ES8406376A1 - Procedimiento para la purificacion de acido fosforico bruto de procedimiento en humedo - Google Patents

Procedimiento para la purificacion de acido fosforico bruto de procedimiento en humedo

Info

Publication number
ES8406376A1
ES8406376A1 ES527210A ES527210A ES8406376A1 ES 8406376 A1 ES8406376 A1 ES 8406376A1 ES 527210 A ES527210 A ES 527210A ES 527210 A ES527210 A ES 527210A ES 8406376 A1 ES8406376 A1 ES 8406376A1
Authority
ES
Spain
Prior art keywords
phosphoric acid
solution
wet
organic
raffinate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES527210A
Other languages
English (en)
Other versions
ES527210A0 (es
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst AG filed Critical Hoechst AG
Publication of ES527210A0 publication Critical patent/ES527210A0/es
Publication of ES8406376A1 publication Critical patent/ES8406376A1/es
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/46—Preparation involving solvent-solvent extraction
    • C01B25/461—Preparation involving solvent-solvent extraction the phosphoric acid present in the medium obtained after reaction being first extracted from the liquid phase formed or separated then re-extracted as free acid by using water or as a phosphate by using a basic compound
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/46—Preparation involving solvent-solvent extraction
    • C01B25/461—Preparation involving solvent-solvent extraction the phosphoric acid present in the medium obtained after reaction being first extracted from the liquid phase formed or separated then re-extracted as free acid by using water or as a phosphate by using a basic compound
    • C01B25/462—Preparation involving solvent-solvent extraction the phosphoric acid present in the medium obtained after reaction being first extracted from the liquid phase formed or separated then re-extracted as free acid by using water or as a phosphate by using a basic compound the extracting agent being alcohol or a mixture of alcohols

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Removal Of Specific Substances (AREA)
  • Fuel Cell (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Chemical Treatment Of Metals (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Catalysts (AREA)

Abstract

PROCEDIMIENTO PARA LA PURIFICACION DE ACIDO FOSFORICO BRUTO DE PROCEDIMIENTO EN HUMEDO.CONSISTE EN: A) MEZCLAR EL PRODUCTO DE PARTIDA CON UN DISOLVENTE NO MISCIBLE EN AGUA, CON UNA RELACION DE VOLUMEN, DISOLVENTE/PRODUCTO DE PARTIDA DE 4:1, PARA EXTRAER DEL COMPUESTO DE PARTIDA TANTA CANTIDAD DE ACIDO FOSFORICO Y TRANSFERIR A LA FASE ORGANICA UN CONTENIDO ENTRE 40 Y 78 EN PESO DEL P2O5, QUEDANDO EL REFINADO ACUOSO CON UNA CANTIDAD DE 28 A 32 EN PESO DE P2O5; B) SEPARAR LA SOLUCION ORGANICA RESULTANTE DE ACIDO FOSFORICO DEL REFINADO ACUOSO DEL MISMO;Y C0 AISLAR LA SOLUCION ORGANICA, SEPARADA DE ACIDO FOSFORICO, POR LAVADO CON UNA SOLUCION DE LAVADO, QUE TIENE EL 5 DEL VOLUMEN DE LA SOLUCION DE ACIDO FOSFORICO COMO MAXIMO PARA OBTENER EL ACIDO FOSFORICO PURIFICADO O UNA SOLUCION PURIFICADA DE SAL FOSFATO. EL COMPUESTO DE PARTIDA ES UN ACIDO FOSFORICO CON UN 45 A 54 EN PESO DE P2O5 Y EL DISOLVENTE ORGANICO ES ALCOHOL AMILICO.
ES527210A 1982-12-15 1983-11-11 Procedimiento para la purificacion de acido fosforico bruto de procedimiento en humedo Expired ES8406376A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19823246415 DE3246415A1 (de) 1982-12-15 1982-12-15 Verfahren zur reinigung von nassverfahrenphosphorsaeure

Publications (2)

Publication Number Publication Date
ES527210A0 ES527210A0 (es) 1984-08-01
ES8406376A1 true ES8406376A1 (es) 1984-08-01

Family

ID=6180733

Family Applications (1)

Application Number Title Priority Date Filing Date
ES527210A Expired ES8406376A1 (es) 1982-12-15 1983-11-11 Procedimiento para la purificacion de acido fosforico bruto de procedimiento en humedo

Country Status (13)

Country Link
US (1) US4596703A (es)
EP (1) EP0111801B1 (es)
JP (1) JPS59116111A (es)
AT (1) ATE33014T1 (es)
BR (1) BR8306875A (es)
CA (1) CA1208880A (es)
DE (2) DE3246415A1 (es)
ES (1) ES8406376A1 (es)
MA (1) MA19975A1 (es)
MX (1) MX159243A (es)
PH (1) PH20955A (es)
TR (1) TR21939A (es)
ZA (1) ZA839284B (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3522822A1 (de) * 1985-06-26 1987-01-02 Hoechst Ag Verfahren zur aufarbeitung von schwermetallhaltigen rueckstaenden aus der reinigung von rohphosphorsaeuren
US4751066A (en) * 1986-05-08 1988-06-14 Fmc Corporation Process for preparing alkali metal phosphate
DE3622597A1 (de) * 1986-07-04 1988-01-07 Budenheim Rud A Oetker Chemie Verfahren zur faellung und abtrennung von cadmiumsulfid aus den raffinaten der phosphorsaeurereinigung
US4780295A (en) * 1987-07-06 1988-10-25 Fmc Corporation Process for purifying phosphoric acid
SE536607C2 (sv) * 2012-06-21 2014-03-25 Easymining Sweden Ab Framställning av ammoniumfosfater
CN114408887A (zh) * 2022-01-28 2022-04-29 江苏电科环保有限公司 一种制备电子级磷酸的方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1929442A (en) * 1930-08-26 1933-10-10 American Agricultural Chem Co Process for obtaining orthophosphoric acid and/or conversion products thereof
US3318661A (en) * 1962-12-31 1967-05-09 Tennessee Corp Process for purifying phosphoric acid
US3684438A (en) * 1970-11-05 1972-08-15 Fmc Corp Purification of phosphoric acid
GB1436113A (en) * 1972-04-26 1976-05-19 Albright & Wilson Purification of phosphoric acid
GB1436114A (en) * 1972-04-26 1976-05-19 Albright & Wilson Purification of phosphoric acid crystallization process
GB1436115A (en) * 1972-10-02 1976-05-19 Albright & Wilson Crystallization process
US4196180A (en) * 1973-07-04 1980-04-01 Hoechst Aktiengesellschaft Purification of phosphoric acid by means of organic solvents
DE2334019C3 (de) * 1973-07-04 1982-11-04 Hoechst Ag, 6000 Frankfurt Verfahren zur Reinigung von verunreinigter wäßriger Phosphorsäure
US4118462A (en) * 1974-02-01 1978-10-03 Rhone-Poulenc Industries Process for the preparation of purified phosphoric solutions from phosphoric acid
DE2605106C2 (de) * 1976-02-10 1984-06-14 Hoechst Ag, 6230 Frankfurt Verfahren und Vorrichtung zur Herstellung von alkoholischen Phosphorsäurelösungen aus sauren Phosphaten
DE2926943A1 (de) * 1979-07-04 1981-01-29 Hoechst Ag Verfahren zur reinigung von nassverfahrensphosphorsaeure
DE3127900A1 (de) * 1981-07-15 1983-02-03 Hoechst Ag, 6000 Frankfurt Verfahren zur extraktion von schwermetallionen aus waessrigen loesungen

Also Published As

Publication number Publication date
CA1208880A (en) 1986-08-05
EP0111801A3 (en) 1985-07-10
ATE33014T1 (de) 1988-04-15
PH20955A (en) 1987-06-10
MX159243A (es) 1989-05-08
ES527210A0 (es) 1984-08-01
MA19975A1 (fr) 1984-07-01
US4596703A (en) 1986-06-24
JPH0445444B2 (es) 1992-07-24
TR21939A (tr) 1985-11-28
BR8306875A (pt) 1984-07-24
JPS59116111A (ja) 1984-07-04
DE3376000D1 (en) 1988-04-21
DE3246415A1 (de) 1984-06-20
EP0111801B1 (de) 1988-03-16
EP0111801A2 (de) 1984-06-27
ZA839284B (en) 1984-08-29

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Legal Events

Date Code Title Description
FD1A Patent lapsed

Effective date: 19970203