FR3080852B1 - Procede et dispositif de separation d'aromatiques inverse - Google Patents

Procede et dispositif de separation d'aromatiques inverse Download PDF

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Publication number
FR3080852B1
FR3080852B1 FR1853885A FR1853885A FR3080852B1 FR 3080852 B1 FR3080852 B1 FR 3080852B1 FR 1853885 A FR1853885 A FR 1853885A FR 1853885 A FR1853885 A FR 1853885A FR 3080852 B1 FR3080852 B1 FR 3080852B1
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FR
France
Prior art keywords
column
toluene
cut
benzene
reverse
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR1853885A
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English (en)
French (fr)
Other versions
FR3080852A1 (fr
Inventor
Jerome Pigourier
Isabelle Prevost
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Axens SA
Original Assignee
Axens SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Axens SA filed Critical Axens SA
Priority to FR1853885A priority Critical patent/FR3080852B1/fr
Priority to ES19169111T priority patent/ES2867960T3/es
Priority to PT191691112T priority patent/PT3563916T/pt
Priority to EP19169111.2A priority patent/EP3563916B1/fr
Priority to JP2019084808A priority patent/JP7369542B2/ja
Priority to TW108114853A priority patent/TWI808166B/zh
Priority to CN201910360792.6A priority patent/CN110437026B/zh
Priority to US16/402,300 priority patent/US10669493B2/en
Priority to KR1020190052337A priority patent/KR102802711B1/ko
Publication of FR3080852A1 publication Critical patent/FR3080852A1/fr
Application granted granted Critical
Publication of FR3080852B1 publication Critical patent/FR3080852B1/fr
Priority to HRP20210834TT priority patent/HRP20210834T1/hr
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G61/00—Treatment of naphtha by at least one reforming process and at least one process of refining in the absence of hydrogen
    • C10G61/08—Treatment of naphtha by at least one reforming process and at least one process of refining in the absence of hydrogen plural parallel stages only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G55/00—Treatment of hydrocarbon oils, in the absence of hydrogen, by at least one refining process and at least one cracking process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/007—Energy recuperation; Heat pumps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/10—Vacuum distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
    • B01D3/322—Reboiler specifications
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C07C5/22—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by isomerisation
    • C07C5/27—Rearrangement of carbon atoms in the hydrocarbon skeleton
    • C07C5/2729—Changing the branching point of an open chain or the point of substitution on a ring
    • C07C5/2732—Catalytic processes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C6/00—Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions
    • C07C6/08—Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions by conversion at a saturated carbon-to-carbon bond
    • C07C6/12—Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions by conversion at a saturated carbon-to-carbon bond of exclusively hydrocarbons containing a six-membered aromatic ring
    • C07C6/123—Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions by conversion at a saturated carbon-to-carbon bond of exclusively hydrocarbons containing a six-membered aromatic ring of only one hydrocarbon
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/005—Processes comprising at least two steps in series
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/04—Purification; Separation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • C07C7/13—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers by molecular-sieve technique
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G29/00—Refining of hydrocarbon oils, in the absence of hydrogen, with other chemicals
    • C10G29/20—Organic compounds not containing metal atoms
    • C10G29/205—Organic compounds not containing metal atoms by reaction with hydrocarbons added to the hydrocarbon oil
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G55/00—Treatment of hydrocarbon oils, in the absence of hydrogen, by at least one refining process and at least one cracking process
    • C10G55/08—Treatment of hydrocarbon oils, in the absence of hydrogen, by at least one refining process and at least one cracking process plural parallel stages only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G7/00—Distillation of hydrocarbon oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1096—Aromatics or polyaromatics
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/201—Impurities
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/4006—Temperature
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/4012—Pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
    • C10G2400/30—Aromatics

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Water Supply & Treatment (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Working-Up Tar And Pitch (AREA)
FR1853885A 2018-05-04 2018-05-04 Procede et dispositif de separation d'aromatiques inverse Expired - Fee Related FR3080852B1 (fr)

Priority Applications (10)

Application Number Priority Date Filing Date Title
FR1853885A FR3080852B1 (fr) 2018-05-04 2018-05-04 Procede et dispositif de separation d'aromatiques inverse
ES19169111T ES2867960T3 (es) 2018-05-04 2019-04-12 Procedimiento y dispositivo de separación inversa de aromáticos
PT191691112T PT3563916T (pt) 2018-05-04 2019-04-12 Processo e dispositivo de separação inversa de aromáticos
EP19169111.2A EP3563916B1 (fr) 2018-05-04 2019-04-12 Procede et dispositif de separation d'aromatiques inverse
JP2019084808A JP7369542B2 (ja) 2018-05-04 2019-04-26 芳香族化合物の逆転式分離のための方法およびデバイス
TW108114853A TWI808166B (zh) 2018-05-04 2019-04-29 用於逆向分離芳香族化合物之方法及裝置
CN201910360792.6A CN110437026B (zh) 2018-05-04 2019-04-30 用于反向分离芳族化合物的方法和装置
US16/402,300 US10669493B2 (en) 2018-05-04 2019-05-03 Process and device for the inverted separation of aromatics
KR1020190052337A KR102802711B1 (ko) 2018-05-04 2019-05-03 방향족들의 역 분리를 위한 프로세스 및 기기
HRP20210834TT HRP20210834T1 (hr) 2018-05-04 2021-05-25 Postupak i uređaj za inverzno razdvajanje aromata

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1853885 2018-05-04
FR1853885A FR3080852B1 (fr) 2018-05-04 2018-05-04 Procede et dispositif de separation d'aromatiques inverse

Publications (2)

Publication Number Publication Date
FR3080852A1 FR3080852A1 (fr) 2019-11-08
FR3080852B1 true FR3080852B1 (fr) 2020-05-08

Family

ID=63963087

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1853885A Expired - Fee Related FR3080852B1 (fr) 2018-05-04 2018-05-04 Procede et dispositif de separation d'aromatiques inverse

Country Status (10)

Country Link
US (1) US10669493B2 (https=)
EP (1) EP3563916B1 (https=)
JP (1) JP7369542B2 (https=)
KR (1) KR102802711B1 (https=)
CN (1) CN110437026B (https=)
ES (1) ES2867960T3 (https=)
FR (1) FR3080852B1 (https=)
HR (1) HRP20210834T1 (https=)
PT (1) PT3563916T (https=)
TW (1) TWI808166B (https=)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102814192B1 (ko) * 2020-06-16 2025-05-30 주식회사 엘지화학 방향족 탄화수소의 제조방법
KR102464478B1 (ko) * 2020-06-16 2022-11-07 주식회사 엘지화학 방향족 탄화수소 제조장치
KR102819375B1 (ko) * 2020-06-16 2025-06-11 주식회사 엘지화학 방향족 탄화수소의 제조방법
FR3126976A1 (fr) * 2021-09-10 2023-03-17 IFP Energies Nouvelles Oxycombustion de composés hydrocarbonés riches en oxygène pour la production de xylènes.
FR3126977A1 (fr) * 2021-09-10 2023-03-17 IFP Energies Nouvelles Combustion en boucle chimique de composés hydrocarbonés riches en oxygène pour la production de xylènes.

Family Cites Families (20)

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Publication number Priority date Publication date Assignee Title
JPS61186334A (ja) * 1985-02-14 1986-08-20 Mitsubishi Chem Ind Ltd Ｃ８芳香族炭化水素異性体の分離方法
JPS63196528A (ja) * 1985-09-13 1988-08-15 ユ−オ−ピ−　インコ−ポレイテツド 異性化／トランスアルキル化兼用帯域を用いたキシレンの製造法
DE3942950A1 (de) * 1989-12-23 1991-06-27 Krupp Koppers Gmbh Verfahren zur gleichzeitigen gewinnung von reinem benzol und reinem tuluol
US6740788B1 (en) * 2002-12-19 2004-05-25 Uop Llc Integrated process for aromatics production
JP2007269647A (ja) * 2006-03-30 2007-10-18 Mitsubishi Chemicals Corp α−メチルスチレンの精製方法
RU2527961C1 (ru) * 2010-08-25 2014-09-10 Юоп Ллк Сохранение энергии при дистилляции тяжелых углеводородов
US8993825B2 (en) * 2010-08-25 2015-03-31 Uop Llc Energy conservation in heavy-hydrocarbon distillation
US8754281B2 (en) * 2010-08-25 2014-06-17 Uop Llc Energy conservation in heavy-hydrocarbon distillation
JP6033050B2 (ja) * 2012-11-16 2016-11-30 東洋エンジニアリング株式会社 芳香族炭化水素製造装置
FR2998301B1 (fr) * 2012-11-22 2016-01-01 Axens Methode de recuperation de chaleur a basse temperature et application de la methode au complexe aromatique
RU2687104C2 (ru) * 2014-02-13 2019-05-07 Бипи Корпорейшен Норт Америка Инк. Энергосберегающий способ фракционирования для разделения выходящего потока реактора процессов переалкилирования tol/с9+
US9328040B2 (en) * 2014-03-03 2016-05-03 Uop Llc Process for recovering benzene and fuel gas in an aromatics complex
US9302953B2 (en) * 2014-06-30 2016-04-05 Exxonmobil Chemicals Patents Inc. Process for the production of xylenes
KR101917490B1 (ko) * 2014-06-30 2018-11-09 엑손모빌 케미칼 패턴츠 인코포레이티드 파라-크실렌의 제조 방법
US9221729B1 (en) * 2015-02-23 2015-12-29 Allnew Chemical Technology Company Extractive distillation for aromatics recovery
US20160347689A1 (en) * 2015-05-29 2016-12-01 Uop Llc Processes and apparatuses for separating streams to provide a transalkylation feed stream in an aromatics complex
EP3455195B1 (en) * 2016-03-31 2022-06-08 Uop Llc Processes and apparatuses for naphthene recycle in the production of aromatic products
US10865169B2 (en) * 2016-06-07 2020-12-15 Uop Llc Liquid phase isomerization process integration
US10023509B2 (en) * 2016-09-30 2018-07-17 Uop Llc Processes and apparatuses for production of aromatic products
FR3080857B1 (fr) * 2018-05-04 2020-05-08 Axens Procede et dispositif de separation d'aromatiques sous vide

Also Published As

Publication number Publication date
JP7369542B2 (ja) 2023-10-26
PT3563916T (pt) 2021-04-14
TWI808166B (zh) 2023-07-11
KR20190127597A (ko) 2019-11-13
FR3080852A1 (fr) 2019-11-08
CN110437026A (zh) 2019-11-12
EP3563916B1 (fr) 2021-03-17
EP3563916A1 (fr) 2019-11-06
US20190338202A1 (en) 2019-11-07
KR102802711B1 (ko) 2025-04-30
US10669493B2 (en) 2020-06-02
HRP20210834T1 (hr) 2021-08-06
JP2019194187A (ja) 2019-11-07
CN110437026B (zh) 2023-07-21
ES2867960T3 (es) 2021-10-21
TW202003426A (zh) 2020-01-16

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