ES8304533A1 - "procedimiento de hidrogenacion de anilina para producir ciclohexilamina". - Google Patents
"procedimiento de hidrogenacion de anilina para producir ciclohexilamina".Info
- Publication number
- ES8304533A1 ES8304533A1 ES512889A ES512889A ES8304533A1 ES 8304533 A1 ES8304533 A1 ES 8304533A1 ES 512889 A ES512889 A ES 512889A ES 512889 A ES512889 A ES 512889A ES 8304533 A1 ES8304533 A1 ES 8304533A1
- Authority
- ES
- Spain
- Prior art keywords
- cyclohexylamine
- aniline
- production
- catalyst
- recycled
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- PAFZNILMFXTMIY-UHFFFAOYSA-N cyclohexylamine Chemical compound NC1CCCCC1 PAFZNILMFXTMIY-UHFFFAOYSA-N 0.000 title abstract 4
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 abstract 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 238000009903 catalytic hydrogenation reaction Methods 0.000 abstract 1
- 229910052707 ruthenium Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/68—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
- C07C209/70—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton by reduction of unsaturated amines
- C07C209/72—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton by reduction of unsaturated amines by reduction of six-membered aromatic rings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/18—Carbon
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
- B01J23/46—Ruthenium, rhodium, osmium or iridium
- B01J23/462—Ruthenium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J38/00—Regeneration or reactivation of catalysts, in general
- B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C211/00—Compounds containing amino groups bound to a carbon skeleton
- C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
- C07C211/26—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an unsaturated carbon skeleton containing at least one six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/06—Systems containing only non-condensed rings with a five-membered ring
- C07C2601/08—Systems containing only non-condensed rings with a five-membered ring the ring being saturated
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US06/271,869 US4384142A (en) | 1981-06-09 | 1981-06-09 | Production of cyclohexylamine |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES512889A0 ES512889A0 (es) | 1983-03-01 |
| ES8304533A1 true ES8304533A1 (es) | 1983-03-01 |
Family
ID=23037431
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES512889A Expired ES8304533A1 (es) | 1981-06-09 | 1982-06-07 | "procedimiento de hidrogenacion de anilina para producir ciclohexilamina". |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US4384142A (enEXAMPLES) |
| EP (1) | EP0067058B1 (enEXAMPLES) |
| JP (1) | JPS57212145A (enEXAMPLES) |
| KR (1) | KR860000751B1 (enEXAMPLES) |
| AU (1) | AU546303B2 (enEXAMPLES) |
| BR (1) | BR8203345A (enEXAMPLES) |
| CA (1) | CA1175071A (enEXAMPLES) |
| DE (1) | DE3261126D1 (enEXAMPLES) |
| ES (1) | ES8304533A1 (enEXAMPLES) |
| IN (1) | IN155993B (enEXAMPLES) |
| MX (1) | MX157607A (enEXAMPLES) |
| ZA (1) | ZA824021B (enEXAMPLES) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3225879A1 (de) * | 1982-07-10 | 1984-01-12 | Basf Ag, 6700 Ludwigshafen | Trans-3-(4'-tert.-butylcyclohexyl-1')-2-methyl-1-dialkyl-aminopropane, ihre herstellung und verwendung als arzneimittel |
| US5214212A (en) * | 1992-02-27 | 1993-05-25 | Olin Corporation | Promoters for hydrogenation of aromatic amines |
| DE4207314A1 (de) * | 1992-03-07 | 1993-09-09 | Basf Ag | Verfahren zur herstellung von cycloaliphatischen aminen |
| DE19533718A1 (de) * | 1995-09-12 | 1997-03-13 | Basf Ag | Verfahren zur Hydrierung von aromatischen Verbindungen, in denen mindestens eine Aminogruppe an einen aromatischen Kern gebunden ist |
| DE59706719D1 (de) * | 1996-04-26 | 2002-05-02 | Basf Ag | Verfahren zur Umsetzung einer organischen Verbindung in Gegenwart eines in situ gebildeten Ruthenium-katalysators |
| TW300214B (en) * | 1996-06-06 | 1997-03-11 | Sanfu Chemical Co Ltd | Method for preparing cyclohexylamine |
| US6248924B1 (en) | 1996-06-19 | 2001-06-19 | Basf Aktiengesellschaft | Process for reacting an organic compound in the presence of a supported ruthenium catalyst |
| DE19641688A1 (de) * | 1996-10-10 | 1998-04-16 | Bayer Ag | Katalysatoren und Verfahren zur Herstellung von cycloaliphatischen Aminen |
| DE19651129A1 (de) * | 1996-12-09 | 1998-06-10 | Basf Ag | Verfahren zur Hydrierung einer aromatischen Verbindung in Gegenwart eines Trägerkatalysators |
| DE10128242A1 (de) | 2001-06-11 | 2002-12-12 | Basf Ag | Verfahren zur Hydrierung organischer Verbindungen |
| US7143462B2 (en) * | 2002-09-20 | 2006-12-05 | Colgate-Palmolive Company | Oral care implement |
| DE10225565A1 (de) | 2002-06-10 | 2003-12-18 | Oxeno Olefinchemie Gmbh | Katalysator und Verfahren zur Hydrierung von aromatischen Verbindungen |
| DE102004061608A1 (de) * | 2004-12-17 | 2006-07-06 | Basf Ag | Verfahren zur Herstellung von 1,2-Diamino-3-methylcyclohexan und/oder 1,2-Diamino-4-methylcyclohexan |
| WO2010059421A1 (en) * | 2008-11-18 | 2010-05-27 | Invista Technologies S.A.R.L. | 1,2-diaminocyclohexane and chemical process |
| CN102633649B (zh) * | 2012-03-29 | 2013-08-21 | 山东潍焦集团有限公司 | 一种苯胺气相催化加氢合成环己胺的方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2511028A (en) * | 1947-12-04 | 1950-06-13 | Du Pont | 4-[(para-aminophenyl) alkyl] cyclo-hexylamine |
| US2606924A (en) * | 1949-06-09 | 1952-08-12 | Du Pont | Bis (4-aminocyclohexyl)-methane |
| US2606925A (en) * | 1949-12-15 | 1952-08-12 | Du Pont | Ruthenium catalyzed hydrogenation process for obtaining aminocyclohexyl compounds |
| US2822392A (en) * | 1954-09-20 | 1958-02-04 | Abbott Lab | Process for producing cyclohexylamine |
| US2955926A (en) * | 1954-09-20 | 1960-10-11 | Abbott Lab | High pressure chemical apparatus |
| US3347917A (en) * | 1961-12-29 | 1967-10-17 | Du Pont | Process for the preparation of di (paraaminocyclohexyl) methane |
| US3636108A (en) * | 1965-12-23 | 1972-01-18 | Du Pont | Catalytic hydrogenation of aromatic nitrogen containing compounds over alkali moderated ruthenium |
| FR1530477A (fr) * | 1967-04-14 | 1968-06-28 | Ugine Kuhlmann | Procédé de fabrication de cyclohexylamine ou de cyclohexylamine et de dicyclohexylamine par hydrogénation de l'aniline |
| NL6709040A (enEXAMPLES) * | 1967-06-28 | 1968-12-30 | ||
| US3644522A (en) * | 1969-04-04 | 1972-02-22 | Du Pont | Catalytic hydrogenation of nitrogen containing compounds over supported ruthenium catalysts |
| US3914307A (en) * | 1973-12-27 | 1975-10-21 | Universal Oil Prod Co | Hydrogenation of aromatic amines |
| US4161492A (en) * | 1975-01-24 | 1979-07-17 | Bayer Aktiengesellschaft | Cycloaliphatic amines and process for preparing same |
-
1981
- 1981-06-09 US US06/271,869 patent/US4384142A/en not_active Expired - Lifetime
-
1982
- 1982-06-07 ES ES512889A patent/ES8304533A1/es not_active Expired
- 1982-06-07 DE DE8282302916T patent/DE3261126D1/de not_active Expired
- 1982-06-07 EP EP82302916A patent/EP0067058B1/en not_active Expired
- 1982-06-08 CA CA000404703A patent/CA1175071A/en not_active Expired
- 1982-06-08 MX MX193060A patent/MX157607A/es unknown
- 1982-06-08 ZA ZA824021A patent/ZA824021B/xx unknown
- 1982-06-08 JP JP57097062A patent/JPS57212145A/ja active Granted
- 1982-06-08 KR KR8202554A patent/KR860000751B1/ko not_active Expired
- 1982-06-08 AU AU84673/82A patent/AU546303B2/en not_active Ceased
- 1982-06-08 IN IN654/CAL/82A patent/IN155993B/en unknown
- 1982-06-08 BR BR8203345A patent/BR8203345A/pt not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| EP0067058A1 (en) | 1982-12-15 |
| DE3261126D1 (en) | 1984-12-06 |
| JPS57212145A (en) | 1982-12-27 |
| AU546303B2 (en) | 1985-08-29 |
| IN155993B (enEXAMPLES) | 1985-04-20 |
| MX157607A (es) | 1988-12-05 |
| US4384142A (en) | 1983-05-17 |
| ES512889A0 (es) | 1983-03-01 |
| KR840000472A (ko) | 1984-02-22 |
| JPH05376B2 (enEXAMPLES) | 1993-01-05 |
| EP0067058B1 (en) | 1984-10-31 |
| CA1175071A (en) | 1984-09-25 |
| BR8203345A (pt) | 1984-01-17 |
| KR860000751B1 (ko) | 1986-06-18 |
| AU8467382A (en) | 1982-12-16 |
| ZA824021B (en) | 1983-04-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FD1A | Patent lapsed |
Effective date: 19970303 |