ES467957A1 - Procedimiento para la obtencion de un material separador pa-ra cromatografia de capa delgada - Google Patents

Procedimiento para la obtencion de un material separador pa-ra cromatografia de capa delgada

Info

Publication number
ES467957A1
ES467957A1 ES467957A ES467957A ES467957A1 ES 467957 A1 ES467957 A1 ES 467957A1 ES 467957 A ES467957 A ES 467957A ES 467957 A ES467957 A ES 467957A ES 467957 A1 ES467957 A1 ES 467957A1
Authority
ES
Spain
Prior art keywords
layer chromatography
preparation
thin layer
separating materials
sorbent layer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES467957A
Other languages
English (en)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Merck Patent GmbH
Original Assignee
Merck Patent GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE2712113A external-priority patent/DE2712113C2/de
Application filed by Merck Patent GmbH filed Critical Merck Patent GmbH
Publication of ES467957A1 publication Critical patent/ES467957A1/es
Expired legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/90—Plate chromatography, e.g. thin layer or paper chromatography
    • G01N30/92—Construction of the plate
    • G01N30/93—Application of the sorbent layer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/103—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/2803—Sorbents comprising a binder, e.g. for forming aggregated, agglomerated or granulated products
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28057—Surface area, e.g. B.E.T specific surface area
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/286—Phases chemically bonded to a substrate, e.g. to silica or to polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/286—Phases chemically bonded to a substrate, e.g. to silica or to polymers
    • B01J20/287—Non-polar phases; Reversed phases
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3042—Use of binding agents; addition of materials ameliorating the mechanical properties of the produced sorbent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
    • B01J20/3204—Inorganic carriers, supports or substrates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3242—Layers with a functional group, e.g. an affinity material, a ligand, a reactant or a complexing group
    • B01J20/3244—Non-macromolecular compounds
    • B01J20/3246—Non-macromolecular compounds having a well defined chemical structure
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/50—Conditioning of the sorbent material or stationary liquid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/54—Sorbents specially adapted for analytical or investigative chromatography

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Inorganic Chemistry (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)

Abstract

Procedimiento para la obtención de un material separador para cromatografía de capa delgada, del tipo que comprende un material soporte recubierto de una delgada capa de absorbente, que puede contener en caso dado aglutinante y/o indicadores, caracterizado porque se impregna, bajo condiciones de temperatura y humedad ambientes, la capa de absorbente de un material separador para cromatografía de capa delgada, cuya superficie está sin modificar, con una solución de un agente de silanización en un disolvente orgánico inerte frente al agente de silanización, con un punto de ebullición comprendido entre 30 y 180ºC, a continuación se seca al aire, bajo condiciones de humedad ambiente, seguidamente se lava el producto de la etapa anterior, en primer lugar con al menos un disolvente aprótico, y a continuación, tras secado al aire, con al menos un disolvente prótico.
ES467957A 1977-03-19 1978-03-17 Procedimiento para la obtencion de un material separador pa-ra cromatografia de capa delgada Expired ES467957A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE2712113A DE2712113C2 (de) 1977-03-19 1977-03-19 Trennmaterial für die Dünnschichtchromatographie und Verfahren zu dessen Herstellung

Publications (1)

Publication Number Publication Date
ES467957A1 true ES467957A1 (es) 1979-11-16

Family

ID=6004087

Family Applications (1)

Application Number Title Priority Date Filing Date
ES467957A Expired ES467957A1 (es) 1977-03-19 1978-03-17 Procedimiento para la obtencion de un material separador pa-ra cromatografia de capa delgada

Country Status (14)

Country Link
US (1) US4295968A (es)
JP (1) JPS5811573B2 (es)
AT (1) AT361898B (es)
BE (1) BE864995A (es)
CA (1) CA1112634A (es)
CH (1) CH633451A5 (es)
CS (1) CS209889B2 (es)
DD (1) DD135649A5 (es)
ES (1) ES467957A1 (es)
FR (1) FR2383690A1 (es)
GB (1) GB1580675A (es)
IT (1) IT1105161B (es)
NL (1) NL7802954A (es)
SE (1) SE427422B (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU532164B2 (en) * 1978-11-15 1983-09-22 British Petroleum Company Plc, The Removing metals from solution
JPS56150354A (en) * 1980-04-22 1981-11-20 Shionogi & Co Ltd Plate for reversed-phase chromatography and its production
DE3427923A1 (de) * 1984-07-28 1986-01-30 Merck Patent Gmbh, 6100 Darmstadt Trennmaterial fuer die duennschichtchromatographie
JPS61210956A (ja) * 1985-03-15 1986-09-19 Cosmo Co Ltd クロマトグラフイ−用薄層棒
DE19805395A1 (de) * 1998-02-11 1999-08-12 Merck Patent Gmbh Dünne poröse Schichten für die planare Chromatographie
JP5703514B2 (ja) * 2010-11-02 2015-04-22 日立化成株式会社 金の捕集材および分離回収方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2614135A (en) * 1950-08-30 1952-10-14 Sun Oil Co Selective adsorption of nonpolar organic compounds
DE1442446C3 (de) * 1965-06-18 1974-03-14 Merck Patent Gmbh, 6100 Darmstadt Sorptionsmittel für die Schichtchromatographie:
US3922431A (en) * 1969-02-20 1975-11-25 Edmund Radmacher Elements for thin-layer chromatography
US3664967A (en) * 1970-02-11 1972-05-23 Dow Chemical Co Pellicular column packing for liquid chromatography
DE2313073C2 (de) * 1973-03-16 1984-11-29 Istvan Prof. Dr. 6600 Saarbruecken Halasz Verfahren zur chemischen Modifizierung von Oberflächen anorganischer Festkörper und deren Verwendung
US3987058A (en) * 1975-02-27 1976-10-19 The United States Of America As Represented By The Secretary Of Agriculture Preparation and uses of stable, bound stationary phases

Also Published As

Publication number Publication date
IT1105161B (it) 1985-10-28
FR2383690A1 (fr) 1978-10-13
JPS5811573B2 (ja) 1983-03-03
AT361898B (de) 1981-04-10
SE7803104L (sv) 1978-09-20
FR2383690B1 (es) 1982-12-03
JPS53117498A (en) 1978-10-13
IT7848487A0 (it) 1978-03-17
GB1580675A (en) 1980-12-03
DD135649A5 (de) 1979-05-16
SE427422B (sv) 1983-04-11
CA1112634A (en) 1981-11-17
US4295968A (en) 1981-10-20
CS209889B2 (en) 1981-12-31
ATA192478A (de) 1980-09-15
CH633451A5 (de) 1982-12-15
NL7802954A (nl) 1978-09-21
BE864995A (nl) 1978-09-18

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Legal Events

Date Code Title Description
FD1A Patent lapsed

Effective date: 20010301