FR2356599A1 - Procede et appareil pour le traitement des acides residuaires - Google Patents

Procede et appareil pour le traitement des acides residuaires

Info

Publication number
FR2356599A1
FR2356599A1 FR7720023A FR7720023A FR2356599A1 FR 2356599 A1 FR2356599 A1 FR 2356599A1 FR 7720023 A FR7720023 A FR 7720023A FR 7720023 A FR7720023 A FR 7720023A FR 2356599 A1 FR2356599 A1 FR 2356599A1
Authority
FR
France
Prior art keywords
treatment
pickling
hydrochloric acid
residual acids
bath
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7720023A
Other languages
English (en)
Other versions
FR2356599B1 (fr
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TOLEDO PICKLING STEEL SERV
Original Assignee
TOLEDO PICKLING STEEL SERV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by TOLEDO PICKLING STEEL SERV filed Critical TOLEDO PICKLING STEEL SERV
Publication of FR2356599A1 publication Critical patent/FR2356599A1/fr
Application granted granted Critical
Publication of FR2356599B1 publication Critical patent/FR2356599B1/fr
Granted legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23GCLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
    • C23G1/00Cleaning or pickling metallic material with solutions or molten salts
    • C23G1/36Regeneration of waste pickling liquors
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00Halogens; Halogen acids
    • C01B7/01Chlorine; Hydrogen chloride
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00Compounds of iron
    • C01G49/02Oxides; Hydroxides
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S423/00Chemistry of inorganic compounds
    • Y10S423/01Waste acid containing iron

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Treating Waste Gases (AREA)
  • Compounds Of Iron (AREA)
  • Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)

Abstract

L'appareillage selon l'invention comprend un appareil pour concentrer le bain acide résiduaire et un réacteur relié à cet appareil de concentration pour faire réagir le bain concentré sur des particules solides s'écoulant en même temps à travers le réacteur. Cet appareil est destiné en particulier à traiter les bains usés d'acide chlorhydrique utilisés pour le décapage du fer, de façon à produire un oxyde de fer pigmentaire et de l'acide chlorhydrique à nouveau utilisable pour le décapage.
FR7720023A 1976-07-02 1977-06-29 Procede et appareil pour le traitement des acides residuaires Granted FR2356599A1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US70208276A 1976-07-02 1976-07-02

Publications (2)

Publication Number Publication Date
FR2356599A1 true FR2356599A1 (fr) 1978-01-27
FR2356599B1 FR2356599B1 (fr) 1984-05-11

Family

ID=24819794

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7720023A Granted FR2356599A1 (fr) 1976-07-02 1977-06-29 Procede et appareil pour le traitement des acides residuaires

Country Status (9)

Country Link
US (2) US4083693A (fr)
JP (1) JPS535097A (fr)
AT (1) AT359355B (fr)
AU (1) AU512846B2 (fr)
CA (1) CA1099902A (fr)
DE (1) DE2729535A1 (fr)
FR (1) FR2356599A1 (fr)
GB (1) GB1561607A (fr)
IN (1) IN146440B (fr)

Families Citing this family (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA1149582A (fr) * 1979-02-09 1983-07-12 Pfizer Limited Pigment synthetique a base de magnetite rhomboedrique
US4382822A (en) * 1979-09-14 1983-05-10 Pfizer Inc. Synthetic rhombohedral magnetite pigment
US4436681A (en) 1982-05-17 1984-03-13 Barczak Virgil J Process for producing iron oxide weighting material from iron chloride solutions
AT395312B (de) * 1987-06-16 1992-11-25 Andritz Ag Maschf Verfahren zur gewinnung bzw. rueckgewinnung von saeure aus metallhaltigen loesungen dieser saeure
CA1327342C (fr) * 1987-11-30 1994-03-01 James Kelly Kindig Procede d'enrichissement de materiau particulaire
US5219531A (en) * 1988-04-29 1993-06-15 Atochem Production of concentrated aqueous solutions of ferric chloride
FR2670508B1 (fr) * 1990-12-13 1994-08-12 Siderurgie Fse Inst Rech Procede de separation des composes de silicium contenus dans un bain de decapage chlorhydrique de pieces notamment des toles d'acier.
AU663130B2 (en) * 1991-11-22 1995-09-28 Technological Resources Pty Limited Regeneration of hydrochloric acid
US5846510A (en) * 1991-11-22 1998-12-08 Technological Resources Pty Ltd Regeneration of hydrochloric acid
BR9205481A (pt) * 1991-11-22 1994-04-26 Tech Resources Pty Ltd Processo e aparelho para formar um lixiviante aquoso de cloreto
CN1040417C (zh) * 1992-12-18 1998-10-28 技术信息有限公司 一种从变含水氯化物浸提液生成含水氯化物浸提剂的方法
US5500098A (en) * 1993-08-05 1996-03-19 Eco-Tec Limited Process for regeneration of volatile acids
US5597547A (en) * 1995-04-13 1997-01-28 Shell Oil Company Reduction of residual chloride in iron oxides
US5730950A (en) * 1996-06-25 1998-03-24 Jennifer L. Klotz Sulfuric acid waste recycling by regenerative process
AT403665B (de) * 1996-10-30 1998-04-27 Andritz Patentverwaltung Verfahren und anlage zur abscheidung feinster oxidteilchen
EP0850881B1 (fr) * 1996-12-27 2002-08-21 Ruthner, Michael Johann, Dipl.Ing. Dr.mont. Procédé et dispositif pour la préparation d'oxydes de fer à partir de solutions d'acide chlorychique contenant des chlorures ferriques
KR100486919B1 (ko) * 1999-01-13 2005-05-03 진수곤 폐산을 이용한 금속산화물 추출장치 및 그 방법
AT407756B (de) * 1999-03-22 2001-06-25 Andritz Patentverwaltung Verfahren zur rückgewinnung von säuren aus metallhaltigen lösungen dieser säuren, vorzugsweise hc1 und fe-verbindungen
IT1311147B1 (it) * 1999-11-04 2002-03-04 Edk Res Ag Macchina per pulizia localizzata con cella, elettrolitica e/o adultrasuoni, di decapaggio e/o lucidatura
US20020005210A1 (en) * 2000-01-05 2002-01-17 Olsen Douglas R. Regenerating spent pickling liquor
US6692719B1 (en) * 2000-11-08 2004-02-17 Hatch Ltd. Process for regeneration of acid halide solutions
US7810674B2 (en) * 2005-07-26 2010-10-12 Millipore Corporation Liquid dispensing system with enhanced mixing
US7950547B2 (en) * 2006-01-12 2011-05-31 Millipore Corporation Reservoir for liquid dispensing system with enhanced mixing
CN102502880B (zh) * 2011-08-23 2016-06-22 青岛三友科技有限公司 利用酸洗废酸生产铁系净水剂的方法
CN102660751B (zh) * 2012-04-28 2014-05-21 浙江大学 金属酸洗废液的资源化处理方法及装置
CN103214050A (zh) * 2013-04-22 2013-07-24 沈阳华泰科鉴环保设备有限公司 盐酸酸洗废液铁盐与盐酸分离回收再利用装置及方法
CN103276399A (zh) * 2013-06-13 2013-09-04 句容恒达金属制品有限公司 一种减少脚手架喷涂工艺中烟雾的清洗液
CN104649335B (zh) * 2013-11-21 2016-08-17 张家港市骏马钢帘线有限公司 从盐酸酸洗废液中回收氯化亚铁晶体和盐酸的方法及装置
CN106241887A (zh) * 2016-07-20 2016-12-21 山东好帮环保科技有限公司 一种化工厂废盐酸综合利用处理工艺及其专用mvr蒸发浓缩器
CN107416959A (zh) * 2017-05-17 2017-12-01 同济大学 一种去除酸洗废液中铬镍的方法
CN113981459B (zh) * 2021-10-20 2023-10-03 北京首钢冷轧薄板有限公司 一种酸洗酸再生控制方法
CN114940514A (zh) * 2022-06-28 2022-08-26 常熟科弘材料科技有限公司 一种从废酸中制备高纯氧化铁的回收工艺

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3342557A (en) * 1967-09-19 Process of regenerating granular ma- terials impregnated with active com- ponents in a cyclic process of produc- ing chlorine
US1882864A (en) * 1926-08-18 1932-10-18 Tyler Co W S Method of and apparatus for distributing materials
US1918398A (en) * 1930-06-07 1933-07-18 Richmond Chase Company Distributor for grading machines
US1955038A (en) * 1933-03-30 1934-04-17 Fairfield Eng Co Apparatus for handling material
US3549351A (en) * 1968-01-16 1970-12-22 Hy Met Eng Ltd Method and apparatus for gas-solids reaction in production of sulfur,iron and related products
US3745207A (en) * 1971-01-25 1973-07-10 Environmental Technology Process for the recovery of waste pickle liquor

Also Published As

Publication number Publication date
US4107267A (en) 1978-08-15
CA1099902A (fr) 1981-04-28
AU2610477A (en) 1978-12-21
ATA439177A (de) 1980-03-15
IN146440B (fr) 1979-06-02
AU512846B2 (en) 1980-10-30
FR2356599B1 (fr) 1984-05-11
GB1561607A (en) 1980-02-27
AT359355B (de) 1980-11-10
DE2729535A1 (de) 1978-01-05
US4083693A (en) 1978-04-11
JPS535097A (en) 1978-01-18

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