CN103960558B - A kind of acesulfame potassium anticaking agent and using method thereof - Google Patents
A kind of acesulfame potassium anticaking agent and using method thereof Download PDFInfo
- Publication number
- CN103960558B CN103960558B CN201410220408.XA CN201410220408A CN103960558B CN 103960558 B CN103960558 B CN 103960558B CN 201410220408 A CN201410220408 A CN 201410220408A CN 103960558 B CN103960558 B CN 103960558B
- Authority
- CN
- China
- Prior art keywords
- acesulfame potassium
- sodium polyacrylate
- surfactant
- dimethicone
- caking agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- WBZFUFAFFUEMEI-UHFFFAOYSA-M Acesulfame k Chemical compound [K+].CC1=CC(=O)[N-]S(=O)(=O)O1 WBZFUFAFFUEMEI-UHFFFAOYSA-M 0.000 title claims abstract description 42
- 229960004998 acesulfame potassium Drugs 0.000 title claims abstract description 42
- 235000010358 acesulfame potassium Nutrition 0.000 title claims abstract description 42
- 239000000619 acesulfame-K Substances 0.000 title claims abstract description 42
- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 31
- 238000000034 method Methods 0.000 title claims abstract description 12
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 claims abstract description 23
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 claims abstract description 23
- 239000000243 solution Substances 0.000 claims abstract description 20
- 229940008099 dimethicone Drugs 0.000 claims abstract description 15
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 15
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims abstract description 15
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 15
- 239000004094 surface-active agent Substances 0.000 claims abstract description 13
- 238000003756 stirring Methods 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 3
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 239000003945 anionic surfactant Substances 0.000 claims description 4
- 239000007864 aqueous solution Substances 0.000 claims description 3
- CODAYFPFZXWNLD-UHFFFAOYSA-N 2-hydroxypropanoyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC(=O)C(C)O CODAYFPFZXWNLD-UHFFFAOYSA-N 0.000 claims description 2
- 229920001219 Polysorbate 40 Polymers 0.000 claims description 2
- 229920001214 Polysorbate 60 Polymers 0.000 claims description 2
- 229920000223 polyglycerol Polymers 0.000 claims description 2
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 2
- 235000010483 polyoxyethylene sorbitan monopalmitate Nutrition 0.000 claims description 2
- 239000000249 polyoxyethylene sorbitan monopalmitate Substances 0.000 claims description 2
- 235000010989 polyoxyethylene sorbitan monostearate Nutrition 0.000 claims description 2
- 239000001818 polyoxyethylene sorbitan monostearate Substances 0.000 claims description 2
- 229940101027 polysorbate 40 Drugs 0.000 claims description 2
- 229940113124 polysorbate 60 Drugs 0.000 claims description 2
- 229920000053 polysorbate 80 Polymers 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 11
- 235000013373 food additive Nutrition 0.000 abstract description 3
- 239000002778 food additive Substances 0.000 abstract description 3
- 238000010790 dilution Methods 0.000 description 9
- 239000012895 dilution Substances 0.000 description 9
- 235000003599 food sweetener Nutrition 0.000 description 3
- 239000003765 sweetening agent Substances 0.000 description 3
- 238000005054 agglomeration Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- PNWSHHILERSSLF-UHFFFAOYSA-N 4-methylbenzene-1,3-dicarboxylic acid Chemical compound CC1=CC=C(C(O)=O)C=C1C(O)=O PNWSHHILERSSLF-UHFFFAOYSA-N 0.000 description 1
- 108010011485 Aspartame Proteins 0.000 description 1
- 208000008589 Obesity Diseases 0.000 description 1
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000605 aspartame Substances 0.000 description 1
- 235000010357 aspartame Nutrition 0.000 description 1
- IAOZJIPTCAWIRG-QWRGUYRKSA-N aspartame Chemical compound OC(=O)C[C@H](N)C(=O)N[C@H](C(=O)OC)CC1=CC=CC=C1 IAOZJIPTCAWIRG-QWRGUYRKSA-N 0.000 description 1
- 229960003438 aspartame Drugs 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000000967 suction filtration Methods 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/30—Artificial sweetening agents
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/03—Organic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention is specifically related to a kind of acesulfame potassium anti-caking agent and using method thereof, belongs to food additives field, and it is by comprising sodium polyacrylate solution, and surfactant and dimethicone configuration form; Shared by each raw material, mass percent is: sodium polyacrylate solution 20% ~ 60%, surfactant 30% ~ 70%, dimethicone 10% ~ 20%; Its using method is: sodium polyacrylate solution, surfactant, dimethicone successively join in suitable quantity of water by example in mass ratio, can obtain acesulfame potassium anti-caking agent after stirring and dissolving.The present invention is when applying, and its addition is 0.1% ~ 0.5% of acesulfame potassium quality.
Description
Technical field
The invention belongs to food additives field, be specifically related to a kind of acesulfame potassium anticaking agent and using method thereof.
Background technology
Acesulfame potassium (AcesulfamePotassium) chemical name: 6-methyl isophthalic acid, 2,3-oxygen oxazines-4-(3H)-one-2,2-dioxy sylvite, molecular formula: C
4h
4kNO
4s, acesulfame potassium is a kind of food additives, is chemicals, is similar to asccharin, soluble in water, increase food sweet taste, nonnutritive, mouthfeel is good, empty calory, having not metabolism in human body, do not absorb (being the elderly, adiposis patient, sweetener that diabetic is desirable), to heat and the feature such as absolute acid stability is good, is forth generation synthetic sweetener on our times.The production technology of acesulfame potassium is uncomplicated, low price, performance are better than Aspartame, is considered to one of the most promising sweetener.Structural formula is as follows:
Acesulfame potassium is white crystalline powder, store, transport process in be subject to temperature, humidity, pressure change time, plane of crystal easily produces the situation of the dissolution-recrystallization of dissolution-crystallization-more repeatedly, make brilliant bridge phenomenon occurs between crystal, thus cause caking, be difficult to pulverize, bring very large inconvenience to use.At present, the anti-caking of acesulfame potassium mainly prevents by improving stock's condition and packing and alleviates caking phenomenon, adopt in this way, can prevent or alleviate the caking phenomenon of acesulfame potassium in a short time, but be above a month acesulfame potassium and just there will be comparatively serious caking phenomenon.
Summary of the invention
Technical problem: in order to solve the caking phenomenon of acesulfame potassium, the invention provides a kind of acesulfame potassium anti-caking agent, can well prevent the generation of acesulfame potassium caking phenomenon.The present invention provides a kind of and processes the acesulfame potassium anti-caking agent simple, use cost is low, agglomeration preventing performance is good and using method thereof.
Technical scheme: a kind of acesulfame potassium anticaking agent of the present invention is by sodium polyacrylate solution soon, surfactant and dimethicone; Shared by each raw material, mass percent is:
Sodium polyacrylate solution 20% ~ 60%,
Surfactant 30% ~ 70%,
Dimethicone 10% ~ 20%.
In described sodium polyacrylate solution, the mass fraction of Sodium Polyacrylate is 30% ~ 70%.
In described sodium polyacrylate solution, the molecular weight of Sodium Polyacrylate is 4500000 ~ 7000000.
Described surfactant is one or both the mixture in anion surfactant and non-ionic surface active agent.
Described anion surfactant is one or both the mixture in lauryl sodium sulfate, enuatrol or stearoyl lactate.
Described non-ionic surface active agent is the mixture of one or more in polysorbas20, polysorbate40, polysorbate60, Tween 80, polyglycereol monolaurate or polyglycerol monooleate.
The using method of acesulfame potassium anti-caking agent of the present invention is: described anti-caking agent is diluted to the solution that mass fraction is 1% ~ 10%, evenly joins in the acesulfame potassium aqueous solution, and the addition of anti-caking agent is 0.1% ~ 0.5% of acesulfame potassium quality.And stir.
Beneficial effect: the acesulfame potassium anti-caking agent prepared by this invention effectively solves the caking phenomenon that acesulfame potassium occurs in long term storage, transportation.There is provided a kind of and process the acesulfame potassium anti-caking agent simple, use cost is low, agglomeration preventing performance is good and using method thereof.
Detailed description of the invention
Explain the present invention further with embodiment below, but the present invention is not limited to these embodiments.
One, anticaking agent is prepared:
Embodiment 1:
Take sodium polyacrylate solution 1g, lauryl sodium sulfate 1g respectively, dimethicone 0.5g is placed in beaker, add 50ml water and stir 10min, obtain acesulfame potassium anticaking agent dilution I.
Embodiment 2:
Take sodium polyacrylate solution 1g, lauryl sodium sulfate 2g respectively, dimethicone 0.5g is placed in beaker, add 50ml water and stir 10min, obtain acesulfame potassium anticaking agent dilution II.
Embodiment 3:
Take sodium polyacrylate solution 1g, lauryl sodium sulfate 3g respectively, dimethicone 0.5g is placed in beaker, add 50ml water and stir 10min, obtain acesulfame potassium anticaking agent dilution III.
Embodiment 4:
Take sodium polyacrylate solution 1g, polysorbas20 1g respectively, dimethicone 0.5g is placed in beaker, add 50ml water and stir 10min, obtaining acesulfame potassium anticaking agent dilution IV.
Embodiment 5:
Take sodium polyacrylate solution 1g, polysorbas20 2g respectively, dimethicone 0.5g is placed in beaker, add 50ml water and stir 10min, obtaining acesulfame potassium anticaking agent dilution V.
Embodiment 6:
Take sodium polyacrylate solution 1g, polysorbas20 3g respectively, dimethicone 0.5g is placed in beaker, add 50ml water and stir 10min, obtaining acesulfame potassium anticaking agent dilution VI.
Embodiment 7:
Take sodium polyacrylate solution 2g, lauryl sodium sulfate 2g respectively, dimethicone 0.5g is placed in beaker, add 50ml water and stir 10min, obtain acesulfame potassium anticaking agent dilution VII.
Embodiment 8:
Take sodium polyacrylate solution 2g, polysorbas20 2g respectively, dimethicone 0.5g is placed in beaker, add 50ml water and stir 10min, obtaining acesulfame potassium anticaking agent dilution VIII.
Two, blocking test:
Added to by the various embodiments described above gained anticaking agent dilution in the acesulfame potassium aqueous solution of 1000g boiling respectively, stir min, after leaving standstill 24h, acesulfame potassium crystallizes out from water.Carry out suction filtration, drying, pack deposit under being placed in the pressure of 1KPa after three months and observe caking phenomenon subsequently.Get to deposit after three months the acesulfame potassium not adding anticaking agent is also placed in the pressure of 1KPa as blank under simultaneously and observe caking phenomenon, last result is that the acesulfame potassium sample that with the addition of anti-caking agent does not lump, and the acesulfame potassium sample caking phenomenon not adding anti-caking agent is comparatively serious.
Claims (2)
1. an acesulfame potassium anti-caking agent, is characterized in that this anti-caking agent comprises sodium polyacrylate solution, surfactant and dimethicone; Shared by each raw material, mass percent is:
Sodium polyacrylate solution 20% ~ 60%,
Surfactant 30% ~ 70%,
Dimethicone 10% ~ 20%;
Wherein:
In described sodium polyacrylate solution, the mass fraction of Sodium Polyacrylate is 30% ~ 70%;
In described sodium polyacrylate solution, the molecular weight of Sodium Polyacrylate is 4500000 ~ 7000000;
Described surfactant is one or both the mixture in anion surfactant and non-ionic surface active agent;
Described anion surfactant is one or both the mixture in lauryl sodium sulfate, enuatrol or stearoyl lactate; Described non-ionic surface active agent is the mixture of one or more in polysorbas20, polysorbate40, polysorbate60, Tween 80, polyglycereol monolaurate or polyglycerol monooleate.
2. the using method of an acesulfame potassium anti-caking agent as claimed in claim 1, described anti-caking agent is it is characterized in that to be diluted to the solution that mass fraction is 1% ~ 10%, evenly join in the acesulfame potassium aqueous solution, the addition of anti-caking agent is 0.1% ~ 0.5% of acesulfame potassium quality, and stirs.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410220408.XA CN103960558B (en) | 2014-05-22 | 2014-05-22 | A kind of acesulfame potassium anticaking agent and using method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410220408.XA CN103960558B (en) | 2014-05-22 | 2014-05-22 | A kind of acesulfame potassium anticaking agent and using method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103960558A CN103960558A (en) | 2014-08-06 |
| CN103960558B true CN103960558B (en) | 2015-08-26 |
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| CN201410220408.XA Expired - Fee Related CN103960558B (en) | 2014-05-22 | 2014-05-22 | A kind of acesulfame potassium anticaking agent and using method thereof |
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9024016B2 (en) | 2012-06-08 | 2015-05-05 | Nutrinova Nutrition Specialists & Food Ingredients GmbH | Process for producing acesulfame potassium |
| SI3319948T1 (en) | 2016-09-21 | 2021-11-30 | Celanese International Corporation | Acesulfame potassium compositions and processes for producing same |
| PT3317260T (en) | 2016-09-21 | 2020-02-06 | Celanese Int Corp | Acesulfame potassium compositions and processes for producing same |
| CN108884064A (en) | 2016-09-21 | 2018-11-23 | 国际人造丝公司 | Acesulfame-K composition and its production method |
| EP3753930A1 (en) | 2016-09-21 | 2020-12-23 | Celanese International Corporation | Acesulfame potassium compositions and processes for producing same |
| CN109111278B (en) * | 2017-06-23 | 2021-06-22 | 深圳市芭田生态工程股份有限公司 | Anti-hardening oil, preparation method thereof and anti-hardening fertilizer |
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| CN101361479A (en) * | 2008-09-19 | 2009-02-11 | 广州市顾地丰农药有限公司 | Water dispersion granule of methylamino avermectin benzoate and preparation method thereof |
| JP5339980B2 (en) * | 2009-03-23 | 2013-11-13 | 富士フイルム株式会社 | Dispersion composition and method for producing dispersion composition |
| CN103057005B (en) * | 2012-12-20 | 2015-04-08 | 洛阳惠尔纳米科技有限公司 | Stearic acid water-based dispersion and preparation method thereof |
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| CN103960558A (en) | 2014-08-06 |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150826 Termination date: 20180522 |