FR3081457B1 - Procede de preparation du sel de lithium du bis(fluorosulfonyl)imide - Google Patents

Procede de preparation du sel de lithium du bis(fluorosulfonyl)imide Download PDF

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Publication number
FR3081457B1
FR3081457B1 FR1854313A FR1854313A FR3081457B1 FR 3081457 B1 FR3081457 B1 FR 3081457B1 FR 1854313 A FR1854313 A FR 1854313A FR 1854313 A FR1854313 A FR 1854313A FR 3081457 B1 FR3081457 B1 FR 3081457B1
Authority
FR
France
Prior art keywords
preparation
fluorosulfonyl
lithium bis
imide salt
so2nhso2cl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1854313A
Other languages
English (en)
Other versions
FR3081457A1 (fr
Inventor
Philippe Leduc
Dominique Deur-Bert
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Arkema France SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR1854313A priority Critical patent/FR3081457B1/fr
Application filed by Arkema France SA filed Critical Arkema France SA
Priority to JP2020564516A priority patent/JP2021524429A/ja
Priority to KR1020207033443A priority patent/KR20210010470A/ko
Priority to EP19733854.4A priority patent/EP3797086A1/fr
Priority to CN201980034516.9A priority patent/CN112154121A/zh
Priority to PCT/FR2019/051148 priority patent/WO2019224470A1/fr
Priority to US17/056,781 priority patent/US11261087B2/en
Publication of FR3081457A1 publication Critical patent/FR3081457A1/fr
Application granted granted Critical
Publication of FR3081457B1 publication Critical patent/FR3081457B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D47/00—Separating dispersed particles from gases, air or vapours by liquid as separating agent
    • B01D47/02—Separating dispersed particles from gases, air or vapours by liquid as separating agent by passing the gas or air or vapour over or through a liquid bath
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/086—Compounds containing nitrogen and non-metals and optionally metals containing one or more sulfur atoms
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/087—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms
    • C01B21/093—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms containing also one or more sulfur atoms
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0564—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
    • H01M10/0566—Liquid materials
    • H01M10/0568—Liquid materials characterised by the solutes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2251/00—Reactants
    • B01D2251/10—Oxidants
    • B01D2251/106—Peroxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2251/00—Reactants
    • B01D2251/10—Oxidants
    • B01D2251/108—Halogens or halogen compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2251/00—Reactants
    • B01D2251/50—Inorganic acids
    • B01D2251/502—Hydrochloric acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2251/00—Reactants
    • B01D2251/50—Inorganic acids
    • B01D2251/506—Sulfuric acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/20—Halogens or halogen compounds
    • B01D2257/202—Single element halogens
    • B01D2257/2027—Fluorine
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/80—Water
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/48—Sulfur compounds
    • B01D53/50—Sulfur oxides
    • B01D53/507—Sulfur oxides by treating the gases with other liquids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/68—Halogens or halogen compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Electrochemistry (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Gas Separation By Absorption (AREA)
  • Treating Waste Gases (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

La présente invention concerne une procédé de préparation de Cl-SO2NHSO2Cl comprenant une étape de chloration de l'acide sulfamique avec au moins un agent chlorant et au moins un agent soufré, ledit procédé conduisant à un flux F1, de préférence liquide, comprenant Cl-SO2NHSO2Cl et un flux gazeux F2 comprenant HCI et SO2, ledit procédé comprenant une étape a) de traitement du flux gazeux F2. L'invention concerne également un procédé de préparation de LiFSI comprenant le procédé de préparation de Cl-SO2NHSO2Cl susmentionné.
FR1854313A 2018-05-23 2018-05-23 Procede de preparation du sel de lithium du bis(fluorosulfonyl)imide Active FR3081457B1 (fr)

Priority Applications (7)

Application Number Priority Date Filing Date Title
FR1854313A FR3081457B1 (fr) 2018-05-23 2018-05-23 Procede de preparation du sel de lithium du bis(fluorosulfonyl)imide
KR1020207033443A KR20210010470A (ko) 2018-05-23 2019-05-21 리튬 비스(플루오로설포닐)이미드 염의 제조 방법
EP19733854.4A EP3797086A1 (fr) 2018-05-23 2019-05-21 Procede de préparation du sel de lithium du bis(fluorosulfonyl)imide
CN201980034516.9A CN112154121A (zh) 2018-05-23 2019-05-21 制备双(氟磺酰基)酰亚胺的锂盐的方法
JP2020564516A JP2021524429A (ja) 2018-05-23 2019-05-21 リチウム ビス（フルオロスルホニル）イミド塩を調製するための方法
PCT/FR2019/051148 WO2019224470A1 (fr) 2018-05-23 2019-05-21 Procede de préparation du sel de lithium du bis(fluorosulfonyl)imide
US17/056,781 US11261087B2 (en) 2018-05-23 2019-05-21 Method for preparing lithium bis(fluorosulphonyl)imide salt

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1854313 2018-05-23
FR1854313A FR3081457B1 (fr) 2018-05-23 2018-05-23 Procede de preparation du sel de lithium du bis(fluorosulfonyl)imide

Publications (2)

Publication Number Publication Date
FR3081457A1 FR3081457A1 (fr) 2019-11-29
FR3081457B1 true FR3081457B1 (fr) 2020-05-08

Family

ID=63036136

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1854313A Active FR3081457B1 (fr) 2018-05-23 2018-05-23 Procede de preparation du sel de lithium du bis(fluorosulfonyl)imide

Country Status (7)

Country Link
US (1) US11261087B2 (fr)
EP (1) EP3797086A1 (fr)
JP (1) JP2021524429A (fr)
KR (1) KR20210010470A (fr)
CN (1) CN112154121A (fr)
FR (1) FR3081457B1 (fr)
WO (1) WO2019224470A1 (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113336248B (zh) * 2021-06-09 2023-04-07 深圳市研一新材料有限责任公司 一种氟磺酸锂的制法及氟磺酸锂和应用
CN113800486B (zh) * 2021-09-14 2023-06-23 山东凯盛新材料股份有限公司 双氯磺酰亚胺的生产工艺

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS48101378A (fr) * 1972-04-05 1973-12-20
US3956385A (en) * 1973-04-18 1976-05-11 Sumitomo Chemical Company, Limited Process for producing sulfonylamides
JPS627419A (ja) * 1985-01-30 1987-01-14 Kuraray Co Ltd 酸化イオウ系ガスの分離法
JP3976444B2 (ja) * 1998-06-23 2007-09-19 株式会社タクマ 排ガス処理方法および処理装置
FR2975694B1 (fr) 2011-05-24 2013-08-02 Arkema France Procede de preparation de bis(fluorosulfonyl)imidure de lithium
CN102764572A (zh) * 2012-05-15 2012-11-07 山西三维丰海化工有限公司 一种氯化法生产三氯乙酰氯尾气吸收新方法
KR101738789B1 (ko) 2012-08-06 2017-05-22 닛뽕소다 가부시키가이샤 비스(할로술포닐)아민의 제조 방법
US8377406B1 (en) * 2012-08-29 2013-02-19 Boulder Ionics Corporation Synthesis of bis(fluorosulfonyl)imide
FR2998297B1 (fr) 2012-11-22 2014-11-14 Arkema France Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle
FR3020060B1 (fr) 2014-04-18 2016-04-01 Arkema France Preparation d'imides contenant un groupement fluorosulfonyle
CN104447329A (zh) * 2014-10-29 2015-03-25 山东汇海医药化工有限公司 一种2-氯乙酰乙酸乙酯的制备方法
CN106006586B (zh) * 2016-05-27 2018-10-19 上海康鹏科技有限公司 一种双氟磺酰亚胺钾的制备方法
FR3081866B1 (fr) * 2018-06-01 2020-05-08 Arkema France Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle

Also Published As

Publication number Publication date
US11261087B2 (en) 2022-03-01
KR20210010470A (ko) 2021-01-27
US20210122634A1 (en) 2021-04-29
EP3797086A1 (fr) 2021-03-31
JP2021524429A (ja) 2021-09-13
FR3081457A1 (fr) 2019-11-29
WO2019224470A1 (fr) 2019-11-28
CN112154121A (zh) 2020-12-29

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