FR2128968A6 - Purification of wet-process phosphoric acid - by extraction - with part water-misc organic solvent - Google Patents

Purification of wet-process phosphoric acid - by extraction - with part water-misc organic solvent

Info

Publication number
FR2128968A6
FR2128968A6 FR7108242A FR7108242A FR2128968A6 FR 2128968 A6 FR2128968 A6 FR 2128968A6 FR 7108242 A FR7108242 A FR 7108242A FR 7108242 A FR7108242 A FR 7108242A FR 2128968 A6 FR2128968 A6 FR 2128968A6
Authority
FR
France
Prior art keywords
organic solvent
phosphoric acid
wet
extraction
misc
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
FR7108242A
Other languages
French (fr)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Azote et Produits Chimiques SA
Original Assignee
Azote et Produits Chimiques SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Azote et Produits Chimiques SA filed Critical Azote et Produits Chimiques SA
Priority to FR7108242A priority Critical patent/FR2128968A6/en
Priority to SE667371A priority patent/SE366972B/xx
Priority to DE19712127141 priority patent/DE2127141C3/en
Priority to FI154371A priority patent/FI54908C/en
Priority to NL7107718A priority patent/NL157578B/en
Priority to GB1951571A priority patent/GB1357614A/en
Priority to NO219671A priority patent/NO132389C/no
Priority to BE768426A priority patent/BE768426A/en
Application granted granted Critical
Publication of FR2128968A6 publication Critical patent/FR2128968A6/en
Priority to US05/440,333 priority patent/US3956465A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/16Oxyacids of phosphorus; Salts thereof
    • C01B25/18Phosphoric acid
    • C01B25/234Purification; Stabilisation; Concentration

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Saccharide Compounds (AREA)

Abstract

The wet-process phosphoric acid is extracted with an organic solvent which is capable of extracting phosphoric acid, and which is partially miscible with H2O, but contains not more than 40-50% of the H2O required to saturate it. Suitable solvents are those which contain 2-30 wt.% of H2O at 25 degrees C. when saturated e.g. 4-10C aliphatic alcohols, cyclopentanol, benzyl alcohol, isopropyl acetate, tributyl phosphate. The phosphoric may be sepd. form the organic solvent by re-extraction with H2O, in which case the solvent is distilled before recycling to remove some of its H2O or by neutralisation with NaOH, CA2CO3, KOH, K2CO3 or NH3. In this case the recovered organic solvent may be recycled without further treatment. High yields are obtained, even from dil. phosphoric acid soln., and the product is suitable for use in the food and detergent industries.
FR7108242A 1970-06-12 1971-03-10 Purification of wet-process phosphoric acid - by extraction - with part water-misc organic solvent Expired FR2128968A6 (en)

Priority Applications (9)

Application Number Priority Date Filing Date Title
FR7108242A FR2128968A6 (en) 1971-03-10 1971-03-10 Purification of wet-process phosphoric acid - by extraction - with part water-misc organic solvent
SE667371A SE366972B (en) 1970-06-12 1971-05-24
DE19712127141 DE2127141C3 (en) 1970-06-12 1971-06-01 Process for purifying wet process phosphoric acid
FI154371A FI54908C (en) 1970-06-12 1971-06-03 SAETT ATT RENA PAO VAOT VAEG FRAMSTAELLD FOSFORSYRA
NL7107718A NL157578B (en) 1970-06-12 1971-06-04 PROCESS FOR THE PURIFICATION OF PHOSPHORIC ACID PREPARED ALONG WET ROAD.
GB1951571A GB1357614A (en) 1970-06-12 1971-06-08 Purification of phosphoric acid
NO219671A NO132389C (en) 1970-06-12 1971-06-10
BE768426A BE768426A (en) 1970-06-12 1971-06-11 WET PHOSPHORIC ACID PURIFICATION
US05/440,333 US3956465A (en) 1970-06-12 1974-02-07 Solvent purification of wet process phosphoric acid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR7108242A FR2128968A6 (en) 1971-03-10 1971-03-10 Purification of wet-process phosphoric acid - by extraction - with part water-misc organic solvent

Publications (1)

Publication Number Publication Date
FR2128968A6 true FR2128968A6 (en) 1972-10-27

Family

ID=9073256

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7108242A Expired FR2128968A6 (en) 1970-06-12 1971-03-10 Purification of wet-process phosphoric acid - by extraction - with part water-misc organic solvent

Country Status (1)

Country Link
FR (1) FR2128968A6 (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2374262A1 (en) * 1976-12-17 1978-07-13 Hoechst Ag PROCESS FOR DECONTAMINATION OF PHOSPHORIC ACID PREPARED BY WET METHOD
FR2374263A1 (en) * 1976-12-17 1978-07-13 Hoechst Ag PROCESS FOR PURIFYING PHOSPHORIC ACID PREPARED BY WET METHOD

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2374262A1 (en) * 1976-12-17 1978-07-13 Hoechst Ag PROCESS FOR DECONTAMINATION OF PHOSPHORIC ACID PREPARED BY WET METHOD
FR2374263A1 (en) * 1976-12-17 1978-07-13 Hoechst Ag PROCESS FOR PURIFYING PHOSPHORIC ACID PREPARED BY WET METHOD

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