FR2380228A1 - Procede de traitement de liqueurs alcalines contenant des ions sulfate - Google Patents

Procede de traitement de liqueurs alcalines contenant des ions sulfate

Info

Publication number
FR2380228A1
FR2380228A1 FR7703640A FR7703640A FR2380228A1 FR 2380228 A1 FR2380228 A1 FR 2380228A1 FR 7703640 A FR7703640 A FR 7703640A FR 7703640 A FR7703640 A FR 7703640A FR 2380228 A1 FR2380228 A1 FR 2380228A1
Authority
FR
France
Prior art keywords
sulphate ions
separation
liquors containing
containing sulphate
treating alkaline
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7703640A
Other languages
English (en)
Other versions
FR2380228B1 (fr
Inventor
Pierre Mouret
Georges Claude Louis Lyaudet
Angelo Ernest Sialino
Rino Ferdinando Celeste Berri
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Orano Cycle SA
Original Assignee
Compagnie Generale des Matieres Nucleaires SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Compagnie Generale des Matieres Nucleaires SA filed Critical Compagnie Generale des Matieres Nucleaires SA
Priority to FR7703640A priority Critical patent/FR2380228A1/fr
Priority to PT6759278A priority patent/PT67592B/fr
Priority to ZA00780694A priority patent/ZA78694B/xx
Priority to DE2804908A priority patent/DE2804908C3/de
Priority to ES466697A priority patent/ES466697A1/es
Priority to CA296,452A priority patent/CA1111156A/fr
Priority to US05/876,158 priority patent/US4321235A/en
Priority to AU33092/78A priority patent/AU524601B2/en
Priority to OA56406A priority patent/OA05885A/fr
Publication of FR2380228A1 publication Critical patent/FR2380228A1/fr
Application granted granted Critical
Publication of FR2380228B1 publication Critical patent/FR2380228B1/fr
Granted legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B60/00Obtaining metals of atomic number 87 or higher, i.e. radioactive metals
    • C22B60/02Obtaining thorium, uranium, or other actinides
    • C22B60/0204Obtaining thorium, uranium, or other actinides obtaining uranium
    • C22B60/0217Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes
    • C22B60/0252Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries
    • C22B60/0278Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries by chemical methods
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/04Processes using organic exchangers
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/42Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/44Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B60/00Obtaining metals of atomic number 87 or higher, i.e. radioactive metals
    • C22B60/02Obtaining thorium, uranium, or other actinides
    • C22B60/0204Obtaining thorium, uranium, or other actinides obtaining uranium
    • C22B60/0217Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes
    • C22B60/0252Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries
    • C22B60/026Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries liquid-liquid extraction with or without dissolution in organic solvents
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Geology (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Removal Of Specific Substances (AREA)

Abstract

Procédé de traitement d'une liqueur alcaline, contenant des sulfates et des ions sodium, telle qu'un effluent obtenu à partir d'une solution d'attaque d'un minerai uranifère sulfuré, à base de carbonate de sodium, en présence d'un oxydant, et après séparation de l'uranium à partir de la solution d'extraction. Ce procédé comprend la mise en contact de cette liqueur avec une résine échangeuse d'ions, cationique, préalablement mise sous forme ammonium, et la précipitation ultérieure du sulfate d'ammonium hors de la solution obtenue, à l'état de sulfate de calcium insoluble. Application à la séparation des effluents liquides polluants.
FR7703640A 1977-02-09 1977-02-09 Procede de traitement de liqueurs alcalines contenant des ions sulfate Granted FR2380228A1 (fr)

Priority Applications (9)

Application Number Priority Date Filing Date Title
FR7703640A FR2380228A1 (fr) 1977-02-09 1977-02-09 Procede de traitement de liqueurs alcalines contenant des ions sulfate
PT6759278A PT67592B (fr) 1977-02-09 1978-01-27 Procede de traitement de liqueurs alcalines contenant des ions sulfate
DE2804908A DE2804908C3 (de) 1977-02-09 1978-02-06 Verfahren zur verbesserten Fällung von Sulfaten unter Rückgewinnung von Natriumcarbonatlösungen aus alkalischen Auslauglösungen
ES466697A ES466697A1 (es) 1977-02-09 1978-02-06 Procedimiento de tratamiento de un licor alcalino
ZA00780694A ZA78694B (en) 1977-02-09 1978-02-06 A process for the treatment of an alkaline solution
CA296,452A CA1111156A (fr) 1977-02-09 1978-02-08 Procede de traitement de liqueurs alcalines contenant des ions sulfates
US05/876,158 US4321235A (en) 1977-02-09 1978-02-08 Process for the treatment of alkaline liquors containing sulfate ions
AU33092/78A AU524601B2 (en) 1977-02-09 1978-02-08 Separating sulfates and recovery by ton exchange of sodium in solutions containing sodium and so4 ions
OA56406A OA05885A (fr) 1977-02-09 1978-02-09 Procédé de traitement de liqueurs alcalines contenant des ions sulfate.

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR7703640A FR2380228A1 (fr) 1977-02-09 1977-02-09 Procede de traitement de liqueurs alcalines contenant des ions sulfate

Publications (2)

Publication Number Publication Date
FR2380228A1 true FR2380228A1 (fr) 1978-09-08
FR2380228B1 FR2380228B1 (fr) 1980-04-30

Family

ID=9186529

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7703640A Granted FR2380228A1 (fr) 1977-02-09 1977-02-09 Procede de traitement de liqueurs alcalines contenant des ions sulfate

Country Status (9)

Country Link
US (1) US4321235A (fr)
AU (1) AU524601B2 (fr)
CA (1) CA1111156A (fr)
DE (1) DE2804908C3 (fr)
ES (1) ES466697A1 (fr)
FR (1) FR2380228A1 (fr)
OA (1) OA05885A (fr)
PT (1) PT67592B (fr)
ZA (1) ZA78694B (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2479792A2 (fr) * 1977-09-30 1981-10-09 Pechiney Aluminium Procede de purification de solutions contenant des carbonate et sulfate alcalins, eventuellement de l'hydroxyde alcalin ainsi que l'un au moins des metaux, vanadium, uranium et molybdene

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4423009A (en) * 1980-04-02 1983-12-27 Aluminium Pechiney Carbonate, sulphate and hydroxide or hydrogen carbonate
DZ283A1 (fr) * 1980-04-02 2004-09-13 Pechiney Aluminium Procédé de purification de solutions contenant descarbonate, sulfate, hydroxyde ou éventuellement hydrogenocarbonate alcalins ainsi que l'un au moins des métaux vanadium, uranium, molybdène.
IL69384A0 (en) * 1983-08-01 1983-11-30 Israel Atomic Energy Comm Recovery of uranium from wet process phosphoric acid by liquid-solid ion exchange
US4756897A (en) * 1986-06-23 1988-07-12 Kerr-Mcgee Corporation Process for preparing concentrated byproduct nitrate solutions
US5944868A (en) * 1998-01-28 1999-08-31 Tessenderlo Kerley, Inc. Production of liquid fertilizers by ion exchange
CN115572848B (zh) * 2022-09-26 2023-12-15 核工业北京化工冶金研究院 一种可实现载铀树脂高效淋洗及淋洗剂再生的工艺方法
CN115874071A (zh) * 2022-12-09 2023-03-31 核工业北京化工冶金研究院 一种含铁硼铀混合精矿高效提纯铀的方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2656245A (en) * 1950-07-15 1953-10-20 Rayonier Inc Preparation of sodium salts of carbonic acid by ion exchange
US2863717A (en) * 1954-04-07 1958-12-09 Kunin Robert Recovery of uranium values from copper-bearing solutions
GB775415A (en) * 1954-10-05 1957-05-22 Commw Scient Ind Res Org Improved method and means for extracting an adsorbable solute from a suspension of finely divided solids in a solution
US2900227A (en) * 1956-01-13 1959-08-18 Int Minerals & Chem Corp Ion exchange process-removal of sulfate ions from eluate
US3000696A (en) * 1956-07-27 1961-09-19 Texaco Development Corp Process for recovery of uranium from fossil fuels
FR1193092A (fr) * 1958-03-06 1959-10-30 Commissariat Energie Atomique Procédé de traitement et de recyclage des liqueurs alcalines provenant des traitements alcalins des minerais d'uranium
FR1373734A (fr) * 1963-07-11 1964-10-02 Comvissariat A L En Atomique Procédé d'élution de l'uranium et son application à l'échange ionique en milieu alcalin
US3378336A (en) * 1966-06-17 1968-04-16 Interior Usa Sulfate removal from brines
US3497314A (en) * 1967-04-24 1970-02-24 Sun Oil Co Recovery of potassium from sea water
US3445201A (en) * 1968-03-27 1969-05-20 Atomic Energy Commission Ion exchange process for recovering americium and curium
US3961027A (en) * 1973-10-18 1976-06-01 Westinghouse Electric Corporation Cyclic process for re-use of waste water generated during the production of UO2

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2479792A2 (fr) * 1977-09-30 1981-10-09 Pechiney Aluminium Procede de purification de solutions contenant des carbonate et sulfate alcalins, eventuellement de l'hydroxyde alcalin ainsi que l'un au moins des metaux, vanadium, uranium et molybdene

Also Published As

Publication number Publication date
OA05885A (fr) 1981-05-31
DE2804908B2 (de) 1980-03-13
ZA78694B (en) 1979-03-28
ES466697A1 (es) 1979-02-01
AU524601B2 (en) 1982-09-23
FR2380228B1 (fr) 1980-04-30
CA1111156A (fr) 1981-10-20
AU3309278A (en) 1979-08-16
PT67592B (fr) 1979-06-22
DE2804908C3 (de) 1980-10-30
PT67592A (fr) 1978-02-01
DE2804908A1 (de) 1978-08-10
US4321235A (en) 1982-03-23

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