ES2603643B1 - Procedimiento para sintetizar glicidol - Google Patents

Procedimiento para sintetizar glicidol Download PDF

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Publication number
ES2603643B1
ES2603643B1 ES201531136A ES201531136A ES2603643B1 ES 2603643 B1 ES2603643 B1 ES 2603643B1 ES 201531136 A ES201531136 A ES 201531136A ES 201531136 A ES201531136 A ES 201531136A ES 2603643 B1 ES2603643 B1 ES 2603643B1
Authority
ES
Spain
Prior art keywords
metal
glycidol
catalyst
stannates
alkaline earth
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
ES201531136A
Other languages
English (en)
Spanish (es)
Other versions
ES2603643A1 (es
Inventor
José Ramón OCHOA GÓMEZ
Olga GÓMEZ DE MIRANDA JIMÉNEZ DE ABERASTUI
Noelia BLANCO PÉREZ
Belén MAESTRO MADURGA
Soraya PRIETO FERNÁNDEZ
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fundación Tecnalia Research and Innovation
Original Assignee
Fundación Tecnalia Research and Innovation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fundación Tecnalia Research and Innovation filed Critical Fundación Tecnalia Research and Innovation
Priority to ES201531136A priority Critical patent/ES2603643B1/es
Priority to EP16829907.1A priority patent/EP3330261A4/en
Priority to PCT/ES2016/070573 priority patent/WO2017017307A1/es
Priority to JP2018504787A priority patent/JP6839172B2/ja
Priority to US15/748,599 priority patent/US10640478B2/en
Publication of ES2603643A1 publication Critical patent/ES2603643A1/es
Application granted granted Critical
Publication of ES2603643B1 publication Critical patent/ES2603643B1/es
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
    • C07D303/14—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by free hydroxyl radicals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
    • B01J21/04—Alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/066—Zirconium or hafnium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/08—Silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/10—Magnesium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/02—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the alkali- or alkaline earth metals or beryllium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/02—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the alkali- or alkaline earth metals or beryllium
    • B01J23/04—Alkali metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/10—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of rare earths
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/14—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of germanium, tin or lead
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/20—Vanadium, niobium or tantalum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/04—Mixing
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
ES201531136A 2015-07-30 2015-07-30 Procedimiento para sintetizar glicidol Active ES2603643B1 (es)

Priority Applications (5)

Application Number Priority Date Filing Date Title
ES201531136A ES2603643B1 (es) 2015-07-30 2015-07-30 Procedimiento para sintetizar glicidol
EP16829907.1A EP3330261A4 (en) 2015-07-30 2016-07-28 GLYCIDOLSYNTHESEVERFAHREN
PCT/ES2016/070573 WO2017017307A1 (es) 2015-07-30 2016-07-28 Procedimiento para sintetizar glicidol
JP2018504787A JP6839172B2 (ja) 2015-07-30 2016-07-28 グリシドールの合成方法
US15/748,599 US10640478B2 (en) 2015-07-30 2016-07-28 Glycidol synthesis method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ES201531136A ES2603643B1 (es) 2015-07-30 2015-07-30 Procedimiento para sintetizar glicidol

Publications (2)

Publication Number Publication Date
ES2603643A1 ES2603643A1 (es) 2017-02-28
ES2603643B1 true ES2603643B1 (es) 2017-12-13

Family

ID=57884656

Family Applications (1)

Application Number Title Priority Date Filing Date
ES201531136A Active ES2603643B1 (es) 2015-07-30 2015-07-30 Procedimiento para sintetizar glicidol

Country Status (5)

Country Link
US (1) US10640478B2 (enExample)
EP (1) EP3330261A4 (enExample)
JP (1) JP6839172B2 (enExample)
ES (1) ES2603643B1 (enExample)
WO (1) WO2017017307A1 (enExample)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2572385B (en) 2018-03-28 2023-05-31 Green Lizard Tech Ltd Process for the preparation of glycidol

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2856413A (en) 1956-07-23 1958-10-14 Jefferson Chem Co Inc Method for preparing glycidol
US5164497A (en) * 1990-09-20 1992-11-17 Union Carbide Chemicals & Plastics Technology Corporation Decarboxylation processes using mixed metal oxide catalysts
DE4225870A1 (de) 1992-08-05 1994-02-10 Basf Ag Verfahren zur Herstellung von Glycerincarbonat
FR2760747B1 (fr) 1997-03-12 1999-06-04 Organisation Nationale Interpr Procede de fabrication de glycidol ou d'un compose glycidyle
WO2007145278A1 (ja) 2006-06-15 2007-12-21 Kao Corporation グリシドールの製造方法
US7868192B1 (en) * 2009-07-15 2011-01-11 Kao Corporation Process for producing glycidol
KR101416706B1 (ko) 2012-11-14 2014-07-09 한국과학기술연구원 글리시돌의 제조방법
CN103554060A (zh) * 2013-09-13 2014-02-05 华中科技大学 甘油和碳酸二甲酯一步法合成缩水甘油的催化剂

Also Published As

Publication number Publication date
WO2017017307A1 (es) 2017-02-02
JP2018524395A (ja) 2018-08-30
JP6839172B2 (ja) 2021-03-03
EP3330261A1 (en) 2018-06-06
ES2603643A1 (es) 2017-02-28
US20180319756A1 (en) 2018-11-08
US10640478B2 (en) 2020-05-05
EP3330261A4 (en) 2019-03-20

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