ES2552760T3 - Método para la producción de dinitrotolueno - Google Patents

Método para la producción de dinitrotolueno Download PDF

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Publication number
ES2552760T3
ES2552760T3 ES05701305.4T ES05701305T ES2552760T3 ES 2552760 T3 ES2552760 T3 ES 2552760T3 ES 05701305 T ES05701305 T ES 05701305T ES 2552760 T3 ES2552760 T3 ES 2552760T3
Authority
ES
Spain
Prior art keywords
stage
mnt
acid
dnt
toluene
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES05701305.4T
Other languages
English (en)
Spanish (es)
Inventor
Johannes Büttner
Wolfgang Mackenroth
Heinrich Hermann
Peter Konieczny
Jürgen Gebauer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of ES2552760T3 publication Critical patent/ES2552760T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/14—Preparation of nitro compounds by formation of nitro groups together with reactions not involving the formation of nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/06—Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to carbon atoms of six-membered aromatic rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
ES05701305.4T 2004-02-05 2005-02-02 Método para la producción de dinitrotolueno Expired - Lifetime ES2552760T3 (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102004005913A DE102004005913A1 (de) 2004-02-05 2004-02-05 Verfahren zur Herstellung von Dinitrotoluol
DE102004005913 2004-02-05
PCT/EP2005/001017 WO2005075407A1 (de) 2004-02-05 2005-02-02 Verfahren zur herstellung von dinitrotoluol

Publications (1)

Publication Number Publication Date
ES2552760T3 true ES2552760T3 (es) 2015-12-02

Family

ID=34801677

Family Applications (1)

Application Number Title Priority Date Filing Date
ES05701305.4T Expired - Lifetime ES2552760T3 (es) 2004-02-05 2005-02-02 Método para la producción de dinitrotolueno

Country Status (13)

Country Link
US (1) US7851661B2 (enExample)
EP (1) EP1713756B1 (enExample)
JP (1) JP4554622B2 (enExample)
KR (1) KR101151068B1 (enExample)
CN (1) CN100488941C (enExample)
BR (1) BRPI0507293B1 (enExample)
DE (1) DE102004005913A1 (enExample)
ES (1) ES2552760T3 (enExample)
HU (1) HUE025592T2 (enExample)
PL (1) PL1713756T3 (enExample)
PT (1) PT1713756E (enExample)
WO (1) WO2005075407A1 (enExample)
ZA (1) ZA200607374B (enExample)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102006033722A1 (de) 2006-07-21 2008-01-24 Bayer Materialscience Ag Verfahren zur Herstellung von Dinitrotoluol
DE102006060572A1 (de) 2006-12-19 2008-06-26 Bayer Materialscience Ag Verfahren zur Herstellung von Toluylendiaminen durch katalytische Hydrierung von Dinitrotoluolen
JP2012518674A (ja) 2009-02-26 2012-08-16 ビーエーエスエフ ソシエタス・ヨーロピア ニトロ化芳香族化合物及びそれらの混合物の製造方法
JP5175235B2 (ja) * 2009-03-31 2013-04-03 三井化学株式会社 ジニトロトルエンの製造方法および製造装置
CN101612535B (zh) * 2009-08-04 2013-05-01 上海巴斯夫聚氨酯有限公司 混合罐设有喷射式混合器的二硝基甲苯生产装置
CN102276470A (zh) * 2010-06-08 2011-12-14 中国石油化工集团公司 连续逆流硝化芳烃化合物的方法
EP2714650A1 (de) 2011-05-24 2014-04-09 Basf Se Verfahren zur herstellung von polyisocyanaten aus biomasse
US8933262B2 (en) 2011-05-24 2015-01-13 Basf Se Process for preparing polyisocyanates from biomass
WO2014094270A1 (en) * 2012-12-20 2014-06-26 Basf Se Separation method for dinitrotoluene and mixed acid in toluene to dinitrotoluene process
CN105102419B (zh) * 2012-12-20 2017-09-29 巴斯夫欧洲公司 在甲苯至二硝基甲苯的方法中二硝基甲苯与混合酸的分离方法
KR102474434B1 (ko) * 2014-11-20 2022-12-07 코베스트로 도이칠란드 아게 적어도 2개의 함께 커플링된 화학 반응을 통한 생성물의 연속 제조 방법
CN109467508B (zh) * 2018-11-22 2021-08-10 四川金象赛瑞化工股份有限公司 一种微通道反应器合成二硝基甲苯的方法
CN116283594A (zh) * 2021-12-20 2023-06-23 中国石油化工股份有限公司 2,4-二硝基氯苯的制备方法及其应用

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2362743A (en) 1943-02-10 1944-11-14 Hercules Powder Co Ltd Manufacture of dinitrotoluene
US2947791A (en) 1957-01-24 1960-08-02 Du Pont Two-zone mononitration of toluene
NL233692A (enExample) 1957-11-29
DE1468362A1 (de) 1964-10-23 1968-11-28 Meissner Fa Josef Zweistufige Anlage zur Nitrierung von aromatischen Kohlenwasserstoffen
PL126089B1 (en) 1979-12-20 1983-07-30 Inst Ciezkiej Syntezy Orga Method of manufacture of dinitrotoluene
US4367347A (en) * 1981-06-01 1983-01-04 Air Products And Chemicals, Inc. High purity 2,4-dinitrotoluene from toluene nitration process
DE3409719A1 (de) 1984-03-16 1985-09-19 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von dinitrotoluol
TW236610B (en) 1992-11-13 1994-12-21 Bayer Ag Preparation of dinitrotoluene
US5275701A (en) 1993-03-15 1994-01-04 Air Products And Chemicals, Inc. Process for purification and concentration of sulfuric acid
DE4428459A1 (de) 1994-08-11 1996-02-15 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
DE4428462A1 (de) * 1994-08-11 1996-02-15 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
DE19512114C2 (de) 1995-04-04 2000-04-27 Meissner Gmbh & Co Kg Josef Rückgewinnung von Salpetersäure aus Nitrierprozessen
US5902910A (en) 1997-09-19 1999-05-11 Air Products And Chemicals, Inc. Weak acid process for producing dinitrotoluene
US5948944A (en) 1998-11-18 1999-09-07 Arco Chemical Technology, L.P. Two-stage dinitrotoluene production process
DE10055359C1 (de) 2000-11-08 2002-03-28 Bayer Ag Kontinuierliches isothermes Verfahren zur Herstellung von Mononitrotoluolen

Also Published As

Publication number Publication date
KR101151068B1 (ko) 2012-06-01
EP1713756A1 (de) 2006-10-25
PT1713756E (pt) 2015-11-30
CN100488941C (zh) 2009-05-20
WO2005075407A1 (de) 2005-08-18
DE102004005913A1 (de) 2005-08-25
KR20060130203A (ko) 2006-12-18
US20080242900A1 (en) 2008-10-02
ZA200607374B (en) 2008-06-25
JP4554622B2 (ja) 2010-09-29
BRPI0507293A (pt) 2007-07-03
CN1918109A (zh) 2007-02-21
JP2007520512A (ja) 2007-07-26
HUE025592T2 (en) 2016-05-30
PL1713756T3 (pl) 2016-01-29
EP1713756B1 (de) 2015-08-19
US7851661B2 (en) 2010-12-14
BRPI0507293B1 (pt) 2014-05-20

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