CN102359926B - Method for measuring and calculating acesulfame potassium agglomeration period - Google Patents

Method for measuring and calculating acesulfame potassium agglomeration period Download PDF

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CN102359926B
CN102359926B CN 201110266716 CN201110266716A CN102359926B CN 102359926 B CN102359926 B CN 102359926B CN 201110266716 CN201110266716 CN 201110266716 CN 201110266716 A CN201110266716 A CN 201110266716A CN 102359926 B CN102359926 B CN 102359926B
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acesulfame potassium
caking
leveling board
half cone
cycle
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CN102359926A (en
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夏秋霞
陈小萍
汪清玲
刘纪才
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Nantong Hongxin Chemical Co ltd
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SUZHOU HAOBO TECHNOLOGY HOLDINGS Co Ltd
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Abstract

The present invention discloses a method for measuring and calculating an acesulfame potassium agglomeration period. The method comprises the following steps: (1) preparing a measurement and calculation device for the acesulfame potassium agglomeration period, wherein the structure of the device comprises: a L-shaped baffle and a semi-conical funnel; (2) pouring 100 g of acesulfame potassium to the device, and timing until the acesulfame potassium is completely poured in the device, measuring the falling time t, substituting the t into the following formula: T1=-40.56*t+462.63, and calculating a first period T1; (3) measuring the vertical height H and the pavement length L of the acesulfame potassium, wherein of the vertical height and the pavement length are formed after the acesulfame potassium is completely leaked, calculating a H/L value, substituting the H/L value into the following formula: T2 =-752.58*H/L+544.41, and calculating a second period T2; (4) calculating the arithmetic mean of the T1 and the T2 to obtain the acesulfame potassium agglomeration period T. According to the present invention, the method of the present invention is simple; with the method, the acesulfame potassium agglomeration period can be accurately measured and calculated, such that the storage, the transport and the use can be effective arranged so as to substantially improve the work efficiency and reduce the labor cost.

Description

The measuring method in acesulfame potassium caking cycle
Technical field
The present invention relates to the acesulfame potassium measuring method in caking cycle.
Background technology
Acesulfame potassium is a kind of artificial synthesis edulcorant, and its production technology is uncomplicated, low price, performance are better than Aspartame, is considered to one of the most promising sweetener.But caking is an inevitable phenomenon in the acesulfame potassium storage process, and the time length in caking cycle badly influences the normal productive process of acesulfame potassium and its follow-up use.Acesulfame potassium needs some cycles from producing, store, transport to use to the user again, and the caking cycle of acesulfame potassium does not have special-purpose measuring method at present.Can't accurately calculate the caking cycle of acesulfame potassium, then can't arrange rationally and effectively production, storage, transportation and the use of acesulfame potassium, and the acesulfame potassium caking can make the cost of labor of packing, transportation, use greatly increase.
Summary of the invention
Technical matters to be solved by this invention provides a kind of measuring method that can accurately calculate the acesulfame potassium caking cycle in acesulfame potassium caking cycle.
For addressing the above problem, the technical solution used in the present invention is: the measuring method in acesulfame potassium caking cycle may further comprise the steps.
(1), make the acesulfame potassium measuring and calculating device in caking cycle, its structure is: the L-type baffle plate, the L-type baffle plate comprises: vertical plate and leveling board, an end of described leveling board is vertically fixed on the lower end of vertical plate; The upper end of described vertical plate is fixedly installed the half cone-shaped hopper walls, described half cone-shaped hopper walls and its vertical plate that surrounds partly form the half cone-shaped funnel, the top of described half cone-shaped funnel is provided with open top, the bottom of half cone-shaped funnel is provided with bottom opening, but the bottom opening place is provided with the bottom cover plate of folding, and the length of described leveling board and width can be guaranteed to be tiled on the leveling board after acesulfame potassium falls;
(2), first bottom cover plate is closed, and in the acesulfame potassium measuring and calculating device in caking cycle, pour the 100g acesulfame potassium into, then open bottom cover plate and begin timing, it is complete to have flowed timing to acesulfame potassium, record fall time t, with t substitution formula T1=-40.56t+462.63, calculate period 1 T1;
(3), measure acesulfame potassium after having leaked in vertical height H and the length L that tiles that vertical plate and leveling board form, calculate the value of H/L, with H/L substitution formula T2=-752.58H/L+544.41, calculate T2 second round;
(4), get the mean value of T1 and T2, get the caking cycle T of acesulfame potassium.
Further, the measuring method in aforesaid acesulfame potassium caking cycle, wherein, described bottom opening to the distance of leveling board is 0.81 ~ 0.85 times funnel overall height.
Further, the measuring method in aforesaid acesulfame potassium caking cycle, wherein, the surface of the inwall of described half cone-shaped funnel, vertical plate and leveling board is grinding and polishing all, and smoothness is for being not less than 8k.
Further, the measuring method in aforesaid acesulfame potassium caking cycle, wherein, the measurement number of times of described fall time t is no less than twice, and fall time t gets the arithmetic mean of all fall times.
Beneficial effect of the present invention: method is simple, can calculate exactly the cycle of acesulfame potassium caking, so just can effectively arrange according to the caking cycle that measuring and calculating draws to store, transport and use, and has greatly improved work efficiency, has reduced cost of labor.
Description of drawings
Fig. 1 is the synoptic diagram of the measuring and calculating device in acesulfame potassium caking cycle in the acesulfame potassium of the present invention measuring method in caking cycle.
Fig. 2 is the schematic top plan view of Fig. 1.
Embodiment
The present invention is described in further detail below in conjunction with drawings and the specific embodiments.
The measuring method in acesulfame potassium caking cycle, may further comprise the steps (one), as shown in Figure 1 and Figure 2, make the acesulfame potassium measuring and calculating device in caking cycle, its structure is: the L-type baffle plate, the L-type baffle plate comprises: vertical plate 1 and leveling board 2, and an end of described leveling board 2 is vertically fixed on the lower end of vertical plate 1; Wherein the upper end of vertical plate 1 is fixedly installed half cone-shaped hopper walls 3, described half cone-shaped hopper walls 3 forms the half cone-shaped funnel with its vertical plate that surrounds 1 part, the top of described half cone-shaped funnel is provided with open top 4, the bottom of half cone-shaped funnel is provided with bottom opening 5, but bottom opening 5 places are provided with the bottom cover plate 51 of folding, the length of described leveling board 2 and width can be guaranteed to be tiled on the leveling board 2 after acesulfame potassium falls, all device materials are selected stainless steel in the present embodiment, the inwall of described half cone-shaped funnel, the surface of vertical plate 1 and leveling board 2 is grinding and polishing all, and smoothness is 8k.As shown in Figure 1 and Figure 2, the radius R 1 of open top 4 is 112mm ± 2mm, the radius R 2 of bottom opening 5 is 12mm ± 0.2mm, half cone-shaped funnel height H 1 is 100mm ± 2mm, bottom opening 5 to the distance B of the upper surface of leveling board 2 is 120mm ± 2mm, the length L 1 of leveling board 2 is 250mm ± 2mm, and B1 is 300mm ± 2mm.
Adopt the embodiment 1 of the measuring and calculating device in above-mentioned acesulfame potassium caking cycle.
Take by weighing the acesulfame potassium 100.0g of 20~30 order numbers, first the bottom cover plate 51 at bottom opening place 5 is closed, then pour into the half cone-shaped funnel from open top 4, open bottom cover plate 51 and begin timing, it is complete that acesulfame potassium has flowed timing in the half cone-shaped funnel, repeats twice, average 3.7s consuming time, substitution formula T1=-40.56t+462.63, calculating 1 round numbers of the first caking cycle T is 312 days; Recording simultaneously acesulfame potassium tiling length L is 9.7cm, and height H is 3.1cm, and ratio calculated H/L is 0.3096, substitution formula T2=-752.58H/L+544.41, and then corresponding the second caking cycle T 2 round numbers are 311 days.Then this caking cycle T is got the arithmetic mean of T1 and T2, and round numbers is 311 days.
Adopt the embodiment 2 of the measuring and calculating device in above-mentioned acesulfame potassium caking cycle.
Take by weighing the acesulfame potassium 100.0g of 40~80 order numbers, first the bottom cover plate 51 at bottom opening place 5 is closed, then pour into the half cone-shaped funnel from open top 4, open bottom cover plate 51 and begin timing, it is complete that acesulfame potassium has flowed timing in the half cone-shaped funnel, repeats twice, average 5.8s consuming time, substitution formula T1=-40.56t+462.63, calculating 1 round numbers of the first caking cycle T is 227 days; Recording simultaneously the tiling length L is 8.4cm, and highly piling up H is 3.5cm, and ratio calculated H/L is 0.4167, substitution formula T2=-752.58H/L+544.41, and then corresponding the second caking cycle T 2 round numbers are 230 days.Then this caking cycle T is got the arithmetic mean 228 days of T1 and T2.
Beneficial effect of the present invention: method is simple, can calculate exactly the cycle of acesulfame potassium caking, so just can effectively arrange according to the caking cycle that measuring and calculating draws to store, transport and use, and has greatly improved work efficiency, has reduced cost of labor.

Claims (3)

1. the measuring method in acesulfame potassium caking cycle is characterized in that: may further comprise the steps:
(1), make the acesulfame potassium measuring and calculating device in caking cycle, its structure is: the L-type baffle plate, the L-type baffle plate comprises: vertical plate and leveling board, an end of described leveling board is vertically fixed on the lower end of vertical plate; The upper end of described vertical plate is fixedly installed the half cone-shaped hopper walls, described half cone-shaped hopper walls and its vertical plate that surrounds partly form the half cone-shaped funnel, the top of described half cone-shaped funnel is provided with open top, the bottom of half cone-shaped funnel is provided with bottom opening, but the bottom opening place is provided with the bottom cover plate of folding, and the length of described leveling board and width can be guaranteed to be tiled on the leveling board after acesulfame potassium falls; The surface of the inwall of described half cone-shaped funnel, vertical plate and leveling board is all smooth; The open-topped radius R 1 of half cone-shaped funnel is 112mm ± 2mm, the radius R 2 of bottom opening is 12mm ± 0.2mm, half cone-shaped funnel height H 1 is 100mm ± 2mm, bottom opening to the distance B of the upper surface of leveling board is 120mm ± 2mm, the length L 1 of leveling board is 250mm ± 2mm, and the width B 1 of leveling board is 300mm ± 2mm;
(2), first bottom cover plate is closed, and pour the 100g acesulfame potassium in the acesulfame potassium measuring and calculating device in caking cycle, then open bottom cover plate and begin timing, it is complete to have flowed timing to acesulfame potassium, records fall time t second, with t substitution formula T1=
-40.56t+462.63 calculates period 1 T1 days;
(3), measure vertical height H that the acesulfame potassium after having leaked forms at vertical plate and leveling board centimetre and the length L centimetre of tiling, calculate the value of H/L, with H/L substitution formula T2=-752.58H/L+544.41, calculate T2 days second round;
(4), get the arithmetic mean of T1 and T2, get the caking cycle T sky of acesulfame potassium.
2. the measuring method in acesulfame potassium according to claim 1 caking cycle, it is characterized in that: the surface of the inwall of described half cone-shaped funnel, vertical plate and leveling board is grinding and polishing all, and smoothness is for being not less than 8k.
3. according to sharp prescription 1 or the measuring method in 2 described acesulfame potassium caking cycles, it is characterized in that: the measurement number of times of described fall time t is no less than twice, and fall time t gets the arithmetic mean of all fall times.
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US9024016B2 (en) 2012-06-08 2015-05-05 Nutrinova Nutrition Specialists & Food Ingredients GmbH Process for producing acesulfame potassium
SI3319948T1 (en) 2016-09-21 2021-11-30 Celanese International Corporation Acesulfame potassium compositions and processes for producing same
PT3317260T (en) 2016-09-21 2020-02-06 Celanese Int Corp Acesulfame potassium compositions and processes for producing same
CN108884064A (en) 2016-09-21 2018-11-23 国际人造丝公司 Acesulfame-K composition and its production method
EP3753930A1 (en) 2016-09-21 2020-12-23 Celanese International Corporation Acesulfame potassium compositions and processes for producing same

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WO1996020608A1 (en) * 1994-12-29 1996-07-11 Wm. Wrigley Jr. Company Chewing gum containing encapsulated combinations of aspartame and acesulfame k
JP3643922B2 (en) * 1998-05-08 2005-04-27 味の素株式会社 Sweetener composition
JP4255972B2 (en) * 2004-06-11 2009-04-22 日本電信電話株式会社 Crystal manufacturing method and apparatus
CN1308668C (en) * 2005-01-18 2007-04-04 武汉理工大学 Tester and testing method for high-sensitivity cement thick liquid flowability
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Denomination of invention: Method for measuring and calculating acesulfame potassium agglomeration period

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