FR2366220A1 - Procede de regeneration d'acide sulfurique - Google Patents
Procede de regeneration d'acide sulfuriqueInfo
- Publication number
- FR2366220A1 FR2366220A1 FR7722530A FR7722530A FR2366220A1 FR 2366220 A1 FR2366220 A1 FR 2366220A1 FR 7722530 A FR7722530 A FR 7722530A FR 7722530 A FR7722530 A FR 7722530A FR 2366220 A1 FR2366220 A1 FR 2366220A1
- Authority
- FR
- France
- Prior art keywords
- regeneration process
- sulfuric acid
- acid
- acid regeneration
- vapors
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 2
- 230000008929 regeneration Effects 0.000 title abstract 2
- 238000011069 regeneration method Methods 0.000 title abstract 2
- 239000002253 acid Substances 0.000 abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- 238000001816 cooling Methods 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000007800 oxidant agent Substances 0.000 abstract 1
- 230000001590 oxidative effect Effects 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/69—Sulfur trioxide; Sulfuric acid
- C01B17/90—Separation; Purification
- C01B17/905—Removal of organic impurities
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
Procédé de régénération d'acide sulfurique. 1. On concentre l'acide par échange de chaleur indirect 2 avec les vapeurs de la deuxième étape. 2. L'acide ainsi concentré circule à contre-courant 11 avec un mélange de vapeurs d'eau et d'acide. 3. Echange de chaleur direct avec vapeur d'eau surchauffée 12. Les impuretés organiques peuvent être détruites par un oxydant 16, 17, les sels précipités par refroidissement 7.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19762632989 DE2632989A1 (de) | 1976-07-22 | 1976-07-22 | Verfahren zum regenerieren von schwefelsaeure |
Publications (1)
Publication Number | Publication Date |
---|---|
FR2366220A1 true FR2366220A1 (fr) | 1978-04-28 |
Family
ID=5983671
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7722530A Withdrawn FR2366220A1 (fr) | 1976-07-22 | 1977-07-22 | Procede de regeneration d'acide sulfurique |
Country Status (9)
Country | Link |
---|---|
US (1) | US4157381A (fr) |
JP (1) | JPS5312795A (fr) |
BE (1) | BE857042A (fr) |
CA (1) | CA1086476A (fr) |
DE (1) | DE2632989A1 (fr) |
FR (1) | FR2366220A1 (fr) |
GB (1) | GB1589732A (fr) |
IT (1) | IT1081296B (fr) |
NL (1) | NL7707924A (fr) |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2493823A1 (fr) * | 1980-11-13 | 1982-05-14 | Ugine Kuhlmann | Purification des acides sulfuriques residuaires provenant de la synthese des alcools |
US4510445A (en) * | 1981-11-02 | 1985-04-09 | Joseph Kvaternik | Miniature circuit processing devices and matrix test heads for use therein |
GB2110681B (en) * | 1981-11-25 | 1985-08-07 | Exxon Research Engineering Co | Process for treating spent sulfuric acid streams from the olefin hydration reaction |
US4406760A (en) * | 1981-11-25 | 1983-09-27 | Exxon Research & Engineering Co. | Electrolytic process for treating sulfuric acid streams |
SE464299B (sv) * | 1988-11-16 | 1991-04-08 | Boliden Contech Ab | Foerfarande foer avfaergning av svavelsyra framstaelld enligt kontaktmetoden |
US5114699A (en) * | 1989-04-12 | 1992-05-19 | Freeport-Mcmoran Resource Partners | Spent alkylation acid treatment process |
DE3927751A1 (de) * | 1989-08-23 | 1991-02-28 | Bayer Ag | Verfahren zum konzentrieren metallsulfathaltiger schwefelsaeure |
DE3935892C2 (de) * | 1989-10-27 | 1994-08-25 | Metallgesellschaft Ag | Verfahren und Vorrichtung zum Konzentrieren einer Schwefelsäure und Wasser enthaltenden Flüssigkeit |
US5275701A (en) * | 1993-03-15 | 1994-01-04 | Air Products And Chemicals, Inc. | Process for purification and concentration of sulfuric acid |
ES2105969B1 (es) * | 1995-07-14 | 1998-07-01 | Gen Quimica S A | Procedimiento para la recuperacion de acido sulfurico a partir de corrientes residuales de sulfurico de mediana concentracion contaminadas con materia organica. |
DE102005049084A1 (de) * | 2005-10-13 | 2007-04-26 | Wacker Chemie Ag | Verfahren zur Regenerierung von Schwefelsäure |
JP2013095640A (ja) * | 2011-11-01 | 2013-05-20 | Mitsubishi Gas Chemical Co Inc | 有機物を含有する硫酸を連続的に再生する方法 |
IL236365A0 (en) * | 2014-12-21 | 2015-04-30 | Melodea Ltd | Recycling of acid from acid-rich aqueous solutions |
WO2022101353A1 (fr) * | 2020-11-11 | 2022-05-19 | Basf Se | Procédé de concentration d'acide sulfurique dilué |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB441452A (en) * | 1934-04-12 | 1936-01-20 | Du Pont | Improvements in and relating to the purification of sulphuric acid |
GB512907A (en) * | 1938-03-18 | 1939-09-28 | Nicolay Titlestad | Improvements relating to the concentration and decolorization of denitrated spent sulphuric acid |
DE1233368B (de) * | 1962-08-13 | 1967-02-02 | Heraeus Schott Quarzschmelze | Verfahren zur kontinuierlichen Destillation von Schwefelsaeure in Apparaturen aus keramischen Werkstoffen |
DE2330281A1 (de) * | 1973-06-14 | 1975-01-09 | Hoechst Ag | Verfahren zur regenerierung von schwefelsaeure |
DE2352701A1 (de) * | 1973-10-20 | 1975-06-12 | Hoechst Ag | Verfahren zum aufkonzentrieren salzhaltiger, verduennter schwefelsaeure |
-
1976
- 1976-07-22 DE DE19762632989 patent/DE2632989A1/de not_active Withdrawn
-
1977
- 1977-07-15 NL NL7707924A patent/NL7707924A/xx not_active Application Discontinuation
- 1977-07-20 IT IT25930/77A patent/IT1081296B/it active
- 1977-07-21 GB GB30675/77A patent/GB1589732A/en not_active Expired
- 1977-07-21 JP JP8676277A patent/JPS5312795A/ja active Pending
- 1977-07-21 CA CA283,253A patent/CA1086476A/fr not_active Expired
- 1977-07-22 FR FR7722530A patent/FR2366220A1/fr not_active Withdrawn
- 1977-07-22 BE BE179549A patent/BE857042A/fr unknown
-
1978
- 1978-09-14 US US05/942,264 patent/US4157381A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
US4157381A (en) | 1979-06-05 |
NL7707924A (nl) | 1978-01-24 |
CA1086476A (fr) | 1980-09-30 |
DE2632989A1 (de) | 1978-02-02 |
IT1081296B (it) | 1985-05-16 |
JPS5312795A (en) | 1978-02-04 |
GB1589732A (en) | 1981-05-20 |
BE857042A (fr) | 1978-01-23 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |