ES8201149A1 - Preparation of glycidyl ether - Google Patents

Preparation of glycidyl ether

Info

Publication number
ES8201149A1
ES8201149A1 ES499016A ES499016A ES8201149A1 ES 8201149 A1 ES8201149 A1 ES 8201149A1 ES 499016 A ES499016 A ES 499016A ES 499016 A ES499016 A ES 499016A ES 8201149 A1 ES8201149 A1 ES 8201149A1
Authority
ES
Spain
Prior art keywords
alcohol
epihalohydrin
reacting
integer
aqueous solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES499016A
Other languages
Spanish (es)
Other versions
ES499016A0 (en
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kao Corp
Original Assignee
Kao Corp
Kao Soap Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kao Corp, Kao Soap Co Ltd filed Critical Kao Corp
Publication of ES8201149A1 publication Critical patent/ES8201149A1/en
Publication of ES499016A0 publication Critical patent/ES499016A0/en
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
    • C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
    • C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
    • C07D303/22—Ethers with hydroxy compounds containing no oxirane rings with monohydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
    • C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
    • C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
    • C07D303/24—Ethers with hydroxy compounds containing no oxirane rings with polyhydroxy compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Epoxy Compounds (AREA)

Abstract

PURPOSE:To prepare the titled compound, economically, in high yield, by reacting an alcohol with an epihalohydrin in the presence of an aqueous solution of an alkaline substance and a quaternary ammonium compound having (poly)oxyalkylene group in the molecule. CONSTITUTION:The titled compound having a wide range of industrial applications as intermediates of glycerol derivatives, etc., is prepared easily, in one step from the starting materials, in high yield and an industrial scale, by reacting an alcohol with an epihalohydrin in the presence of an aqueous solution of an alkaline substance such as an alkali metal hydroxide or a weak acid salt of an alkali metal and a catalytic amount (pref. 0.01-0.1mol, based on the alcohol) of a quaternary ammonium compound of formula I or II (R1-R3 are alkyl, aralkyl or cycloalkyl A is alkylene a is an integer of >=1) b and c are an integer of >=0, and b+c>=2 X is anion) at 0-100 deg.C.
ES499016A 1980-02-01 1981-01-30 A PROCEDURE FOR THE PRODUCTION OF A GLYCIDYLIC ETHER FROM AN ALCOHOL Granted ES499016A0 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP1111580A JPS603392B2 (en) 1980-02-01 1980-02-01 Manufacturing method of glycidyl ether

Publications (2)

Publication Number Publication Date
ES8201149A1 true ES8201149A1 (en) 1981-12-01
ES499016A0 ES499016A0 (en) 1981-12-01

Family

ID=11769003

Family Applications (1)

Application Number Title Priority Date Filing Date
ES499016A Granted ES499016A0 (en) 1980-02-01 1981-01-30 A PROCEDURE FOR THE PRODUCTION OF A GLYCIDYLIC ETHER FROM AN ALCOHOL

Country Status (3)

Country Link
JP (1) JPS603392B2 (en)
DE (1) DE3103181A1 (en)
ES (1) ES499016A0 (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5993022A (en) * 1982-11-16 1984-05-29 Kao Corp Polyol ether compound, its preparation and cosmetic containing the same
DE3803213C1 (en) * 1988-02-04 1989-02-23 Th. Goldschmidt Ag, 4300 Essen, De
CN108350252B (en) * 2015-11-05 2021-04-09 日产化学工业株式会社 Epoxy reactive diluent and epoxy resin composition containing same
KR20190140474A (en) * 2017-05-09 2019-12-19 닛산 가가쿠 가부시키가이샤 Method of producing epoxy compound
CN109280038A (en) * 2018-09-17 2019-01-29 大丰跃龙化学有限公司 A kind of synthetic method of Sensiva SC50 ether

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6022414B2 (en) * 1978-04-10 1985-06-01 日立マクセル株式会社 magnetic recording medium
JPS54141708A (en) * 1978-04-26 1979-11-05 Osaka Soda Co Ltd Preparation of glycidyl ether

Also Published As

Publication number Publication date
DE3103181C2 (en) 1989-10-05
DE3103181A1 (en) 1981-11-26
JPS56108781A (en) 1981-08-28
JPS603392B2 (en) 1985-01-28
ES499016A0 (en) 1981-12-01

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Legal Events

Date Code Title Description
FD1A Patent lapsed

Effective date: 20010201