FR2708742A1 - Procédé et dispositiphi pour mesurer des paramètres physiques d'échantillons poreux mouillables par des fluides. - Google Patents

Procédé et dispositiphi pour mesurer des paramètres physiques d'échantillons poreux mouillables par des fluides.

Info

Publication number
FR2708742A1
FR2708742A1 FR9309481A FR9309481A FR2708742A1 FR 2708742 A1 FR2708742 A1 FR 2708742A1 FR 9309481 A FR9309481 A FR 9309481A FR 9309481 A FR9309481 A FR 9309481A FR 2708742 A1 FR2708742 A1 FR 2708742A1
Authority
FR
France
Prior art keywords
fluid
sample
pressure
wettable
fluids
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR9309481A
Other languages
English (en)
Other versions
FR2708742B1 (fr
Inventor
Lenormand Roland
Eisenzimmer Annick
Ringot Gabriel
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IFP Energies Nouvelles IFPEN
Original Assignee
IFP Energies Nouvelles IFPEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to FR9309481A priority Critical patent/FR2708742B1/fr
Priority to GB9414998A priority patent/GB2280512B/en
Priority to NO19942796A priority patent/NO315822B1/no
Priority to CA002129166A priority patent/CA2129166C/fr
Publication of FR2708742A1 publication Critical patent/FR2708742A1/fr
Application granted granted Critical
Publication of FR2708742B1 publication Critical patent/FR2708742B1/fr
Priority to US08/668,371 priority patent/US5679885A/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume, or surface-area of porous materials
    • G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082—Investigating permeability by forcing a fluid through a sample
    • G01N15/0826—Investigating permeability by forcing a fluid through a sample and measuring fluid flow rate, i.e. permeation rate or pressure change
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N29/00—Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
    • G01N29/04—Analysing solids
    • G01N29/07—Analysing solids by measuring propagation velocity or propagation time of acoustic waves
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00—Indexing codes associated with group G01N29/00
    • G01N2291/02—Indexing codes associated with the analysed material
    • G01N2291/024—Mixtures
    • G01N2291/02441—Liquids in porous solids
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00—Indexing codes associated with group G01N29/00
    • G01N2291/02—Indexing codes associated with the analysed material
    • G01N2291/028—Material parameters
    • G01N2291/02872—Pressure

Abstract

- Le procédé consiste essentiellement à placer un échantillon solide (S) imbibé avec un premier fluide (de l'eau par exemple) dans une enceinte close (1), d'injecter par des moyens de pression (11-13) un autre fluide sous pression à une première extrémité de l'enceinte et de balayer l'extrémité opposée par un fluide à basse pression mis en circulation par des moyens de pompage (14-15), qui entraîne au dehors le fluide draîné. Le dispositif comporte des moyens de mesure (11, 21, 22, 28) permettant de connaître la pression et la saturation de l'échantillon en au moins un point de sa longueur, la quantité de fluide évacué et la résistivité électrique de l'échantillon. Par une variation progressive des débits injectés, on peut réaliser sans toucher à l'échantillon, des cycles complets de draînages et d'imbibitions avec établissement de courbes de variation de la pression capillaire, et calcul des perméabilités relatives. - Application notamment à la pétrophysique des roches ou au test de matériaux de construction dans le bâtiment.
FR9309481A 1993-07-29 1993-07-29 Procédé et dispositiphi pour mesurer des paramètres physiques d'échantillons poreux mouillables par des fluides. Expired - Fee Related FR2708742B1 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
FR9309481A FR2708742B1 (fr) 1993-07-29 1993-07-29 Procédé et dispositiphi pour mesurer des paramètres physiques d'échantillons poreux mouillables par des fluides.
GB9414998A GB2280512B (en) 1993-07-29 1994-07-26 A method and a device for measuring physical parameters of porous samples
NO19942796A NO315822B1 (no) 1993-07-29 1994-07-27 Fremgangsmåte og anordning for måling av fysiske parametrer av poröse flytende våtpröver
CA002129166A CA2129166C (fr) 1993-07-29 1994-07-29 Procede et dispositif pour mesurer des parametres physiques d'echantillons poreux mouillables par des fluides
US08/668,371 US5679885A (en) 1993-07-29 1996-06-18 Process and device for measuring physical parameters of porous fluid wet samples

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9309481A FR2708742B1 (fr) 1993-07-29 1993-07-29 Procédé et dispositiphi pour mesurer des paramètres physiques d'échantillons poreux mouillables par des fluides.

Publications (2)

Publication Number Publication Date
FR2708742A1 true FR2708742A1 (fr) 1995-02-10
FR2708742B1 FR2708742B1 (fr) 1995-09-01

Family

ID=9449851

Family Applications (1)

Application Number Title Priority Date Filing Date
FR9309481A Expired - Fee Related FR2708742B1 (fr) 1993-07-29 1993-07-29 Procédé et dispositiphi pour mesurer des paramètres physiques d'échantillons poreux mouillables par des fluides.

Country Status (5)

Country Link
US (1) US5679885A (fr)
CA (1) CA2129166C (fr)
FR (1) FR2708742B1 (fr)
GB (1) GB2280512B (fr)
NO (1) NO315822B1 (fr)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0729022A1 (fr) * 1995-02-27 1996-08-28 Institut Français du Pétrole Méthode et dispositif pour déterminer différents paramètres physiques d'échantillons de matériaux poreux, en présence de fluides di- ou triphasiques
EP0731350A1 (fr) * 1995-02-24 1996-09-11 FINMECCANICA S.p.A. AZIENDA ANSALDO Appareil de détection optique de défauts de surfaces, en particulier dans des bandes laminées
FR2792678A1 (fr) 1999-04-23 2000-10-27 Inst Francais Du Petrole Procede de recuperation assistee d'hydrocarbures par injection combinee d'une phase aqueuse et de gaz au moins partiellement miscible a l'eau
WO2004025317A1 (fr) 2002-09-11 2004-03-25 Institut Francais Du Petrole Methode de mesure de la mouillabilite de roches par resonance magnetique nucleaire
FR3099577A1 (fr) 2019-07-30 2021-02-05 Cydarex Dispositif pour mesurer des caractéristiques physiques d'un échantillon solide poreux

Families Citing this family (49)

* Cited by examiner, † Cited by third party
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FR2728344B1 (fr) * 1994-12-19 1997-01-24 Inst Francais Du Petrole Methode et dispositif pour separer et mesurer le volume des differentes phases d'un melange de fluides
AU4460596A (en) * 1995-01-12 1996-07-31 Vladimir Nikolaevich Belonenko Devices for measuring viscosity and for investigating fluid flow through capillary-porous mediums
FR2734056B1 (fr) * 1995-05-12 1997-06-20 Inst Francais Du Petrole Cellule de mesure a prise de pression multiple
US5731511A (en) * 1995-05-12 1998-03-24 Institut Francais Du Petrole Measuring cell with multiple pressure taps
FR2762681B1 (fr) * 1997-04-29 1999-10-08 Inst Francais Du Petrole Dispositif pour faire des mesures sur un echantillon poreux en presence de fluides, utilisant des membranes semi-permeables resistant a la temperature
FR2781573B1 (fr) * 1998-07-24 2000-08-25 Inst Francais Du Petrole Methode de mesure rapide de l'indice de resistivite d'echantillons solides tels que des roches
US6422063B1 (en) * 1998-08-11 2002-07-23 Ramaswamy C. Anantheswaran Rapid method to experimentally measure the gas permeability of micro-perforated films
FR2785680B1 (fr) * 1998-11-09 2000-12-08 Inst Francais Du Petrole Dispositif pour tester des echantillons de roches a pression et temperature relativement elevees
FR2798734B1 (fr) 1999-09-21 2001-10-12 Inst Francais Du Petrole Methode optimisee pour determiner des parametres physiques d'un echantillon soumis a centrifugation
IT1313693B1 (it) * 1999-11-26 2002-09-09 Eni Spa Procedimento per determinare in continuo l'interazione tra fluidi diperforazione e formazione argillose.
IT1313691B1 (it) 1999-11-26 2002-09-09 Eni Spa Procedimento per verificare l'efficacia dei fluidi di perforazionenello stabilizzare le pareti di pozzi petroliferi.
AU1939400A (en) * 1999-12-14 2001-12-03 Cristina Crawford Multi-directional permeameter
FR2810736B1 (fr) * 2000-06-23 2002-09-20 Inst Francais Du Petrole Methode pour evaluer des parametres physiques d'un gisement souterrain a partir de debris de roche qui y sont preleves
CA2342119A1 (fr) 2001-03-23 2002-09-23 Universite Du Quebec A Montreal (Uqam) Automatisation du test d'absorption d'eau dans les materiaux poreux
GB2374425A (en) * 2001-04-12 2002-10-16 Nigel Alexander Feetham Porosity measuring device for building materials
FR2836228B1 (fr) * 2002-02-21 2005-08-19 Inst Francais Du Petrole Methode et dispositif pour evaluer des parametres physiques d'un gisement souterrain a partir de debris de roche qui y sont preleves
DE10315391A1 (de) * 2003-04-04 2004-11-04 Federal-Mogul Sealing Systems Gmbh Verfahren und Vorrichtung zur Bestimmung stofflicher Emissionen von Prüflingen
FR2854462B1 (fr) * 2003-04-29 2005-06-24 Inst Francais Du Petrole Methode d'evaluation du facteur de formation d'un gisement souterrain a partir de mesures sur des debris de forage qui y sont preleves
US20040255646A1 (en) * 2003-06-17 2004-12-23 Valeriu Smiricinschi Method for control gas diffusion and bubble formation in liquid porosimetry
FR2874696B1 (fr) * 2004-09-02 2007-03-23 Inst Francais Du Petrole Methode de determination de parametres d'ecoulement multiphasique d'un milieu poreux avec prise en compte de l'heterogeneite locale
DE102005010847B4 (de) * 2005-03-07 2007-08-02 Rea Elektronik Gmbh Vorrichtung zur Messung einer austretenden Flüssigkeit
FR2884923B1 (fr) 2005-04-26 2007-10-19 Inst Francais Du Petrole Methode et dispositif pour evaluer des parametres d'ecoulement et des parametres electriques d'un milieu poreux.
KR100642304B1 (ko) 2005-10-31 2006-11-02 한국지질자원연구원 하중압의 변화에 따른 미고결 시료의 물성측정장치
US7472588B2 (en) * 2007-04-18 2009-01-06 Sorowell Production Services Llc Petrophysical fluid flow property determination
US7567079B2 (en) * 2007-06-08 2009-07-28 University Of New Brunswick Methods suitable for measuring capillary pressure and relative permeability curves of porous rocks
GB0721506D0 (en) * 2007-11-02 2007-12-12 Corpro Systems Ltd Method and apparatus
US9291050B2 (en) * 2008-09-30 2016-03-22 Schlumberger Technology Corporation Determining formation wettability from dielectric measurements
US8201439B2 (en) * 2009-11-02 2012-06-19 Schlumberger Technology Corporation Material wettability characterization and chemical additive evaluation
US8507868B2 (en) * 2011-03-04 2013-08-13 Landmark Graphics Corporation Systems and methods for determining fluid mobility in rock samples
GB2492795B (en) * 2011-07-12 2013-11-20 Schlumberger Holdings Testing imbibition of liquid
CN102636574A (zh) * 2012-04-10 2012-08-15 华侨大学 一种工程用承压渗透式声测探头
DE102012012589A1 (de) 2012-06-19 2013-12-19 Technische Universität Bergakademie Freiberg Kernhalter mit Manteldruckbeaufschlagung
KR101481383B1 (ko) * 2014-02-05 2015-01-14 전남대학교산학협력단 유체주입을 통한 원유생산증진 시스템 및 방법
US9835762B2 (en) 2014-02-06 2017-12-05 Schlumberger Technology Corporation Petrophysical rock characterization
US9417168B2 (en) * 2014-03-10 2016-08-16 Dmar Engineering, Inc. Fatigue testing
US10197490B2 (en) * 2015-06-02 2019-02-05 Dci Corporation Apparatus, method, and system for measuring relative permeability of immiscible fluids
CN104931405B (zh) * 2015-06-16 2017-12-22 南京华研智能科技有限公司 密封渗透装置及采用密封装置的全自动混凝土抗渗仪
US9341558B1 (en) * 2015-08-25 2016-05-17 King Saud University System and method for measuring permeation properties of concrete and porous materials
CN108181224A (zh) * 2018-01-05 2018-06-19 中国石油大学(华东) 油藏条件下驱替及吸吮毛管力曲线联测装置及方法
EP3743718A1 (fr) * 2018-01-23 2020-12-02 Total Se Procédé et appareil d'analyse d'un échantillon de roche
CN109030315B (zh) * 2018-08-22 2020-11-27 福州大学 低应力起始一维压缩-渗透试验系统及其工作方法
CN109883917B (zh) * 2019-01-24 2021-06-04 西南石油大学 一种模拟基质-裂缝静动态渗吸排油的实验装置及方法
CN110068527B (zh) * 2019-04-26 2020-07-10 中国矿业大学 一种非平衡状态下煤岩渗透率自动连续测试装置及其方法
US11249001B2 (en) 2019-05-23 2022-02-15 Saudi Arabian Oil Company Determination of scanning loops of capillary pressure and relative permeability curves and wettability distribution of rock samples
CN110261285B (zh) * 2019-08-01 2022-04-29 西南石油大学 一种基于超声衰减的自发渗吸测量装置及方法
EP4038363A4 (fr) * 2019-10-04 2023-10-04 Total Se Système de mesure de pression distribuée destiné à des expériences de balayage sur carotte
CN112096357B (zh) * 2020-09-16 2021-10-15 中国石油大学(北京) 稠油热采相对渗透率测试的产油量校正方法、装置及设备
US11454097B2 (en) 2021-01-04 2022-09-27 Saudi Arabian Oil Company Artificial rain to enhance hydrocarbon recovery
US11828693B2 (en) * 2022-02-11 2023-11-28 Saudi Arabian Oil Company Centrifuge method for evaluating contact angle and wettability alteration

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US4868751A (en) * 1987-09-11 1989-09-19 Mobil Oil Corporation Method for determining relative permeability of a subterranean reservoir
US4926128A (en) * 1989-02-13 1990-05-15 Mobil Oil Corporation Method for utilizing measured resistivities of porous rock under differing fluid saturations to identify fluid distribution equilibrium
US5069065A (en) * 1991-01-16 1991-12-03 Mobil Oil Corporation Method for measuring wettability of porous rock
US5079948A (en) * 1991-01-28 1992-01-14 Mobil Oil Corporation Method for conducting capillary pressure drainage and imbibition on a core sample of a porous rock
FR2666147A1 (fr) * 1990-08-27 1992-02-28 Inst Francais Du Petrole Mesure de la repartition des concentrations de constituants d'un syteme en centrifugation par emission/reception de signaux mecaniques.
US5164672A (en) * 1992-02-19 1992-11-17 Mobil Oil Corporation Method for measuring electrical resistivity of a core sample of porous rock during water drainage and imbibition
US5209104A (en) * 1992-01-23 1993-05-11 Mobil Oil Corporation Method for desaturating a porous rock for electrical resistivity measurements

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US4543821A (en) * 1983-12-14 1985-10-01 Texaco Inc. Method and apparatus for measuring relative permeability and water saturation of a core
US4868751A (en) * 1987-09-11 1989-09-19 Mobil Oil Corporation Method for determining relative permeability of a subterranean reservoir
US4926128A (en) * 1989-02-13 1990-05-15 Mobil Oil Corporation Method for utilizing measured resistivities of porous rock under differing fluid saturations to identify fluid distribution equilibrium
FR2666147A1 (fr) * 1990-08-27 1992-02-28 Inst Francais Du Petrole Mesure de la repartition des concentrations de constituants d'un syteme en centrifugation par emission/reception de signaux mecaniques.
EP0473500A1 (fr) * 1990-08-27 1992-03-04 Institut Français du Pétrole Mesure de la répartition de constituants d'un mélange par ultrasons
US5069065A (en) * 1991-01-16 1991-12-03 Mobil Oil Corporation Method for measuring wettability of porous rock
US5079948A (en) * 1991-01-28 1992-01-14 Mobil Oil Corporation Method for conducting capillary pressure drainage and imbibition on a core sample of a porous rock
US5209104A (en) * 1992-01-23 1993-05-11 Mobil Oil Corporation Method for desaturating a porous rock for electrical resistivity measurements
US5164672A (en) * 1992-02-19 1992-11-17 Mobil Oil Corporation Method for measuring electrical resistivity of a core sample of porous rock during water drainage and imbibition

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0731350A1 (fr) * 1995-02-24 1996-09-11 FINMECCANICA S.p.A. AZIENDA ANSALDO Appareil de détection optique de défauts de surfaces, en particulier dans des bandes laminées
EP0729022A1 (fr) * 1995-02-27 1996-08-28 Institut Français du Pétrole Méthode et dispositif pour déterminer différents paramètres physiques d'échantillons de matériaux poreux, en présence de fluides di- ou triphasiques
FR2731073A1 (fr) * 1995-02-27 1996-08-30 Inst Francais Du Petrole Methode et dispositif pour determiner differents parametres physiques d'echantillons de materiaux poreux, en presence de fluides di- ou triphasiques
FR2792678A1 (fr) 1999-04-23 2000-10-27 Inst Francais Du Petrole Procede de recuperation assistee d'hydrocarbures par injection combinee d'une phase aqueuse et de gaz au moins partiellement miscible a l'eau
WO2004025317A1 (fr) 2002-09-11 2004-03-25 Institut Francais Du Petrole Methode de mesure de la mouillabilite de roches par resonance magnetique nucleaire
FR3099577A1 (fr) 2019-07-30 2021-02-05 Cydarex Dispositif pour mesurer des caractéristiques physiques d'un échantillon solide poreux

Also Published As

Publication number Publication date
CA2129166A1 (fr) 1995-01-30
GB9414998D0 (en) 1994-09-14
NO942796D0 (no) 1994-07-27
FR2708742B1 (fr) 1995-09-01
NO315822B1 (no) 2003-10-27
GB2280512A (en) 1995-02-01
CA2129166C (fr) 2007-07-10
US5679885A (en) 1997-10-21
GB2280512B (en) 1996-12-11
NO942796L (no) 1995-01-30

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