ES8604396A1 - Procedimiento para la preparacion de esteres del acido-14,15-dihidro-14 b-hidroxi-(3x,16x)-eburnamenina-14-carboxilico - Google Patents

Procedimiento para la preparacion de esteres del acido-14,15-dihidro-14 b-hidroxi-(3x,16x)-eburnamenina-14-carboxilico

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Publication number
ES8604396A1
ES8604396A1 ES539022A ES539022A ES8604396A1 ES 8604396 A1 ES8604396 A1 ES 8604396A1 ES 539022 A ES539022 A ES 539022A ES 539022 A ES539022 A ES 539022A ES 8604396 A1 ES8604396 A1 ES 8604396A1
Authority
ES
Spain
Prior art keywords
eburnamenine
carboxylic acid
acid ester
hydroxy
hydro hydroxy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES539022A
Other languages
English (en)
Other versions
ES539022A0 (es
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Covex SA
Original Assignee
Covex SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Covex SA filed Critical Covex SA
Priority to ES539022A priority Critical patent/ES8604396A1/es
Publication of ES8604396A1 publication Critical patent/ES8604396A1/es
Publication of ES539022A0 publication Critical patent/ES539022A0/es
Expired legal-status Critical Current

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

PROCEDIMIENTO PARA LA PREPARACION DE ESTERES DEL ACIDO 14,15-DIHIDRO-14B-HIDROXI-(3A, 16A)-EBURNAMENINA-14-CARBOXILICO. COMPRENDE: A) HACER REACCIONAR LA SAL POTASICA DEL ACIDO 14,15-DIHIDRO-14B-HIDROXI-(3A, 16A)-EBURNAMENINA-14-CARBOXILICO CON UN BROMURO DE ALQUILO, MEDIANTE CATALISIS EN TRANSFERENCIA DE FASE, EN PRESENCIA DE UN CATALIZADOR COMO BROMURO DE TETRABUTILAMONIO, EN UNA MEZCLA DE AGUA, BENCENO Y/O TOLUENO, A UNA TEMPERATURA ENTRE 20JC Y LA DE EBULLICION DEL DISOLVENTE Y DURANTE 3 H A 12 HORAS Y B) CONCENTRAR LA FASE ORGANICA Y RECRISTALIZARLA CON UN DISOLVENTE ORGANICO PARA OBTENER EL ESTER DEL ACIDO 14,15-DIHIDRO-14B-HIDROXI-(3A, 16A)EBURNAMENINA-14-CARBOXILICO DE FORMULA (I). SIENDO: R4 ALQUILO, UN RADICAL METILO, ETILO Y OTROS.
ES539022A 1984-12-24 1984-12-24 Procedimiento para la preparacion de esteres del acido-14,15-dihidro-14 b-hidroxi-(3x,16x)-eburnamenina-14-carboxilico Expired ES8604396A1 (es)

Priority Applications (1)

Application Number Priority Date Filing Date Title
ES539022A ES8604396A1 (es) 1984-12-24 1984-12-24 Procedimiento para la preparacion de esteres del acido-14,15-dihidro-14 b-hidroxi-(3x,16x)-eburnamenina-14-carboxilico

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ES539022A ES8604396A1 (es) 1984-12-24 1984-12-24 Procedimiento para la preparacion de esteres del acido-14,15-dihidro-14 b-hidroxi-(3x,16x)-eburnamenina-14-carboxilico

Publications (2)

Publication Number Publication Date
ES8604396A1 true ES8604396A1 (es) 1986-02-01
ES539022A0 ES539022A0 (es) 1986-02-01

Family

ID=8488402

Family Applications (1)

Application Number Title Priority Date Filing Date
ES539022A Expired ES8604396A1 (es) 1984-12-24 1984-12-24 Procedimiento para la preparacion de esteres del acido-14,15-dihidro-14 b-hidroxi-(3x,16x)-eburnamenina-14-carboxilico

Country Status (1)

Country Link
ES (1) ES8604396A1 (es)

Also Published As

Publication number Publication date
ES539022A0 (es) 1986-02-01

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