FR2197465A5 - Viscosimetric detector for chromatographic eluent - comprising pressure detector pref. sited between column outlet and capillary orifice - Google Patents
Viscosimetric detector for chromatographic eluent - comprising pressure detector pref. sited between column outlet and capillary orificeInfo
- Publication number
- FR2197465A5 FR2197465A5 FR7230347A FR7230347A FR2197465A5 FR 2197465 A5 FR2197465 A5 FR 2197465A5 FR 7230347 A FR7230347 A FR 7230347A FR 7230347 A FR7230347 A FR 7230347A FR 2197465 A5 FR2197465 A5 FR 2197465A5
- Authority
- FR
- France
- Prior art keywords
- detector
- column
- sited
- pref
- capillary orifice
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N11/00—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
- G01N11/02—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material
- G01N11/04—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material through a restricted passage, e.g. tube, aperture
- G01N11/08—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material through a restricted passage, e.g. tube, aperture by measuring pressure required to produce a known flow
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
Abstract
Element peaks in a chromatographic column are detected by an e.g. piezoelectric pressure detector (with minimal dead space), pref. sited between the column outlet and a capillary orifice, or alternatively at the column inlet, or at a point in the column. The detector may be absolute; or may be a differential detector, e.g. between two parallel columns, one of which is fed with solvent only. The column is fed at pressure controlled e.g. to plus-or-minus .1% or at controlled flow; and the measured pressure fluctuations are due to enhancement of carrier viscosity; the area of the peaks being proportional to log. relative viscosity so that mol. wt. or intrinsic viscosity of solute. may be measured. The detector is non-specific but sensitive, and is simple to construct and use.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7230347A FR2197465A5 (en) | 1972-08-25 | 1972-08-25 | Viscosimetric detector for chromatographic eluent - comprising pressure detector pref. sited between column outlet and capillary orifice |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7230347A FR2197465A5 (en) | 1972-08-25 | 1972-08-25 | Viscosimetric detector for chromatographic eluent - comprising pressure detector pref. sited between column outlet and capillary orifice |
Publications (1)
Publication Number | Publication Date |
---|---|
FR2197465A5 true FR2197465A5 (en) | 1974-03-22 |
Family
ID=9103561
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7230347A Expired FR2197465A5 (en) | 1972-08-25 | 1972-08-25 | Viscosimetric detector for chromatographic eluent - comprising pressure detector pref. sited between column outlet and capillary orifice |
Country Status (1)
Country | Link |
---|---|
FR (1) | FR2197465A5 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2519143A1 (en) * | 1981-12-29 | 1983-07-01 | Elf Aquitaine | VISCOSIMETER OPERATING IN CONTINUOUS PARTICULARLY AT HIGH TEMPERATURE |
-
1972
- 1972-08-25 FR FR7230347A patent/FR2197465A5/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2519143A1 (en) * | 1981-12-29 | 1983-07-01 | Elf Aquitaine | VISCOSIMETER OPERATING IN CONTINUOUS PARTICULARLY AT HIGH TEMPERATURE |
EP0083524A1 (en) * | 1981-12-29 | 1983-07-13 | Societe Nationale Elf Aquitaine (Production) | Installation for controlling the continuous functioning of a chromatographic system |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |