FI91278B - Förfarande för framställning av tensidblandningar - Google Patents
Förfarande för framställning av tensidblandningar Download PDFInfo
- Publication number
- FI91278B FI91278B FI922258A FI922258A FI91278B FI 91278 B FI91278 B FI 91278B FI 922258 A FI922258 A FI 922258A FI 922258 A FI922258 A FI 922258A FI 91278 B FI91278 B FI 91278B
- Authority
- FI
- Finland
- Prior art keywords
- mixture
- alkyl
- process according
- triethanolamine
- formula
- Prior art date
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- 239000000203 mixture Substances 0.000 title claims abstract description 42
- 238000004519 manufacturing process Methods 0.000 title description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 38
- -1 alkali metal salt Chemical class 0.000 claims abstract description 28
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims abstract description 27
- 239000002253 acid Substances 0.000 claims abstract description 14
- 229910052783 alkali metal Inorganic materials 0.000 claims abstract description 14
- 150000007524 organic acids Chemical class 0.000 claims abstract description 12
- 235000005985 organic acids Nutrition 0.000 claims abstract description 9
- 238000002360 preparation method Methods 0.000 claims abstract description 6
- 150000007513 acids Chemical class 0.000 claims abstract description 5
- 238000001816 cooling Methods 0.000 claims abstract description 5
- 239000011541 reaction mixture Substances 0.000 claims abstract description 5
- 238000003756 stirring Methods 0.000 claims abstract description 4
- 238000000034 method Methods 0.000 claims description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 239000004094 surface-active agent Substances 0.000 claims description 18
- 150000008052 alkyl sulfonates Chemical class 0.000 claims description 12
- 229910021653 sulphate ion Inorganic materials 0.000 claims description 11
- 239000000654 additive Substances 0.000 claims description 10
- 125000000217 alkyl group Chemical group 0.000 claims description 9
- 150000001875 compounds Chemical class 0.000 claims description 9
- 150000001408 amides Chemical class 0.000 claims description 6
- 125000000129 anionic group Chemical group 0.000 claims description 6
- 159000000000 sodium salts Chemical class 0.000 claims description 6
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 5
- 125000004432 carbon atom Chemical group C* 0.000 claims description 3
- 230000000694 effects Effects 0.000 claims description 3
- 239000002736 nonionic surfactant Substances 0.000 claims description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
- 229910052739 hydrogen Inorganic materials 0.000 claims description 2
- 239000001257 hydrogen Substances 0.000 claims description 2
- QPILZZVXGUNELN-UHFFFAOYSA-M sodium;4-amino-5-hydroxynaphthalene-2,7-disulfonate;hydron Chemical compound [Na+].OS(=O)(=O)C1=CC(O)=C2C(N)=CC(S([O-])(=O)=O)=CC2=C1 QPILZZVXGUNELN-UHFFFAOYSA-M 0.000 claims 1
- 150000003839 salts Chemical class 0.000 abstract description 6
- 239000002453 shampoo Substances 0.000 description 20
- 235000002639 sodium chloride Nutrition 0.000 description 18
- 239000000047 product Substances 0.000 description 14
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 12
- 239000003599 detergent Substances 0.000 description 9
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 8
- 229910052708 sodium Inorganic materials 0.000 description 8
- 239000011734 sodium Substances 0.000 description 8
- 239000006260 foam Substances 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 6
- 238000005406 washing Methods 0.000 description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 5
- 239000004480 active ingredient Substances 0.000 description 5
- 239000011780 sodium chloride Substances 0.000 description 5
- AYFACLKQYVTXNS-UHFFFAOYSA-M sodium;tetradecane-1-sulfonate Chemical compound [Na+].CCCCCCCCCCCCCCS([O-])(=O)=O AYFACLKQYVTXNS-UHFFFAOYSA-M 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 239000002699 waste material Substances 0.000 description 5
- 239000000243 solution Substances 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- 239000013543 active substance Substances 0.000 description 3
- 239000002585 base Substances 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 2
- 150000001340 alkali metals Chemical class 0.000 description 2
- 150000008051 alkyl sulfates Chemical class 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 description 2
- 239000003337 fertilizer Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000006386 neutralization reaction Methods 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- 239000003755 preservative agent Substances 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- GAWIXWVDTYZWAW-UHFFFAOYSA-N C[CH]O Chemical group C[CH]O GAWIXWVDTYZWAW-UHFFFAOYSA-N 0.000 description 1
- 244000060011 Cocos nucifera Species 0.000 description 1
- 235000013162 Cocos nucifera Nutrition 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000004594 Masterbatch (MB) Substances 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 229910006069 SO3H Inorganic materials 0.000 description 1
- 206010039792 Seborrhoea Diseases 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 229910052936 alkali metal sulfate Inorganic materials 0.000 description 1
- 150000005215 alkyl ethers Chemical class 0.000 description 1
- 238000005275 alloying Methods 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000004851 dishwashing Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 230000004720 fertilization Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000008233 hard water Substances 0.000 description 1
- 230000008821 health effect Effects 0.000 description 1
- 125000001183 hydrocarbyl group Chemical group 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 229940083980 lavender extract Drugs 0.000 description 1
- 235000020723 lavender extract Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 239000003895 organic fertilizer Substances 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000000546 pharmaceutical excipient Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 235000010265 sodium sulphite Nutrition 0.000 description 1
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulphite Substances [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 1
- 239000008234 soft water Substances 0.000 description 1
- 239000010675 spruce oil Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 description 1
- 150000008054 sulfonate salts Chemical class 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
- C09K23/017—Mixtures of compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
- C09K23/02—Alkyl sulfonates or sulfuric acid ester salts derived from monohydric alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
- C11D1/143—Sulfonic acid esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/37—Mixtures of compounds all of which are anionic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/52—Carboxylic amides, alkylolamides or imides or their condensation products with alkylene oxides
- C11D1/523—Carboxylic alkylolamides, or dialkylolamides, or hydroxycarboxylic amides (R1-CO-NR2R3), where R1, R2 or R3 contain one hydroxy group per alkyl group
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/65—Mixtures of anionic with cationic compounds
- C11D1/652—Mixtures of anionic compounds with carboxylic amides or alkylol amides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/65—Mixtures of anionic with cationic compounds
- C11D1/655—Mixtures of sulfonated products with alkylolamides of carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/04—Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/52—Carboxylic amides, alkylolamides or imides or their condensation products with alkylene oxides
- C11D1/526—Carboxylic amides (R1-CO-NR2R3), where R1, R2 or R3 are polyalkoxylated
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- Materials Engineering (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Cosmetics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
- Detergent Compositions (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Compounds Of Unknown Constitution (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
- Measurement Of Radiation (AREA)
Claims (10)
1. Förfarande för framställning av tensidblandningar, kännetecknad därav, att man 5. behandlar en blandning, som innehäller - ett alkalimetallsalt av en alkylsulfonsyra, - en etoxylerad alkanolamid som non-jonogen tensld, samt - en N-mono- och/eller Ν,Ν-dialkanolamid, 10 och eventuelit - ett alkalimetallsalt av en etoxylerad alkylsulfat, med en stark, över 70%: ig svavelsyra, som f inns i över-skott, för att frigöra de organiska syrorna under samtidig 15 blandning och vid behov kylning sä att blandningens tempe-ratur stiger högst tili cirka 35°C, - liter reaktionsblandningen separera i tvä skikt, - avskiljer skiktet, som innehäller de organiska syrorna, och neutraliserar detsamma med en di- och/eller trietanol- 20 amin för framställning av di- och/eller trietanolaminsal-terna av de nämnda syrorna, och eventuellt tillsätter vat-ten och vanliga tillsats- och hjälpmedel.
2. Förfarande enligt patentkravet l, kännetecknat därav, 25 att man reglerar blandningens temperatur med tillsatshas- tigheten av svavelsyra.
3. Förfarande enligt patentkravet 1 eller 2, kännetecknat därav, att förhällandet av alkylsulfonat- och -sulfatkom- 30 ponenterna tili amidkomponenterna är cirka 1:1 - 7:1, sär-skilt cirka 2:1 - 4:1.
4. Förfarande enligt patentkravet 3, kännetecknat därav, att förhällandet av alkylsulfonatkomponenten tili alkyl- 35 sulfatkomponenten är ätminstone cirka 3:2, företrädesvis ätminstone 2:1. 91278
5. Förfarande enligt patentkravet 3, kännetecknat därav, att förhällandet av den etoxylerade alkanolamiden tili mono- och dialkylamiden är cirka 1:1 - 6:1, företrädesvis cirka 3:1 - 5:1. 5
6. Förfarande enligt nägot av patentkraven 1-5, känneteck-nat därav, att man använder som alkylsulfonat ett alkalime-tallsalt, särskilt ett natriumsalt, av en syra med formeln
10. S03H i vilken formel R är en primär eller sekundär alkylgrupp med 6-18 kolatomer eller en blandning av alkylgrupper. 15 7. Förfarande enligt nigot av patentkraven 1-6, känneteck nat därav, att man använder som etoxylerad alkanolamid en förening med formeln RCONHC2H4 (OCH2CH2) x0H 20 i vilken R betecknar detsamma som i kravet 5 och x är ett heltal av cirka 2-6, särskilt 5.
8. Förfarande enligt nägot av patentkraven 1-7, känneteck-25 nat därav, att man använder som N-mono- och N,N-dialkanol- amid en förening med formeln R c (=0) -NRjR2 30. vilken R betecknar detsamma som i kravet 6, R, är väte eller en hydroxi-Ci-C3-alkyl och R2 är en hydroxi-C,-C3-al-kyl.
9. Förfarande enligt nägot av patentkraven 1-8, känneteck-35 nat därav, att man använder som etoxylerad alkylsulfat ett alkalimetallsalt, särskilt ett natriumsalt, av en förening med formeln R(0CH2CH2)x0S03H varvid R och x i formeln betecknar detsamma som ovan i kravet 6 och respektive i kravet 7. 5
10. Förfarande enligt patentkravet 1, kännetecknat därav, att man framställer en tensldblandning, som innehäller 1) 30-50 viktdelar av ett di- och/eller trietanolaminsalt 10 av en förening RS03H, 2) 5-10 viktdelar av en förening med formeln RCONHC2H4 (OCH2CH2) xOH , 15 3) 2-5 viktdelar av en amid med formeln RC(=0)-NR,R2/ 4) 0-10 viktdelar av ett di- och/eller trietanolaminsalt av en förening R(0CH2CH2)x0S03H, 20. vilka formler R, x, Rt och R2 betecknar detsamma som i kravet 6, 7 och respektive 8, den mängd vatten som behövs för regiering till en lämplig anjonaktivitet och viskosi-tet, samt eventuellt andra tillsatsämnen.
Priority Applications (14)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FI922258A FI91278C (sv) | 1992-05-18 | 1992-05-18 | Förfarande för framställning av tensidblandningar |
| AU54674/94A AU5467494A (en) | 1992-05-18 | 1993-11-17 | Process for the preparation of tenside mixtures |
| HU9601341A HU218346B (hu) | 1992-05-18 | 1993-11-17 | Eljárás tenzidkeverékek előállítására |
| DE69332313T DE69332313T2 (de) | 1992-05-18 | 1993-11-17 | Verfahren zur herstellung von tensidhaltigen mischungen |
| CA002176922A CA2176922C (en) | 1992-05-18 | 1993-11-17 | Process for the preparation of tenside mixtures |
| DK94900172T DK0729500T3 (da) | 1992-05-18 | 1993-11-17 | Fremgangsmåde til fremstilling af blandinger indeholdende tensid |
| PT94900172T PT729500E (pt) | 1992-05-18 | 1993-11-17 | Processo de preparacao de amisturas que compreendem agentes tensioactivos |
| PCT/FI1993/000487 WO1995014071A1 (en) | 1992-05-18 | 1993-11-17 | Process for the preparation of tenside mixtures |
| EP94900172A EP0729500B1 (en) | 1992-05-18 | 1993-11-17 | Process for the preparation of mixtures comprising tenside |
| AT94900172T ATE224436T1 (de) | 1992-05-18 | 1993-11-17 | Verfahren zur herstellung von tensidhaltigen mischungen |
| US08/648,050 US5981453A (en) | 1992-05-18 | 1993-11-17 | Process for the preparation of tenside mixtures |
| ES94900172T ES2181705T3 (es) | 1992-05-18 | 1993-11-17 | Procedimiento para la preparacion de mezclas que comprenden agentes tensioactivos. |
| EE9400340A EE03113B1 (et) | 1992-05-18 | 1994-11-21 | Tensiidisegu valmistamise meetod |
| NO19962044A NO311581B1 (no) | 1992-05-18 | 1996-05-20 | Fremgangsmåte ved fremstilling av tensidblandinger |
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FI922258 | 1992-05-18 | ||
| FI922258A FI91278C (sv) | 1992-05-18 | 1992-05-18 | Förfarande för framställning av tensidblandningar |
| PCT/FI1993/000487 WO1995014071A1 (en) | 1992-05-18 | 1993-11-17 | Process for the preparation of tenside mixtures |
| FI9300487 | 1993-11-17 |
Publications (4)
| Publication Number | Publication Date |
|---|---|
| FI922258A0 FI922258A0 (sv) | 1992-05-18 |
| FI922258A FI922258A (sv) | 1993-11-19 |
| FI91278B true FI91278B (sv) | 1994-02-28 |
| FI91278C FI91278C (sv) | 1995-04-18 |
Family
ID=26159244
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FI922258A FI91278C (sv) | 1992-05-18 | 1992-05-18 | Förfarande för framställning av tensidblandningar |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US5981453A (sv) |
| EP (1) | EP0729500B1 (sv) |
| AT (1) | ATE224436T1 (sv) |
| AU (1) | AU5467494A (sv) |
| CA (1) | CA2176922C (sv) |
| DE (1) | DE69332313T2 (sv) |
| DK (1) | DK0729500T3 (sv) |
| EE (1) | EE03113B1 (sv) |
| ES (1) | ES2181705T3 (sv) |
| FI (1) | FI91278C (sv) |
| HU (1) | HU218346B (sv) |
| NO (1) | NO311581B1 (sv) |
| PT (1) | PT729500E (sv) |
| WO (1) | WO1995014071A1 (sv) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1995014071A1 (en) * | 1992-05-18 | 1995-05-26 | Oy Ks-Chemitra Ltd. | Process for the preparation of tenside mixtures |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB0819804D0 (en) | 2008-10-29 | 2008-12-03 | Reckitt Benckiser Inc | Concentrated hard surface treatment compositions |
| MX2012012240A (es) * | 2010-04-19 | 2012-11-23 | Procter & Gamble | Proceso para elaborar una composicion detergente liquida. |
| US8563497B2 (en) | 2010-04-19 | 2013-10-22 | The Procter & Gamble Company | Process for making a detergent based composition |
| CA2795931C (en) * | 2010-04-19 | 2015-02-17 | The Procter & Gamble Company | Process for making a detergent base composition |
| FI20115276A0 (sv) | 2011-03-22 | 2011-03-22 | 3S Cosmetics Oy | Borttagningskomposition för nagellack och användning av denna |
| FI20116062L (sv) | 2011-10-28 | 2013-04-29 | Bt Wood Oy | Förfarande för behandling av trämaterial samt med förfarandet producerat trämaterial |
| CN115677877B (zh) * | 2022-10-10 | 2023-09-12 | 石家庄鸿泰橡胶有限公司 | 一种羧基丁腈胶乳用复合乳化剂、羧基丁腈胶乳及制备方法和应用 |
| WO2024182020A1 (en) * | 2023-02-28 | 2024-09-06 | Energizer Auto, Inc. | Vehicle cleaning compositions |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE715798C (de) * | 1940-03-06 | 1942-01-07 | Hansa Muehle Akt Ges | Verfahren zur Herstellung von Rasierseife |
| DE1014067B (de) * | 1953-07-29 | 1957-08-22 | Basf Ag | Netzmittel fuer Merzerisier- und Laugierbaeder |
| DE1619040B2 (de) * | 1967-02-02 | 1974-01-24 | Farbwerke Hoechst Ag, Vormals Meister Lucius & Bruening, 6000 Frankfurt | Netzmittel für alkalische Bäder |
| US3804819A (en) * | 1972-05-03 | 1974-04-16 | Scm Corp | Recovery of fatty acids from tall oil heads |
| US4476044A (en) * | 1982-05-13 | 1984-10-09 | Henkel Corporation | Surfactant product |
| US5308372A (en) * | 1984-01-18 | 1994-05-03 | Daniels Ralph S | Vegetable oil processing to obtain nutrient by-products |
| GB8602589D0 (en) * | 1986-02-03 | 1986-03-12 | Unilever Plc | Detergent compositions |
| US4753747A (en) * | 1987-05-12 | 1988-06-28 | Colgate-Palmolive Co. | Process of neutralizing mono-carboxylic acid |
| GB8906573D0 (en) * | 1989-03-22 | 1989-05-04 | Unilever Plc | Detergent bar manufacture |
| US5075041A (en) * | 1990-06-28 | 1991-12-24 | Shell Oil Company | Process for the preparation of secondary alcohol sulfate-containing surfactant compositions |
| FI91278C (sv) * | 1992-05-18 | 1995-04-18 | Ks Chemitra Ltd Oy | Förfarande för framställning av tensidblandningar |
| FI91274C (sv) * | 1992-05-18 | 1995-11-14 | Ks Chemitra Ltd Oy | Tvättmedel och förfarande för dess framställning |
-
1992
- 1992-05-18 FI FI922258A patent/FI91278C/sv not_active IP Right Cessation
-
1993
- 1993-11-17 AT AT94900172T patent/ATE224436T1/de not_active IP Right Cessation
- 1993-11-17 AU AU54674/94A patent/AU5467494A/en not_active Abandoned
- 1993-11-17 DE DE69332313T patent/DE69332313T2/de not_active Expired - Fee Related
- 1993-11-17 DK DK94900172T patent/DK0729500T3/da active
- 1993-11-17 HU HU9601341A patent/HU218346B/hu not_active IP Right Cessation
- 1993-11-17 CA CA002176922A patent/CA2176922C/en not_active Expired - Fee Related
- 1993-11-17 EP EP94900172A patent/EP0729500B1/en not_active Expired - Lifetime
- 1993-11-17 WO PCT/FI1993/000487 patent/WO1995014071A1/en active IP Right Grant
- 1993-11-17 PT PT94900172T patent/PT729500E/pt unknown
- 1993-11-17 ES ES94900172T patent/ES2181705T3/es not_active Expired - Lifetime
- 1993-11-17 US US08/648,050 patent/US5981453A/en not_active Expired - Lifetime
-
1994
- 1994-11-21 EE EE9400340A patent/EE03113B1/xx unknown
-
1996
- 1996-05-20 NO NO19962044A patent/NO311581B1/no not_active IP Right Cessation
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1995014071A1 (en) * | 1992-05-18 | 1995-05-26 | Oy Ks-Chemitra Ltd. | Process for the preparation of tenside mixtures |
Also Published As
| Publication number | Publication date |
|---|---|
| HU9601341D0 (en) | 1996-07-29 |
| US5981453A (en) | 1999-11-09 |
| ES2181705T3 (es) | 2003-03-01 |
| HU218346B (hu) | 2000-08-28 |
| DK0729500T3 (da) | 2003-01-20 |
| HUT76429A (en) | 1997-08-28 |
| ATE224436T1 (de) | 2002-10-15 |
| EE03113B1 (et) | 1998-08-17 |
| NO962044L (no) | 1996-07-10 |
| AU5467494A (en) | 1995-06-06 |
| PT729500E (pt) | 2003-01-31 |
| WO1995014071A1 (en) | 1995-05-26 |
| DE69332313D1 (de) | 2002-10-24 |
| CA2176922C (en) | 2005-05-17 |
| NO311581B1 (no) | 2001-12-10 |
| NO962044D0 (no) | 1996-05-20 |
| EP0729500B1 (en) | 2002-09-18 |
| FI91278C (sv) | 1995-04-18 |
| DE69332313T2 (de) | 2003-07-31 |
| CA2176922A1 (en) | 1995-05-26 |
| EP0729500A1 (en) | 1996-09-04 |
| FI922258A0 (sv) | 1992-05-18 |
| FI922258A (sv) | 1993-11-19 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| BB | Publication of examined application | ||
| PC | Transfer of assignment of patent |
Owner name: OY FAINTEND LTD |
|
| MA | Patent expired |