ES419805A1 - Procedimiento para la separacion por destilacion extractivade acetato de vinilo y metanol. - Google Patents

Procedimiento para la separacion por destilacion extractivade acetato de vinilo y metanol.

Info

Publication number
ES419805A1
ES419805A1 ES419805A ES419805A ES419805A1 ES 419805 A1 ES419805 A1 ES 419805A1 ES 419805 A ES419805 A ES 419805A ES 419805 A ES419805 A ES 419805A ES 419805 A1 ES419805 A1 ES 419805A1
Authority
ES
Spain
Prior art keywords
mixtures
separation
vinyl acetate
minor amounts
acetaldehyde
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES419805A
Other languages
English (en)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Farbwerke Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE19722252276 external-priority patent/DE2252276C2/de
Priority claimed from DE19732342144 external-priority patent/DE2342144C3/de
Application filed by Hoechst AG, Farbwerke Hoechst AG filed Critical Hoechst AG
Publication of ES419805A1 publication Critical patent/ES419805A1/es
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C07C29/84Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation by extractive distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40Extractive distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/52Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00Distillation: processes, separatory
    • Y10S203/10Vinyl acetate

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
ES419805A 1972-10-25 1973-10-19 Procedimiento para la separacion por destilacion extractivade acetato de vinilo y metanol. Expired ES419805A1 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19722252276 DE2252276C2 (de) 1972-10-25 1972-10-25 Verfahren zur gewinnung von vinylacetat aus gemischen, die im wesentlichen vinylacetat und methanol und als verunreinigung methylacetat und acetaldehyd enthalten
DE19732342144 DE2342144C3 (de) 1973-08-21 Verfahren zur Gewinnung von Vinylacetat aus Gemischen, die im wesentlichen Vinylacetat und Methanol und als Verunreinigung Methylacetat und Acetaldehyd enthalten

Publications (1)

Publication Number Publication Date
ES419805A1 true ES419805A1 (es) 1976-07-16

Family

ID=25764004

Family Applications (1)

Application Number Title Priority Date Filing Date
ES419805A Expired ES419805A1 (es) 1972-10-25 1973-10-19 Procedimiento para la separacion por destilacion extractivade acetato de vinilo y metanol.

Country Status (9)

Country Link
US (1) US3855078A (es)
JP (1) JPS5738567B2 (es)
DD (1) DD107013A5 (es)
ES (1) ES419805A1 (es)
FR (1) FR2204609B1 (es)
GB (1) GB1419465A (es)
IT (1) IT998900B (es)
NL (1) NL185202C (es)
SU (1) SU584758A3 (es)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4473444A (en) * 1981-02-09 1984-09-25 National Distillers And Chemical Corporation Extractive distillation of alcohol-ester mixtures
US4431838A (en) * 1981-02-09 1984-02-14 National Distillers And Chemical Corporation Extractive distillation of alcohol-ester mixtures and transesterification
US7550065B2 (en) * 2005-04-21 2009-06-23 Lyondell Chemical Technology, L.P. Method for recovering solvents
WO2009142616A1 (en) * 2007-12-21 2009-11-26 Celanese International Corporation Process for making low color polyvinyl alcohol
CN109851499B (zh) * 2018-12-24 2022-02-15 天津大学 一种利用共沸精馏分离醋酸乙烯酯中苯的方法及装置
CN110028408A (zh) * 2019-04-28 2019-07-19 青岛科技大学 一种部分热耦合萃取精馏分离乙酸乙酯-乙醇-水混合物的方法
CN115093041B (zh) * 2022-02-22 2024-02-13 杨自林 生产5-氨基-2-硝基三氟甲苯产生的工业废水的资源化处理方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2349807A (en) * 1941-08-30 1944-05-30 Carbide & Carbon Chem Corp Recovery of vinyl acetate from solvent mixtures
US2575244A (en) * 1948-09-08 1951-11-13 Standard Oil Dev Co Process for separating ketones from close-boiling mixtures
US2622060A (en) * 1950-01-26 1952-12-16 Celanese Corp Purification of 1,2-propylene oxide
US3350417A (en) * 1964-02-12 1967-10-31 Monsanto Co Production and recovery of propylene oxide by plural stage distillation and caustic addition
US3636087A (en) * 1966-09-12 1972-01-18 Atlantic Richfield Co Vinyl acetate recovery process
US3616271A (en) * 1968-10-25 1971-10-26 Du Pont Separation of chloroform and/or ethyl acetate from vinyl acetate by extractive distillation
US3551299A (en) * 1968-12-18 1970-12-29 Celanese Corp Method of minimizing polymer formation during distillation of vinyl acetate by the addition of alphamethyl styrene
US3691021A (en) * 1970-03-26 1972-09-12 Nat Distillers Chem Corp Process for purification of vinyl acetate by extractive distillation

Also Published As

Publication number Publication date
US3855078A (en) 1974-12-17
FR2204609B1 (es) 1977-08-12
NL185202C (nl) 1990-02-16
JPS5738567B2 (es) 1982-08-16
IT998900B (it) 1976-02-20
DD107013A5 (es) 1974-07-12
NL7314426A (es) 1974-04-29
NL185202B (nl) 1989-09-18
JPS4975509A (es) 1974-07-20
FR2204609A1 (es) 1974-05-24
SU584758A3 (ru) 1977-12-15
GB1419465A (en) 1975-12-31

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Legal Events

Date Code Title Description
FD1A Patent lapsed

Effective date: 19930211