ES8203628A1 - Procedimiento para regenerar el disolvente de extraccion de acido fosforico - Google Patents
Procedimiento para regenerar el disolvente de extraccion de acido fosforicoInfo
- Publication number
- ES8203628A1 ES8203628A1 ES502270A ES502270A ES8203628A1 ES 8203628 A1 ES8203628 A1 ES 8203628A1 ES 502270 A ES502270 A ES 502270A ES 502270 A ES502270 A ES 502270A ES 8203628 A1 ES8203628 A1 ES 8203628A1
- Authority
- ES
- Spain
- Prior art keywords
- phosphoric acid
- extraction solvent
- acid extraction
- regenerating
- regenerating phosphoric
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/46—Preparation involving solvent-solvent extraction
- C01B25/461—Preparation involving solvent-solvent extraction the phosphoric acid present in the medium obtained after reaction being first extracted from the liquid phase formed or separated then re-extracted as free acid by using water or as a phosphate by using a basic compound
- C01B25/465—Preparation involving solvent-solvent extraction the phosphoric acid present in the medium obtained after reaction being first extracted from the liquid phase formed or separated then re-extracted as free acid by using water or as a phosphate by using a basic compound the extracting agent being an ester or a mixture of esters
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
PROCEDIMIENTO PARA GENERAR EL DISOLVENTE DE EXTRACCION DE ACIDO FOSFORICO. SE TRATA, PARTICULARMENTE, DE LAVAR UN DISOLVENTE SUSTANCIALMENTE INMISCUIBLE EN AGUA CON UNA SOLUCION ACUOSA, PARA SEPARAR IMPUREZAS DEL DISOLVENTE, ELIGIENDOSE ESTE ENTRE ALQUILFOSFATOS, ARILFOSFATOS Y ALQUILARILFOSFATOS, E INCLUYENDO TAMBIEN OPCIONALMENTE UN DILUYENTE ORGANICO INMISCIBLE. EL DISOLVENTE HA SIDO UTILIZADO PARA EXTRACTAR ACIDO FOSFORICO DE UNA SOLUCION IMPURA DE ACIDO FOSFORICO Y DE LA CUAL SE HA SEPARADO EL ACIDO FOSFORICO. EL LAVADO DEL DISOLVENTE SE REALIZA CON UNA SOLUCION ACUOSA QUE CONTIENE SUFICIENTE CANTIDAD DE ORTOFOSFATO DE METAL ALCALINO PARA MANTENER EL PH DE LA MEZCLA DISOLVENNTE/FASE ACUOSA EN 9,5-12,5.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US06/150,866 US4311681A (en) | 1980-05-19 | 1980-05-19 | Method of regenerating phosphoric acid extraction solvent |
Publications (2)
Publication Number | Publication Date |
---|---|
ES8203628A1 true ES8203628A1 (es) | 1982-04-01 |
ES502270A0 ES502270A0 (es) | 1982-04-01 |
Family
ID=22536318
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES502270A Granted ES502270A0 (es) | 1980-05-19 | 1981-05-18 | Procedimiento para regenerar el disolvente de extraccion de acido fosforico |
Country Status (10)
Country | Link |
---|---|
US (1) | US4311681A (es) |
EP (1) | EP0040487B2 (es) |
JP (1) | JPS6044244B2 (es) |
BR (1) | BR8103004A (es) |
CA (1) | CA1159222A (es) |
DE (1) | DE3160865D1 (es) |
ES (1) | ES502270A0 (es) |
MX (1) | MX158958A (es) |
PH (1) | PH17382A (es) |
ZA (1) | ZA813226B (es) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS57109702A (en) * | 1980-12-26 | 1982-07-08 | Kumiai Chem Ind Co Ltd | Powdered agricultural chemical emulsion |
US4394361A (en) * | 1982-05-24 | 1983-07-19 | Fmc Corporation | Method of purifying phosphoric acid |
US4643376A (en) * | 1982-09-30 | 1987-02-17 | The Boeing Company | Shock inducing pod for causing flow separation |
JPS6036402A (ja) * | 1983-08-09 | 1985-02-25 | Nichiden Kagaku Kk | 農薬組成物 |
US4751066A (en) * | 1986-05-08 | 1988-06-14 | Fmc Corporation | Process for preparing alkali metal phosphate |
TR28810A (tr) * | 1991-04-02 | 1997-04-07 | Rhone Poulenc Agrochimie | Bir kaplara koyma sistemi ve toksik veya tehlikeli mamülleri, mesela pestisidler ve bunlarin konsantratlari gibi zirai kimyasal bilesimleri depolamak, ambalajlamak ve nakletmek icin elverisli olan kaplar. |
ATE138046T1 (de) * | 1992-07-31 | 1996-06-15 | Foret Sa | Verfahren zur entfernung von abgelagerten verunreinigungen in einem organischen strom zur erzeugung reiner phosphorsäure |
SE536607C2 (sv) | 2012-06-21 | 2014-03-25 | Easymining Sweden Ab | Framställning av ammoniumfosfater |
CN115974019B (zh) * | 2023-01-19 | 2024-03-12 | 广东邦普循环科技有限公司 | 一种溶剂萃取法净化湿法磷酸的方法 |
Family Cites Families (42)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1929443A (en) * | 1930-08-26 | 1933-10-10 | American Agricultural Chem Co | Process for obtaining alkali metal phosphates |
US1929442A (en) * | 1930-08-26 | 1933-10-10 | American Agricultural Chem Co | Process for obtaining orthophosphoric acid and/or conversion products thereof |
US1929441A (en) * | 1930-08-26 | 1933-10-10 | American Agricultural Chem Co | Process for obtaining orthophosphoric acid and/or conversion product thereof |
US2163100A (en) * | 1934-09-13 | 1939-06-20 | Du Pont | Production of finely divided sodamide |
US2917367A (en) * | 1957-01-22 | 1959-12-15 | Swift & Co | Purifying crude phosphoric acid |
US2962357A (en) * | 1957-02-18 | 1960-11-29 | Int Minerals & Chem Corp | Defluorination of phosphoric acid |
US3072461A (en) * | 1960-07-29 | 1963-01-08 | Dow Chemical Co | Preparation of phosphoric acid |
NL277211A (es) * | 1961-04-20 | |||
GB974610A (en) * | 1962-05-24 | 1964-11-04 | Canadian Ind | Purification of phosphoric acid |
US3361527A (en) * | 1964-02-13 | 1968-01-02 | Monsanto Co | Process for separating iron from phosphoric acid containing the same |
NL151045B (nl) | 1964-11-30 | 1976-10-15 | Windmill Holland Bv | Werkwijze voor het verwijderen van fluor uit fosforzuur. |
FR1434190A (fr) * | 1965-01-05 | 1966-04-08 | Pechiney Saint Gobain | Procédé de fabrication d'acide phosphorique purifié |
FR1435877A (fr) * | 1965-01-18 | 1966-04-22 | Pechiney Saint Gobain | Procédé de purification d'acide phosphorique |
US3379501A (en) * | 1965-02-23 | 1968-04-23 | Fmc Corp | Phosphoric acid purification |
GB1117427A (en) * | 1965-03-25 | 1968-06-19 | Monsanto Co | Acid purification process |
US3410656A (en) * | 1966-06-01 | 1968-11-12 | Fmc Corp | Phosphoric acid purification |
US3433592A (en) * | 1966-04-07 | 1969-03-18 | Avraham Baniel | Method of purifying phosphoric acid |
FR1553095A (es) * | 1967-11-30 | 1969-01-10 | ||
US3964994A (en) * | 1969-11-28 | 1976-06-22 | Marathon Oil Company | H2 O2 -containing micellar dispersions |
US3956465A (en) * | 1970-06-12 | 1976-05-11 | Azote Et Produits Chimiques S.A. | Solvent purification of wet process phosphoric acid |
DE2029564C3 (de) * | 1970-06-16 | 1978-06-22 | Giulini Chemie Gmbh, 6700 Ludwigshafen | Verfahren zur Herstellung von reinen Alkaliphosphaten aus Rohphosphorsäure |
DE2035505C3 (de) * | 1970-07-17 | 1974-06-12 | Knapsack Ag, 5033 Huerth-Knapsack | Verfahren zur Herstellung reiner Alkaliphosphatlösungen |
US3694153A (en) * | 1970-10-30 | 1972-09-26 | Audrey E Stern | Liquid-liquid extraction process for the purification of phosphoric acid |
US3819810A (en) * | 1971-01-22 | 1974-06-25 | Fmc Corp | Phosphoric acid purification |
US3707357A (en) * | 1971-03-23 | 1972-12-26 | United States Steel Corp | Wet-process phosphoric acid extraction including separating solvent from extract by freezing solvent |
FR2132203B1 (es) * | 1971-03-29 | 1977-07-22 | Uss Eng & Consult | |
JPS5333960B2 (es) * | 1972-06-10 | 1978-09-18 | ||
US3840639A (en) * | 1972-07-03 | 1974-10-08 | Pennzoil Co | Method for the production of fluoride-free potassium phosphates |
JPS4995894A (es) * | 1973-01-19 | 1974-09-11 | ||
LU66958A1 (es) * | 1973-02-02 | 1974-09-25 | ||
US4018869A (en) * | 1973-06-06 | 1977-04-19 | Chemische Fabrik Budenheim Rudolf A. Oetker | Process for the extractive purification of phosphoric acid containing cationic impurities |
US4118462A (en) * | 1974-02-01 | 1978-10-03 | Rhone-Poulenc Industries | Process for the preparation of purified phosphoric solutions from phosphoric acid |
US3943204A (en) * | 1974-02-05 | 1976-03-09 | The United States Of America As Represented By The United States Energy Research And Development Administration | Method for improving the extraction properties of a tributyl phosphate solution |
DE2433307C3 (de) * | 1974-07-11 | 1984-03-22 | Chemische Fabrik Budenheim Rudolf A. Oetker, 6501 Budenheim | Verfahren zur Abtrennung eines Phosphorsäure-organisches Lösungsmittel-Wasser-Gemisches |
US4207302A (en) * | 1974-07-18 | 1980-06-10 | Freeport Minerals Company | Method of treating phosphoric acid to prevent crud formation during solvent extraction |
JPS5112395A (ja) | 1974-07-18 | 1976-01-30 | Freeport Minerals Co | Yobaichushutsuchunosuratsujiseiseioboshisururinsanshorihoho |
FR2281892A1 (fr) * | 1974-08-13 | 1976-03-12 | Rhone Poulenc Ind | Procede de defluoration d'acide phosphorique |
US3972982A (en) * | 1975-03-03 | 1976-08-03 | Monsanto Company | Process for removing fluorine compounds from phosphoric acid |
US3993736A (en) * | 1975-08-14 | 1976-11-23 | Stauffer Chemical Company | Food grade phosphoric acid from wet process acid |
JPS5297394A (en) * | 1976-02-13 | 1977-08-16 | Toyo Soda Mfg Co Ltd | Removal of organic matter in phosphoric acid |
ZA774159B (en) * | 1977-10-27 | 1978-07-26 | Albright & Wilson | Process for preparing phosphate salts |
DE2657189B2 (de) * | 1976-12-17 | 1980-02-07 | Hoechst Ag, 6000 Frankfurt | Verfahren zur Reinigung von NaBverfahrensphosphorsäure |
-
1980
- 1980-05-19 US US06/150,866 patent/US4311681A/en not_active Expired - Lifetime
-
1981
- 1981-05-05 DE DE8181301974T patent/DE3160865D1/de not_active Expired
- 1981-05-05 EP EP81301974A patent/EP0040487B2/en not_active Expired
- 1981-05-06 CA CA000376978A patent/CA1159222A/en not_active Expired
- 1981-05-14 ZA ZA00813226A patent/ZA813226B/xx unknown
- 1981-05-14 BR BR8103004A patent/BR8103004A/pt unknown
- 1981-05-15 PH PH25638A patent/PH17382A/en unknown
- 1981-05-18 ES ES502270A patent/ES502270A0/es active Granted
- 1981-05-19 MX MX187391A patent/MX158958A/es unknown
- 1981-05-19 JP JP56074333A patent/JPS6044244B2/ja not_active Expired
Also Published As
Publication number | Publication date |
---|---|
PH17382A (en) | 1984-08-06 |
US4311681A (en) | 1982-01-19 |
CA1159222A (en) | 1983-12-27 |
DE3160865D1 (en) | 1983-10-20 |
MX158958A (es) | 1989-04-04 |
EP0040487B1 (en) | 1983-09-14 |
JPS6044244B2 (ja) | 1985-10-02 |
EP0040487A1 (en) | 1981-11-25 |
ZA813226B (en) | 1982-06-30 |
ES502270A0 (es) | 1982-04-01 |
EP0040487B2 (en) | 1987-09-09 |
JPS5715802A (en) | 1982-01-27 |
BR8103004A (pt) | 1982-02-09 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FD1A | Patent lapsed |
Effective date: 20011110 |