FR2366564A1 - Pressure gas chromatograph - working at 2-50 atm at its outlet for use with spectrometers - Google Patents

Pressure gas chromatograph - working at 2-50 atm at its outlet for use with spectrometers

Info

Publication number
FR2366564A1
FR2366564A1 FR7605681A FR7605681A FR2366564A1 FR 2366564 A1 FR2366564 A1 FR 2366564A1 FR 7605681 A FR7605681 A FR 7605681A FR 7605681 A FR7605681 A FR 7605681A FR 2366564 A1 FR2366564 A1 FR 2366564A1
Authority
FR
France
Prior art keywords
column
samples
outlet
working
pressure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
FR7605681A
Other languages
French (fr)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Block Engineering Inc
Original Assignee
Block Engineering Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Block Engineering Inc filed Critical Block Engineering Inc
Priority to FR7605681A priority Critical patent/FR2366564A1/en
Publication of FR2366564A1 publication Critical patent/FR2366564A1/en
Withdrawn legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • G01N30/46—Flow patterns using more than one column
    • G01N30/466—Flow patterns using more than one column with separation columns in parallel
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/28—Control of physical parameters of the fluid carrier
    • G01N30/32—Control of physical parameters of the fluid carrier of pressure or speed
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N2030/022—Column chromatography characterised by the kind of separation mechanism
    • G01N2030/025—Gas chromatography

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)

Abstract

A gas chromatograph gas a column which can withstand high internal pressures. It has an inlet which means for injecting sample under pressure. A reducing valve at the column outlet controls the pressure at that point at a value between 2-50 atmospheres absolute. The valve also regulates the speed of the gas in the column so that good sepn. of the samples occurs. the reducing valver is preferably adjustable. Where samples of sepd. components are to be taken at the column and analysed. Low flow rates can be used with good sepn. still occuring. The column can be used in line with various types of spectrometer "Stop flow" working can be employed. Samples from the outlet can be taken uncontaminated by components from outside or from the feed. The pressure and concentration of samples allows them to be analysed without extra handling.
FR7605681A 1976-02-27 1976-02-27 Pressure gas chromatograph - working at 2-50 atm at its outlet for use with spectrometers Withdrawn FR2366564A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
FR7605681A FR2366564A1 (en) 1976-02-27 1976-02-27 Pressure gas chromatograph - working at 2-50 atm at its outlet for use with spectrometers

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR7605681A FR2366564A1 (en) 1976-02-27 1976-02-27 Pressure gas chromatograph - working at 2-50 atm at its outlet for use with spectrometers

Publications (1)

Publication Number Publication Date
FR2366564A1 true FR2366564A1 (en) 1978-04-28

Family

ID=9169757

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7605681A Withdrawn FR2366564A1 (en) 1976-02-27 1976-02-27 Pressure gas chromatograph - working at 2-50 atm at its outlet for use with spectrometers

Country Status (1)

Country Link
FR (1) FR2366564A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0419357A1 (en) * 1989-09-22 1991-03-27 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Process and device for dosage of impurities in a gas with gas chromatography and use for calibrating doping impurities in silane

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1109660A (en) 1964-09-08 1968-04-10 Halasz Istvan Method and apparatus for effecting automatic control of the inlet pressure of a gaschromatograph column
US3394582A (en) 1964-10-30 1968-07-30 Phillips Petroleum Co Chromatographic analysis
US3530891A (en) 1967-02-02 1970-09-29 Perkin Elmer Ltd Pressure control
US3624986A (en) 1970-09-04 1971-12-07 California Inst Of Techn Flow controller for carrier gas chromatography
US3879984A (en) 1971-02-18 1975-04-29 John Michael Welland Gas flow control
US3935097A (en) 1974-08-07 1976-01-27 Phillips Petroleum Company Acid and alcohol carrier for HF-H2 O chromatographic separation using anion exchange resin

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1109660A (en) 1964-09-08 1968-04-10 Halasz Istvan Method and apparatus for effecting automatic control of the inlet pressure of a gaschromatograph column
US3394582A (en) 1964-10-30 1968-07-30 Phillips Petroleum Co Chromatographic analysis
US3530891A (en) 1967-02-02 1970-09-29 Perkin Elmer Ltd Pressure control
US3624986A (en) 1970-09-04 1971-12-07 California Inst Of Techn Flow controller for carrier gas chromatography
US3879984A (en) 1971-02-18 1975-04-29 John Michael Welland Gas flow control
US3935097A (en) 1974-08-07 1976-01-27 Phillips Petroleum Company Acid and alcohol carrier for HF-H2 O chromatographic separation using anion exchange resin

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
NEANT *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0419357A1 (en) * 1989-09-22 1991-03-27 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Process and device for dosage of impurities in a gas with gas chromatography and use for calibrating doping impurities in silane
FR2652417A1 (en) * 1989-09-22 1991-03-29 Air Liquide METHOD AND DEVICE FOR DETERMINING IMPURITIES IN GAS BY GAS CHROMATOGRAPHY AND USE FOR CALIBRATION OF DOPING IMPURITIES IN SILANE
US5152176A (en) * 1989-09-22 1992-10-06 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Process and apparatus for determining the quality of impurities in a gas by chromatography in gas phase and utilization for measuring the quantity of doping impurities in silane

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