FR2268798A1 - 3(5)-Phenyl 4-nitro 5(3)-amino pyrazole - prepd by reaction of acetyl nitrate on 3(5)-phenyl 5(3)acylamino pyrazole - Google Patents

3(5)-Phenyl 4-nitro 5(3)-amino pyrazole - prepd by reaction of acetyl nitrate on 3(5)-phenyl 5(3)acylamino pyrazole

Info

Publication number
FR2268798A1
FR2268798A1 FR7413992A FR7413992A FR2268798A1 FR 2268798 A1 FR2268798 A1 FR 2268798A1 FR 7413992 A FR7413992 A FR 7413992A FR 7413992 A FR7413992 A FR 7413992A FR 2268798 A1 FR2268798 A1 FR 2268798A1
Authority
FR
France
Prior art keywords
pyrazole
phenyl
pts
prepd
acylamino
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7413992A
Other languages
French (fr)
Other versions
FR2268798B1 (en
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Produits Chimiques Ugine Kuhlmann
Ugine Kuhlmann SA
Original Assignee
Produits Chimiques Ugine Kuhlmann
Ugine Kuhlmann SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Produits Chimiques Ugine Kuhlmann, Ugine Kuhlmann SA filed Critical Produits Chimiques Ugine Kuhlmann
Priority to FR7413992A priority Critical patent/FR2268798A1/en
Publication of FR2268798A1 publication Critical patent/FR2268798A1/en
Application granted granted Critical
Publication of FR2268798B1 publication Critical patent/FR2268798B1/fr
Granted legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/38Nitrogen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

5(3) amino pyrazole, of formula: is a new cpd. prepd. by reacting acetyl nitrate with 3(5)-phenyl 5(3)-acylamino pyrazole (II). It may be diazotised and coupled to give dyes. Diazotization is pref. carried out in the presence of low mol. wt. acids, e.g. acetic or propionic or concentrated mineral acid. In an example 84 pts. cpd. (II) were dissolved in 100 pts. glacial acetic acid 370 pts., acetic acid were added gradually, then, after 1/2 hr., 42 pts. fuming HNO3 in 300 pts. glacial acetic acid. The product was stirred for 48 hrs. and cpd. (I) pptd. by dilution with ice/water mixture.
FR7413992A 1974-04-23 1974-04-23 3(5)-Phenyl 4-nitro 5(3)-amino pyrazole - prepd by reaction of acetyl nitrate on 3(5)-phenyl 5(3)acylamino pyrazole Granted FR2268798A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
FR7413992A FR2268798A1 (en) 1974-04-23 1974-04-23 3(5)-Phenyl 4-nitro 5(3)-amino pyrazole - prepd by reaction of acetyl nitrate on 3(5)-phenyl 5(3)acylamino pyrazole

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR7413992A FR2268798A1 (en) 1974-04-23 1974-04-23 3(5)-Phenyl 4-nitro 5(3)-amino pyrazole - prepd by reaction of acetyl nitrate on 3(5)-phenyl 5(3)acylamino pyrazole

Publications (2)

Publication Number Publication Date
FR2268798A1 true FR2268798A1 (en) 1975-11-21
FR2268798B1 FR2268798B1 (en) 1976-12-17

Family

ID=9137971

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7413992A Granted FR2268798A1 (en) 1974-04-23 1974-04-23 3(5)-Phenyl 4-nitro 5(3)-amino pyrazole - prepd by reaction of acetyl nitrate on 3(5)-phenyl 5(3)acylamino pyrazole

Country Status (1)

Country Link
FR (1) FR2268798A1 (en)

Also Published As

Publication number Publication date
FR2268798B1 (en) 1976-12-17

Similar Documents

Publication Publication Date Title
FR2268798A1 (en) 3(5)-Phenyl 4-nitro 5(3)-amino pyrazole - prepd by reaction of acetyl nitrate on 3(5)-phenyl 5(3)acylamino pyrazole
GB1316332A (en) Continuous production of alkali metal salts of anthranilic acid and of isatoic anhydride
GB1343118A (en) Salicylic acid derivatives
JPS57187358A (en) Production of arylazo-amino-naphtholsulfonic acid
GB761093A (en) Production of s-acetyl glutathione
US4172098A (en) Manufacture of substituted halobenzenes
GB1164752A (en) Process for the Production of Nitroaryl Sulphonic Acids
GB1509842A (en) Azo-benzothiazolium dyestuffs
GB663870A (en) Diazotisation method for the esters of aminobenzoic acids
US3051750A (en) Nitrosation process
US2445242A (en) Process for producing a 4-amino salicylic acid
GB390556A (en) The manufacture of nitro compounds of the diphenyl series
JPS5735556A (en) Preparation of guanidinomethylcyclohexanecarboxylic acid ester
FR2084591A5 (en) Meta-fluoroanilines from meta-aminoacetanilides
GB1072166A (en) Process for preparing sultones
GB622935A (en) A process for the production of insoluble macro-molecular azo compounds
SU466216A1 (en) The method of obtaining diazo compounds of the difficultly digested amines of the benzene series
GB586217A (en) Manufacture of p-aminobenzene sulphone acyl amides
US2166681A (en) Oiazoamino compounds
JPS6326752B2 (en)
Pettip et al. Studies of trifluoroacetic acid. Part XI. The reactions of diazonium trifluoroacetates with aromatic compounds to give diaryls
Khalifa 369. The effect of substituents on the reduction of azo-compounds
ES429144A1 (en) Nitroguanidine from dicyandiamide by sulphonation then nitration - using above 85 percent sulphuric acid for sulphonation
GB673709A (en) Linear derivatives of nitroguanidine
GB793921A (en) A process for working up products containing the alkali metal salts of terephthalic acid

Legal Events

Date Code Title Description
ST Notification of lapse