FI3210978T3 - Process for producing acesulfame potassium - Google Patents
Process for producing acesulfame potassium Download PDFInfo
- Publication number
- FI3210978T3 FI3210978T3 FIEP17151405.2T FI17151405T FI3210978T3 FI 3210978 T3 FI3210978 T3 FI 3210978T3 FI 17151405 T FI17151405 T FI 17151405T FI 3210978 T3 FI3210978 T3 FI 3210978T3
- Authority
- FI
- Finland
- Prior art keywords
- salt
- acid
- acetoacetamide
- formation reaction
- amine
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims 20
- WBZFUFAFFUEMEI-UHFFFAOYSA-M Acesulfame k Chemical compound [K+].CC1=CC(=O)[N-]S(=O)(=O)O1 WBZFUFAFFUEMEI-UHFFFAOYSA-M 0.000 title claims 5
- 229960004998 acesulfame potassium Drugs 0.000 title claims 5
- 235000010358 acesulfame potassium Nutrition 0.000 title claims 5
- 239000000619 acesulfame-K Substances 0.000 title claims 5
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 15
- 150000003839 salts Chemical class 0.000 claims 15
- 239000002253 acid Substances 0.000 claims 12
- GCPWJFKTWGFEHH-UHFFFAOYSA-N acetoacetamide Chemical class CC(=O)CC(N)=O GCPWJFKTWGFEHH-UHFFFAOYSA-N 0.000 claims 9
- 238000005755 formation reaction Methods 0.000 claims 9
- 150000001412 amines Chemical class 0.000 claims 7
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 claims 6
- LNOPIUAQISRISI-UHFFFAOYSA-N n'-hydroxy-2-propan-2-ylsulfonylethanimidamide Chemical compound CC(C)S(=O)(=O)CC(N)=NO LNOPIUAQISRISI-UHFFFAOYSA-N 0.000 claims 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 3
- 125000004122 cyclic group Chemical group 0.000 claims 3
- 239000011541 reaction mixture Substances 0.000 claims 3
- 238000006243 chemical reaction Methods 0.000 claims 2
- WASQWSOJHCZDFK-UHFFFAOYSA-N diketene Chemical compound C=C1CC(=O)O1 WASQWSOJHCZDFK-UHFFFAOYSA-N 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 230000003301 hydrolyzing effect Effects 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 239000011591 potassium Substances 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C307/00—Amides of sulfuric acids, i.e. compounds having singly-bound oxygen atoms of sulfate groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
- C07C307/02—Monoamides of sulfuric acids or esters thereof, e.g. sulfamic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/34—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfuric acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D291/00—Heterocyclic compounds containing rings having nitrogen, oxygen and sulfur atoms as the only ring hetero atoms
- C07D291/02—Heterocyclic compounds containing rings having nitrogen, oxygen and sulfur atoms as the only ring hetero atoms not condensed with other rings
- C07D291/06—Six-membered rings
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/30—Artificial sweetening agents
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Claims (16)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201261657231P | 2012-06-08 | 2012-06-08 | |
US13/901,735 US9024016B2 (en) | 2012-06-08 | 2013-05-24 | Process for producing acesulfame potassium |
Publications (1)
Publication Number | Publication Date |
---|---|
FI3210978T3 true FI3210978T3 (en) | 2023-11-29 |
Family
ID=48577062
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FIEP17151405.2T FI3210978T3 (en) | 2012-06-08 | 2013-06-06 | Process for producing acesulfame potassium |
Country Status (14)
Country | Link |
---|---|
US (2) | US9024016B2 (en) |
EP (3) | EP2861569B1 (en) |
CN (2) | CN107056660A (en) |
DK (1) | DK3210978T3 (en) |
ES (2) | ES2618937T3 (en) |
FI (1) | FI3210978T3 (en) |
HR (1) | HRP20231424T1 (en) |
HU (1) | HUE064462T2 (en) |
LT (1) | LT3210978T (en) |
PL (2) | PL2861569T3 (en) |
PT (1) | PT3210978T (en) |
RS (1) | RS64912B1 (en) |
SI (1) | SI3210978T1 (en) |
WO (1) | WO2013182651A1 (en) |
Families Citing this family (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104292181B (en) * | 2014-09-27 | 2016-10-26 | 安徽金禾实业股份有限公司 | A kind of MVR system concentrates the method for acesulfame potassium mother solution |
CN105198778B (en) * | 2015-08-28 | 2017-07-04 | 安徽金禾实业股份有限公司 | A kind of acesulfame potassium synthesizing section acylation reaction technique |
CN106365952B (en) * | 2016-08-30 | 2018-10-26 | 安徽金禾实业股份有限公司 | Solvent self-heating separation method in a kind of synthesis of acesulfame potassium |
LT3319948T (en) | 2016-09-21 | 2021-10-11 | Celanese International Corporation | Acesulfame potassium compositions and processes for producing same |
US10029999B2 (en) * | 2016-09-21 | 2018-07-24 | Celanese International Corporation | Acesulfame potassium compositions and processes for producing same |
EP3317260B1 (en) | 2016-09-21 | 2019-10-30 | Celanese International Corporation | Acesulfame potassium compositions and processes for producing same |
PT3322695T (en) | 2016-09-21 | 2020-10-13 | Celanese Int Corp | Acesulfame potassium compositions and processes for producing same |
WO2019141369A1 (en) | 2018-01-18 | 2019-07-25 | Chemadvice Gmbh | Process for the preparation of an acesulfame with sulphuric acid processing |
CN112142688B (en) * | 2019-06-27 | 2023-10-20 | 南通醋酸化工股份有限公司 | Progressive neutralization reaction method in acesulfame potassium preparation |
CN113454071B (en) * | 2021-05-28 | 2023-03-17 | 安徽金禾实业股份有限公司 | Preparation method of acesulfame potassium |
WO2022246865A1 (en) * | 2021-05-28 | 2022-12-01 | 安徽金禾实业股份有限公司 | Preparation method for acesulfame potassium |
WO2022246870A1 (en) * | 2021-05-28 | 2022-12-01 | 安徽金禾实业股份有限公司 | Method for preparing acetoacetamide-n-sulfonic acid triethylamine salt |
CN113454073A (en) * | 2021-05-28 | 2021-09-28 | 安徽金禾实业股份有限公司 | Acetaminothioate composition |
WO2022246861A1 (en) * | 2021-05-28 | 2022-12-01 | 安徽金禾实业股份有限公司 | Preparation method for acesulfame potassium |
CN113527226A (en) * | 2021-07-05 | 2021-10-22 | 南通醋酸化工股份有限公司 | Method for controlling content of ACH in acid in process of preparing acesulfame potassium |
CN113563284A (en) * | 2021-07-26 | 2021-10-29 | 南通醋酸化工股份有限公司 | Preparation method of acesulfame potassium composition |
CN113563283A (en) * | 2021-07-26 | 2021-10-29 | 南通醋酸化工股份有限公司 | Preparation method of acesulfame potassium composition |
CN116322984A (en) * | 2021-12-31 | 2023-06-23 | 安徽金禾实业股份有限公司 | Method for preparing acesulfame potassium |
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CN100591222C (en) | 2007-09-12 | 2010-02-24 | 安徽金禾实业股份有限公司 | Concentrating method and device in acesulfame potassium production |
CN100564367C (en) | 2007-09-12 | 2009-12-02 | 安徽金禾实业股份有限公司 | Triethylamine recovery processing method during acesulfame potassium is produced |
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CN201921689U (en) | 2010-12-23 | 2011-08-10 | 安徽金禾实业股份有限公司 | Acesulfame condensation device |
CN102225333B (en) | 2011-05-06 | 2013-03-27 | 刘少光 | Denitration catalyst and preparation method thereof |
CN102866042B (en) | 2011-07-05 | 2014-09-10 | 内蒙古蒙牛乳业(集团)股份有限公司 | Pretreatment method of Acesulfame-K and detection method for potassium in Acesulfame-K |
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CN102359926B (en) | 2011-09-09 | 2013-01-02 | 苏州浩波科技股份有限公司 | Method for measuring and calculating acesulfame potassium agglomeration period |
CN103130743B (en) | 2012-11-11 | 2015-11-18 | 安徽金禾实业股份有限公司 | Acesulfame potassium cyclization continuous production method |
CN103018368B (en) | 2012-12-17 | 2014-08-27 | 苏州浩波科技股份有限公司 | Method for determining N-methylamino ammate in production of acesulfame |
CN103588728B (en) | 2013-11-01 | 2016-06-22 | 安徽金禾实业股份有限公司 | With direct crystallization production technology in acesulfame potassium |
CN103570592A (en) | 2013-11-01 | 2014-02-12 | 安徽金禾实业股份有限公司 | Acesulfame synthesis and acylation production process |
CN103613566B (en) | 2013-11-01 | 2016-03-23 | 安徽金禾实业股份有限公司 | Acesulfame potassium cyclization continuous production method |
CN103960558B (en) | 2014-05-22 | 2015-08-26 | 东南大学 | A kind of acesulfame potassium anticaking agent and using method thereof |
CN104193625B (en) | 2014-09-27 | 2015-12-09 | 安徽金禾实业股份有限公司 | The recovery method of catalyst of triethylamine in acesulfame potassium production |
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CN204320227U (en) | 2014-09-27 | 2015-05-13 | 安徽金禾实业股份有限公司 | Continous batching device in a kind of acesulfame potassium production |
CN104292181B (en) | 2014-09-27 | 2016-10-26 | 安徽金禾实业股份有限公司 | A kind of MVR system concentrates the method for acesulfame potassium mother solution |
CN104225956B (en) | 2014-09-27 | 2016-09-14 | 安徽金禾实业股份有限公司 | Forced circulation extracting process in acesulfame potassium production |
JP6676615B2 (en) | 2015-03-05 | 2020-04-08 | ライオン株式会社 | α-Sulfo fatty acid alkyl ester salt-containing liquid |
CN105198778B (en) | 2015-08-28 | 2017-07-04 | 安徽金禾实业股份有限公司 | A kind of acesulfame potassium synthesizing section acylation reaction technique |
CN105152446B (en) | 2015-09-25 | 2017-10-17 | 浙江奇彩环境科技股份有限公司 | A kind of acesulfame potassium produces the handling process of waste water |
CN206001439U (en) | 2016-07-29 | 2017-03-08 | 盐城捷康三氯蔗糖制造有限公司 | Sucralose produces waste heat energy-saving utilization device |
CN206001201U (en) | 2016-07-29 | 2017-03-08 | 盐城捷康三氯蔗糖制造有限公司 | A kind of sucralose process units inner high voltage main steam header channel fixing device |
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CN106262665A (en) | 2016-08-12 | 2017-01-04 | 安徽维多食品配料有限公司 | A kind of direct employing film processes the method for equivalent dialysis |
CN106349009B (en) | 2016-08-30 | 2018-11-06 | 安徽金禾实业股份有限公司 | Dichloromethane rectifying condensation method in a kind of synthesis of acesulfame potassium |
CN106349300B (en) | 2016-08-30 | 2019-02-26 | 安徽金禾实业股份有限公司 | Sucralose is esterified single solvent reaction method |
CN106267879B (en) | 2016-09-20 | 2018-06-19 | 苏州浩波科技股份有限公司 | A kind of continuous controllable acesulfame potassium crystallization apparatus |
CN106625198B (en) | 2016-12-26 | 2019-04-09 | 银川市恒益达机械有限公司 | Compound superhard honing stone containing zirconium oxide and preparation method thereof |
-
2013
- 2013-05-24 US US13/901,735 patent/US9024016B2/en not_active Ceased
- 2013-06-06 DK DK17151405.2T patent/DK3210978T3/en active
- 2013-06-06 EP EP13727188.8A patent/EP2861569B1/en not_active Revoked
- 2013-06-06 LT LTEP17151405.2T patent/LT3210978T/en unknown
- 2013-06-06 WO PCT/EP2013/061728 patent/WO2013182651A1/en active Application Filing
- 2013-06-06 CN CN201710388841.8A patent/CN107056660A/en active Pending
- 2013-06-06 EP EP17151405.2A patent/EP3210978B1/en active Active
- 2013-06-06 FI FIEP17151405.2T patent/FI3210978T3/en active
- 2013-06-06 ES ES13727188.8T patent/ES2618937T3/en active Active
- 2013-06-06 CN CN201380029410.2A patent/CN104411693B/en active Active
- 2013-06-06 SI SI201332067T patent/SI3210978T1/en unknown
- 2013-06-06 PT PT171514052T patent/PT3210978T/en unknown
- 2013-06-06 RS RS20231099A patent/RS64912B1/en unknown
- 2013-06-06 HU HUE17151405A patent/HUE064462T2/en unknown
- 2013-06-06 PL PL13727188T patent/PL2861569T3/en unknown
- 2013-06-06 EP EP23189507.9A patent/EP4248762A3/en active Pending
- 2013-06-06 ES ES17151405T patent/ES2964758T3/en active Active
- 2013-06-06 PL PL17151405.2T patent/PL3210978T3/en unknown
- 2013-06-06 HR HRP20231424TT patent/HRP20231424T1/en unknown
-
2017
- 2017-02-13 US US15/431,665 patent/USRE48464E1/en active Active
Also Published As
Publication number | Publication date |
---|---|
EP4248762A3 (en) | 2023-10-18 |
DK3210978T3 (en) | 2023-10-30 |
USRE48464E1 (en) | 2021-03-16 |
EP4248762A2 (en) | 2023-09-27 |
PL3210978T3 (en) | 2024-03-18 |
US20130331565A1 (en) | 2013-12-12 |
EP3210978B1 (en) | 2023-09-06 |
EP3210978A1 (en) | 2017-08-30 |
PL2861569T3 (en) | 2017-05-31 |
HUE064462T2 (en) | 2024-03-28 |
US9024016B2 (en) | 2015-05-05 |
CN104411693A (en) | 2015-03-11 |
EP2861569B1 (en) | 2017-02-08 |
LT3210978T (en) | 2024-01-10 |
ES2964758T3 (en) | 2024-04-09 |
EP2861569A1 (en) | 2015-04-22 |
RS64912B1 (en) | 2023-12-29 |
HRP20231424T1 (en) | 2024-03-01 |
WO2013182651A1 (en) | 2013-12-12 |
CN107056660A (en) | 2017-08-18 |
PT3210978T (en) | 2023-11-16 |
CN104411693B (en) | 2017-10-24 |
ES2618937T3 (en) | 2017-06-22 |
SI3210978T1 (en) | 2024-02-29 |
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