ES383380A1 - Process for restoring propellent charge powder - Google Patents
Process for restoring propellent charge powderInfo
- Publication number
- ES383380A1 ES383380A1 ES383380A ES383380A ES383380A1 ES 383380 A1 ES383380 A1 ES 383380A1 ES 383380 A ES383380 A ES 383380A ES 383380 A ES383380 A ES 383380A ES 383380 A1 ES383380 A1 ES 383380A1
- Authority
- ES
- Spain
- Prior art keywords
- powder
- propellent charge
- restoring
- charge powder
- diphenylamine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000843 powder Substances 0.000 title abstract 7
- DMBHHRLKUKUOEG-UHFFFAOYSA-N diphenylamine Chemical compound C=1C=CC=CC=1NC1=CC=CC=C1 DMBHHRLKUKUOEG-UHFFFAOYSA-N 0.000 abstract 4
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 abstract 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 2
- 239000000020 Nitrocellulose Substances 0.000 abstract 2
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 abstract 2
- 229910002804 graphite Inorganic materials 0.000 abstract 2
- 239000010439 graphite Substances 0.000 abstract 2
- 229920001220 nitrocellulos Polymers 0.000 abstract 2
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 abstract 1
- DYSXLQBUUOPLBB-UHFFFAOYSA-N 2,3-dinitrotoluene Chemical compound CC1=CC=CC([N+]([O-])=O)=C1[N+]([O-])=O DYSXLQBUUOPLBB-UHFFFAOYSA-N 0.000 abstract 1
- 241000723346 Cinnamomum camphora Species 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- FJWGYAHXMCUOOM-QHOUIDNNSA-N [(2s,3r,4s,5r,6r)-2-[(2r,3r,4s,5r,6s)-4,5-dinitrooxy-2-(nitrooxymethyl)-6-[(2r,3r,4s,5r,6s)-4,5,6-trinitrooxy-2-(nitrooxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-3,5-dinitrooxy-6-(nitrooxymethyl)oxan-4-yl] nitrate Chemical compound O([C@@H]1O[C@@H]([C@H]([C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O)O[C@H]1[C@@H]([C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@@H](CO[N+]([O-])=O)O1)O[N+]([O-])=O)CO[N+](=O)[O-])[C@@H]1[C@@H](CO[N+]([O-])=O)O[C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O FJWGYAHXMCUOOM-QHOUIDNNSA-N 0.000 abstract 1
- 229960000846 camphor Drugs 0.000 abstract 1
- 229930008380 camphor Natural products 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 abstract 1
- 229910052939 potassium sulfate Inorganic materials 0.000 abstract 1
- 239000001120 potassium sulphate Substances 0.000 abstract 1
- 235000011151 potassium sulphates Nutrition 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J11/00—Recovery or working-up of waste materials
- C08J11/04—Recovery or working-up of waste materials of polymers
- C08J11/06—Recovery or working-up of waste materials of polymers without chemical reactions
- C08J11/08—Recovery or working-up of waste materials of polymers without chemical reactions using selective solvents for polymer components
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B21/00—Apparatus or methods for working-up explosives, e.g. forming, cutting, drying
- C06B21/0091—Elimination of undesirable or temporary components of an intermediate or finished product, e.g. making porous or low density products, purifying, stabilising, drying; Deactivating; Reclaiming
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2301/00—Characterised by the use of cellulose, modified cellulose or cellulose derivatives
- C08J2301/08—Cellulose derivatives
- C08J2301/16—Esters of inorganic acids
- C08J2301/18—Cellulose nitrate
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/62—Plastics recycling; Rubber recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Carbon And Carbon Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Working-Up Tar And Pitch (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The calorimetric potential of an old propellent charge powder containing nitrocellulose is increased by extracting the powder with methylene chloride. For example, dinitrotoluene, dibutyl phthalate, and diphenylamine are removed from a single base powder by grinding in a stream of water and then extracting with the solvent. In another example a powder containing nitrocellulose, camphor, diphenylamine, potassium sulphate, and graphite is first treated with alcohol to remove the graphite. Extraction may be carried out at about 35 C. either batchwise or continuously. The treated powder may be used in the manufacture of sporting powders.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR6935123A FR2063402A5 (en) | 1969-10-14 | 1969-10-14 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES383380A1 true ES383380A1 (en) | 1973-01-16 |
Family
ID=9041519
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES383380A Expired ES383380A1 (en) | 1969-10-14 | 1970-09-04 | Process for restoring propellent charge powder |
Country Status (5)
| Country | Link |
|---|---|
| BE (1) | BE757442A (en) |
| DE (1) | DE2050375A1 (en) |
| ES (1) | ES383380A1 (en) |
| FR (1) | FR2063402A5 (en) |
| GB (1) | GB1262831A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2264352A1 (en) * | 2004-10-22 | 2006-12-16 | Ecopiro, S.L. | Procedure is for recycling signalling equipment whose useful life is ended or which have deteriorated, as used in pyrotechnics for life-saving at sea and/or on land |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4477297A (en) * | 1983-02-28 | 1984-10-16 | Hercules Incorporated | Manufacture of gel free nitrocellulose lacquers |
| DE4123225C1 (en) * | 1991-07-11 | 1992-11-05 | Mechanische Werkstaetten Koenigswartha Gmbh, O-8613 Koenigswartha, De | |
| DE4230695C1 (en) * | 1992-09-14 | 1994-04-21 | Eilenburger Chemie Werke Ag | Process for isolating cellulose nitrate from non-graphitized monobasic propellant powders, the cellulose nitrate obtainable by the process and its use |
| WO1994006853A1 (en) * | 1992-09-14 | 1994-03-31 | Eilenburger Chemie Werke Aktiengesellschaft | Process for isolating cellulose nitrate from non-graphited monobasic propellant powders |
| DE19818337C1 (en) * | 1998-04-23 | 1999-11-18 | Buck Werke Gmbh & Co Kg | Pyrotechnic active mass with ignition and combustion accelerator |
| CN102230860B (en) * | 2011-06-20 | 2013-01-02 | 西安近代化学研究所 | Accelerated solvent extraction pretreatment method of gunpowder and explosive samples |
| FI3642175T3 (en) * | 2017-06-23 | 2024-06-04 | Knds Ammo Italy S P A | Composition for single-base propelling powder for ammunition and ammunition provided with such composition |
-
0
- BE BE757442D patent/BE757442A/en not_active IP Right Cessation
-
1969
- 1969-10-14 FR FR6935123A patent/FR2063402A5/fr not_active Expired
-
1970
- 1970-09-04 ES ES383380A patent/ES383380A1/en not_active Expired
- 1970-10-05 GB GB4728670A patent/GB1262831A/en not_active Expired
- 1970-10-14 DE DE19702050375 patent/DE2050375A1/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2264352A1 (en) * | 2004-10-22 | 2006-12-16 | Ecopiro, S.L. | Procedure is for recycling signalling equipment whose useful life is ended or which have deteriorated, as used in pyrotechnics for life-saving at sea and/or on land |
Also Published As
| Publication number | Publication date |
|---|---|
| BE757442A (en) | 1971-03-16 |
| FR2063402A5 (en) | 1971-07-09 |
| GB1262831A (en) | 1972-02-09 |
| DE2050375A1 (en) | 1971-04-22 |
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