ES8800662A1 - Metodo de preparar derivados de sulfato de hidroxilamonio - Google Patents
Metodo de preparar derivados de sulfato de hidroxilamonioInfo
- Publication number
- ES8800662A1 ES8800662A1 ES551466A ES551466A ES8800662A1 ES 8800662 A1 ES8800662 A1 ES 8800662A1 ES 551466 A ES551466 A ES 551466A ES 551466 A ES551466 A ES 551466A ES 8800662 A1 ES8800662 A1 ES 8800662A1
- Authority
- ES
- Spain
- Prior art keywords
- hydroxylammonium
- hydroxylamine solutions
- sulfate
- alcoholic hydroxylamine
- alcoholic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
- C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1409—Preparation
- C01B21/1445—Preparation of hydoxylamine from its salts
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1409—Preparation
- C01B21/1454—Preparation of hydroxylamine salts by processes not covered by one or more of groups C01B21/1418 - C01B21/1445, e.g. by conversion of one salt into another
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
METODO PARA PREPARAR DERIVADOS DE SULFATO DE HIDROXILAMONIO. COMPRENDE: A) HACER REACCIONAR UNA DISOLUCION ALCOHOLICA DE UNA BASE O UNA SAL ORGANICA BASICA ELEGIDA DEL GRUPO FORMADO POR HIDROXIDO SODICO, POTASICO, LITICO O AMONICO, EN AUSENCIA SUSTANCIAL DE ADICION DE AGUA A UNA TEMPERATURA NO SUPERIOR A UNOS 30JC CON UN SULFATO SOLIDO DE METAL ALCALINO O AMONICO CORRESPONDIENTE A LA BASE O A LA SAL BASICA; B) SEPARAR LA FASE SOLIDA QUE COMPRENDE SAL SULFATO DE UNA FASE LIQUIDA QUE CONTIENE UNA SAL ORGANICA DE HIDROXILAMONIO CORRESPONDIENTE A LA SAL ORGANICA BASICA O AL ACIDO ORGANICO, ESTANDO LA FASE LIQUIDA SUSTANCIALMENTE LIBRE DE SULFATO. SE UTILIZA COMO REACTIVO EN LA SINTESIS DE PRODUCTOS FARMACEUTICOS.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US06/437,920 US4551323A (en) | 1982-11-01 | 1982-11-01 | Preparation of alcoholic hydroxylamine solution from hydroxylammonium sulfate |
US06/534,291 US4507248A (en) | 1982-11-01 | 1983-09-23 | Preparation from hydroxylammonium sulfate of oximes and hydroxamic acids via alcoholic hydroxylamine solution |
US06/534,292 US4551324A (en) | 1982-11-01 | 1983-09-23 | Preparation from hydroxylammonium sulfate of other hydroxylammonium salts via alcoholic hydroxylamine |
Publications (2)
Publication Number | Publication Date |
---|---|
ES8800662A1 true ES8800662A1 (es) | 1987-12-01 |
ES551466A0 ES551466A0 (es) | 1987-12-01 |
Family
ID=27411964
Family Applications (3)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES526734A Expired ES8607222A1 (es) | 1982-11-01 | 1983-10-25 | Procedimiento de preparar derivados de sulfato de hidroxilamonio |
ES551464A Expired ES8703411A1 (es) | 1982-11-01 | 1986-01-16 | Procedimiento de producir derivados de sulfato de hidroxilamonio |
ES551466A Expired ES8800662A1 (es) | 1982-11-01 | 1986-01-16 | Metodo de preparar derivados de sulfato de hidroxilamonio |
Family Applications Before (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES526734A Expired ES8607222A1 (es) | 1982-11-01 | 1983-10-25 | Procedimiento de preparar derivados de sulfato de hidroxilamonio |
ES551464A Expired ES8703411A1 (es) | 1982-11-01 | 1986-01-16 | Procedimiento de producir derivados de sulfato de hidroxilamonio |
Country Status (5)
Country | Link |
---|---|
EP (1) | EP0108294B1 (es) |
AU (1) | AU559815B2 (es) |
CA (1) | CA1204914A (es) |
DE (1) | DE3382155D1 (es) |
ES (3) | ES8607222A1 (es) |
Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3601216A1 (de) * | 1986-01-17 | 1987-07-23 | Basf Ag | Verfahren zur herstellung von reinen hydroxylammoniumsalzen von fettsaeuren mit 1 bis 4 kohlenstoffatomen |
DE3601803A1 (de) * | 1986-01-22 | 1987-07-23 | Basf Ag | Verfahren zur herstellung von waessrigen loesungen von freiem hydroxylamin |
WO1991018867A1 (en) * | 1990-06-06 | 1991-12-12 | Eastman Kodak Company | Process for the preparation of ketoximes |
US5213784A (en) * | 1992-06-18 | 1993-05-25 | Olin Corporation | Process for the production of high purity hydroxylammonium nitrate |
US5266290A (en) * | 1992-07-10 | 1993-11-30 | Thiokol Corporation | Process for making high purity hydroxylammonium nitrate |
DE19725851A1 (de) * | 1997-06-18 | 1998-12-24 | Basf Ag | Verfahren zur Herstellung hochreiner, wässriger Hydroxylaminlösungen |
DE19733681A1 (de) | 1997-08-04 | 1999-02-11 | Basf Ag | Verfahren zur Herstellung einer wäßrigen Lösung von freiem Hydroxylamin |
JO2258B1 (en) * | 1999-05-11 | 2004-10-07 | اف . هوفمان لاروش ايه جي | Method for preparing hydroxamic acids |
WO2017204935A1 (en) | 2016-05-26 | 2017-11-30 | Exxonmobil Chemical Patents Inc. | Production of cyclic imides suitable for oxidation catalysis |
WO2017204936A1 (en) | 2016-05-26 | 2017-11-30 | Exxonmobil Chemical Patents Inc. | Production of cyclic imides suitable for oxidation catalysis |
WO2018075176A1 (en) | 2016-10-18 | 2018-04-26 | Exxonmobil Chemical Patents Inc. | Cyclic imide slurry compositions |
CN110465328B (zh) * | 2018-05-09 | 2022-07-12 | 万华化学集团股份有限公司 | 酮的肟化方法 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2483252A (en) * | 1945-04-20 | 1949-09-27 | Commercial Solvents Corp | Method for preparing hydroxylammonium salts of organic acids |
DE1247284B (de) * | 1965-10-20 | 1967-08-17 | Basf Ag | Verfahren zur Herstellung von reinem Hydroxylamin oder von Loesungen des Hydroxylamins in Alkoholen |
US3420621A (en) * | 1966-08-17 | 1969-01-07 | Us Navy | Process for producing hydroxylammonium perchlorate |
-
1983
- 1983-10-17 EP EP19830110342 patent/EP0108294B1/en not_active Expired
- 1983-10-17 DE DE8383110342T patent/DE3382155D1/de not_active Expired - Lifetime
- 1983-10-25 ES ES526734A patent/ES8607222A1/es not_active Expired
- 1983-10-28 AU AU20807/83A patent/AU559815B2/en not_active Ceased
- 1983-10-28 CA CA000439937A patent/CA1204914A/en not_active Expired
-
1986
- 1986-01-16 ES ES551464A patent/ES8703411A1/es not_active Expired
- 1986-01-16 ES ES551466A patent/ES8800662A1/es not_active Expired
Also Published As
Publication number | Publication date |
---|---|
ES8607222A1 (es) | 1986-06-01 |
ES526734A0 (es) | 1986-06-01 |
EP0108294B1 (en) | 1991-02-06 |
ES8703411A1 (es) | 1987-03-01 |
EP0108294A3 (en) | 1986-08-13 |
ES551464A0 (es) | 1987-03-01 |
EP0108294A2 (en) | 1984-05-16 |
AU559815B2 (en) | 1987-03-19 |
AU2080783A (en) | 1984-05-10 |
DE3382155D1 (de) | 1991-03-14 |
ES551466A0 (es) | 1987-12-01 |
CA1204914A (en) | 1986-05-27 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FD1A | Patent lapsed |
Effective date: 19970303 |