ES2259677T3 - Modificacion del peso molecular de polimeros termoplasticos. - Google Patents
Modificacion del peso molecular de polimeros termoplasticos.Info
- Publication number
- ES2259677T3 ES2259677T3 ES01981920T ES01981920T ES2259677T3 ES 2259677 T3 ES2259677 T3 ES 2259677T3 ES 01981920 T ES01981920 T ES 01981920T ES 01981920 T ES01981920 T ES 01981920T ES 2259677 T3 ES2259677 T3 ES 2259677T3
- Authority
- ES
- Spain
- Prior art keywords
- alkyl
- acid
- group
- hydrogen
- tert
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
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- 238000012986 modification Methods 0.000 title description 3
- 229920000642 polymer Polymers 0.000 claims abstract description 71
- 238000000034 method Methods 0.000 claims abstract description 54
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- 150000001875 compounds Chemical class 0.000 claims abstract description 48
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- 125000005262 alkoxyamine group Chemical group 0.000 claims abstract description 20
- 238000002844 melting Methods 0.000 claims abstract description 20
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- 238000004132 cross linking Methods 0.000 claims abstract description 19
- 238000012545 processing Methods 0.000 claims abstract description 14
- 229910052736 halogen Inorganic materials 0.000 claims abstract description 12
- 150000002367 halogens Chemical class 0.000 claims abstract description 12
- 229920006125 amorphous polymer Polymers 0.000 claims abstract description 5
- -1 polyethylene Polymers 0.000 claims description 177
- 125000000217 alkyl group Chemical group 0.000 claims description 69
- 239000002253 acid Substances 0.000 claims description 53
- 229910052739 hydrogen Inorganic materials 0.000 claims description 48
- 239000001257 hydrogen Substances 0.000 claims description 46
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 36
- 125000003118 aryl group Chemical group 0.000 claims description 35
- 150000002431 hydrogen Chemical group 0.000 claims description 33
- 125000004432 carbon atom Chemical group C* 0.000 claims description 25
- 125000001931 aliphatic group Chemical group 0.000 claims description 23
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 22
- 125000002947 alkylene group Chemical group 0.000 claims description 21
- 239000004743 Polypropylene Substances 0.000 claims description 18
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 16
- 125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 claims description 16
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- 239000004698 Polyethylene Substances 0.000 claims description 15
- 150000002148 esters Chemical class 0.000 claims description 15
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 claims description 14
- 229910052799 carbon Inorganic materials 0.000 claims description 14
- 125000003342 alkenyl group Chemical group 0.000 claims description 12
- 125000003236 benzoyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C(*)=O 0.000 claims description 12
- 125000001589 carboacyl group Chemical group 0.000 claims description 12
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- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 11
- 125000003710 aryl alkyl group Chemical group 0.000 claims description 11
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 claims description 10
- 229920000098 polyolefin Polymers 0.000 claims description 10
- 125000001731 2-cyanoethyl group Chemical group [H]C([H])(*)C([H])([H])C#N 0.000 claims description 9
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims description 9
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- 125000000753 cycloalkyl group Chemical group 0.000 claims description 8
- 125000001624 naphthyl group Chemical group 0.000 claims description 8
- 150000007933 aliphatic carboxylic acids Chemical class 0.000 claims description 7
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- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 6
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 claims description 6
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical group C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 5
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- 125000004429 atom Chemical group 0.000 claims description 5
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- KXDHJXZQYSOELW-UHFFFAOYSA-N carbonic acid monoamide Natural products NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 claims description 5
- 125000001511 cyclopentyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C1([H])[H] 0.000 claims description 5
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 5
- 229910052760 oxygen Inorganic materials 0.000 claims description 5
- BJELTSYBAHKXRW-UHFFFAOYSA-N 2,4,6-triallyloxy-1,3,5-triazine Chemical compound C=CCOC1=NC(OCC=C)=NC(OCC=C)=N1 BJELTSYBAHKXRW-UHFFFAOYSA-N 0.000 claims description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 4
- 229920000089 Cyclic olefin copolymer Polymers 0.000 claims description 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 4
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- 125000003884 phenylalkyl group Chemical group 0.000 claims description 4
- 229910052698 phosphorus Inorganic materials 0.000 claims description 4
- 239000011574 phosphorus Substances 0.000 claims description 4
- 229920002223 polystyrene Polymers 0.000 claims description 4
- 230000003252 repetitive effect Effects 0.000 claims description 4
- OLRJXMHANKMLTD-UHFFFAOYSA-N silyl Chemical compound [SiH3] OLRJXMHANKMLTD-UHFFFAOYSA-N 0.000 claims description 4
- KJAMZCVTJDTESW-UHFFFAOYSA-N tiracizine Chemical compound C1CC2=CC=CC=C2N(C(=O)CN(C)C)C2=CC(NC(=O)OCC)=CC=C21 KJAMZCVTJDTESW-UHFFFAOYSA-N 0.000 claims description 4
- 125000006839 xylylene group Chemical group 0.000 claims description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 3
- 125000002768 hydroxyalkyl group Chemical group 0.000 claims description 3
- 239000001301 oxygen Substances 0.000 claims description 3
- RGSFGYAAUTVSQA-UHFFFAOYSA-N pentamethylene Natural products C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 claims description 3
- 125000000843 phenylene group Chemical group C1(=C(C=CC=C1)*)* 0.000 claims description 3
- 125000004642 (C1-C12) alkoxy group Chemical group 0.000 claims description 2
- 125000004178 (C1-C4) alkyl group Chemical group 0.000 claims description 2
- FERLGYOHRKHQJP-UHFFFAOYSA-N 1-[2-[2-[2-(2,5-dioxopyrrol-1-yl)ethoxy]ethoxy]ethyl]pyrrole-2,5-dione Chemical compound O=C1C=CC(=O)N1CCOCCOCCN1C(=O)C=CC1=O FERLGYOHRKHQJP-UHFFFAOYSA-N 0.000 claims description 2
- IPJGAEWUPXWFPL-UHFFFAOYSA-N 1-[3-(2,5-dioxopyrrol-1-yl)phenyl]pyrrole-2,5-dione Chemical compound O=C1C=CC(=O)N1C1=CC=CC(N2C(C=CC2=O)=O)=C1 IPJGAEWUPXWFPL-UHFFFAOYSA-N 0.000 claims description 2
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 claims description 2
- 125000004450 alkenylene group Chemical group 0.000 claims description 2
- 125000004183 alkoxy alkyl group Chemical group 0.000 claims description 2
- 125000003545 alkoxy group Chemical group 0.000 claims description 2
- 125000003282 alkyl amino group Chemical group 0.000 claims description 2
- 125000000304 alkynyl group Chemical group 0.000 claims description 2
- 125000000732 arylene group Chemical group 0.000 claims description 2
- 239000000460 chlorine Substances 0.000 claims description 2
- 229910052801 chlorine Inorganic materials 0.000 claims description 2
- 125000001309 chloro group Chemical group Cl* 0.000 claims description 2
- 125000002993 cycloalkylene group Chemical group 0.000 claims description 2
- 125000004663 dialkyl amino group Chemical group 0.000 claims description 2
- 125000001841 imino group Chemical group [H]N=* 0.000 claims description 2
- 230000001939 inductive effect Effects 0.000 claims description 2
- 125000004430 oxygen atom Chemical group O* 0.000 claims description 2
- 125000004817 pentamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 claims description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims description 2
- 150000007934 α,β-unsaturated carboxylic acids Chemical class 0.000 claims description 2
- 239000004711 α-olefin Substances 0.000 claims description 2
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- 125000006702 (C1-C18) alkyl group Chemical group 0.000 claims 1
- ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 claims 1
- 229920006037 cross link polymer Polymers 0.000 abstract 1
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- 229930003799 tocopherol Natural products 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- 235000019149 tocopherols Nutrition 0.000 description 1
- 238000005809 transesterification reaction Methods 0.000 description 1
- JREYOWJEWZVAOR-UHFFFAOYSA-N triazanium;[3-methylbut-3-enoxy(oxido)phosphoryl] phosphate Chemical compound [NH4+].[NH4+].[NH4+].CC(=C)CCOP([O-])(=O)OP([O-])([O-])=O JREYOWJEWZVAOR-UHFFFAOYSA-N 0.000 description 1
- 150000003918 triazines Chemical class 0.000 description 1
- INNSFNJTGFCSRN-UHFFFAOYSA-N tridecyl 2-[(3,5-ditert-butyl-4-hydroxyphenyl)methylsulfanyl]acetate Chemical compound CCCCCCCCCCCCCOC(=O)CSCC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 INNSFNJTGFCSRN-UHFFFAOYSA-N 0.000 description 1
- 125000002889 tridecyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- IVIIAEVMQHEPAY-UHFFFAOYSA-N tridodecyl phosphite Chemical compound CCCCCCCCCCCCOP(OCCCCCCCCCCCC)OCCCCCCCCCCCC IVIIAEVMQHEPAY-UHFFFAOYSA-N 0.000 description 1
- CNUJLMSKURPSHE-UHFFFAOYSA-N trioctadecyl phosphite Chemical compound CCCCCCCCCCCCCCCCCCOP(OCCCCCCCCCCCCCCCCCC)OCCCCCCCCCCCCCCCCCC CNUJLMSKURPSHE-UHFFFAOYSA-N 0.000 description 1
- 229920000785 ultra high molecular weight polyethylene Polymers 0.000 description 1
- 229920001862 ultra low molecular weight polyethylene Polymers 0.000 description 1
- 229920001866 very low density polyethylene Polymers 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 150000003751 zinc Chemical class 0.000 description 1
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 description 1
- 239000002076 α-tocopherol Substances 0.000 description 1
- 235000004835 α-tocopherol Nutrition 0.000 description 1
- 239000011590 β-tocopherol Substances 0.000 description 1
- 235000007680 β-tocopherol Nutrition 0.000 description 1
- 239000002478 γ-tocopherol Substances 0.000 description 1
- QUEDXNHFTDJVIY-UHFFFAOYSA-N γ-tocopherol Chemical class OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-UHFFFAOYSA-N 0.000 description 1
- QUEDXNHFTDJVIY-DQCZWYHMSA-N γ-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-DQCZWYHMSA-N 0.000 description 1
- 239000002446 δ-tocopherol Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/32—Compounds containing nitrogen bound to oxygen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
- C08K5/0025—Crosslinking or vulcanising agents; including accelerators
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/34—Heterocyclic compounds having nitrogen in the ring
- C08K5/3412—Heterocyclic compounds having nitrogen in the ring having one nitrogen atom in the ring
- C08K5/3432—Six-membered rings
- C08K5/3435—Piperidines
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/26—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers modified by chemical after-treatment
- C08L2023/40—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers modified by chemical after-treatment by reaction with compounds changing molecular weight
- C08L2023/44—Coupling; Molecular weight increase
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Paper (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH10832000 | 2000-05-30 | ||
| CH1083/00 | 2000-05-30 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2259677T3 true ES2259677T3 (es) | 2006-10-16 |
Family
ID=4556514
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES01981920T Expired - Lifetime ES2259677T3 (es) | 2000-05-30 | 2001-05-22 | Modificacion del peso molecular de polimeros termoplasticos. |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US6949594B2 (enExample) |
| EP (1) | EP1287064B1 (enExample) |
| JP (1) | JP5042435B2 (enExample) |
| AT (1) | ATE321095T1 (enExample) |
| AU (1) | AU1013402A (enExample) |
| CA (1) | CA2405108C (enExample) |
| DE (1) | DE60118235T2 (enExample) |
| ES (1) | ES2259677T3 (enExample) |
| TW (1) | TWI255279B (enExample) |
| WO (1) | WO2001092397A1 (enExample) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003029332A1 (en) * | 2001-09-25 | 2003-04-10 | Ciba Specialty Chemicals Holding Inc. | Crosslinking of unsaturated polymers by the use of hydroxylamine-esters |
| PL1601719T3 (pl) * | 2003-03-12 | 2006-11-30 | Basf Se | Kompozycje powłokowe zawierające estry hydroksyloaminy |
| DE102004010162A1 (de) * | 2004-02-27 | 2005-09-15 | Degussa Ag | Polymerpulver mit Copolymer, Verwendung in einem formgebenden Verfahren mit nicht fokussiertem Energieeintrag und Formkörper, hergestellt aus diesem Polymerpulver |
| US8859843B2 (en) | 2009-02-27 | 2014-10-14 | The Procter & Gamble Company | Absorbent article with containment barrier |
| US8653196B2 (en) * | 2010-01-11 | 2014-02-18 | Dow Global Technologies, Llc | Method for preparing polyethylene with high melt strength |
| JP5698269B2 (ja) | 2010-02-10 | 2015-04-08 | ザ プロクター アンド ギャンブルカンパニー | 結合ウェブ材料を備える吸収性物品 |
| JP5591956B2 (ja) * | 2010-02-10 | 2014-09-17 | ザ プロクター アンド ギャンブル カンパニー | 収容バリアを備える吸収性物品 |
| CN105193556B (zh) | 2010-02-10 | 2018-10-09 | 宝洁公司 | 用于吸收制品的材料纤维网 |
| KR101408922B1 (ko) * | 2010-04-02 | 2014-06-17 | 엘에스전선 주식회사 | 직류용 전력 케이블용 절연 재료 조성물 및 이를 이용하여 제조된 케이블 |
| EP2995631A1 (en) | 2014-09-12 | 2016-03-16 | Borealis AG | Process for producing graft copolymers on polyolefin backbone |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5204473A (en) * | 1987-09-21 | 1993-04-20 | Ciba-Geigy Corporation | O-substituted N-hydroxy hindered amine stabilizers |
| JPH07252392A (ja) * | 1994-03-17 | 1995-10-03 | Japan Synthetic Rubber Co Ltd | 蒸気架橋用エチレン−プロピレン系共重合ゴム組成物 |
| IT1273607B (it) * | 1995-04-26 | 1997-07-08 | Ciba Geigy Spa | Combinazione di stabilizzanti per polimeri sintetici organici |
| EP0742257B1 (en) | 1995-05-11 | 2004-01-28 | Basell Poliolefine Italia S.p.A. | Process for the dynamic cross-linking and stabilization of a heterophasic polypropylene composition |
| ES2223068T3 (es) | 1995-12-18 | 2005-02-16 | General Electric Company | Mezclas de silano, de generador de radicales libres y de amina, para la reticulacion de polimeros de olefina. |
| US5910549A (en) * | 1996-08-22 | 1999-06-08 | Carnegie-Mellon University | Method for preparation of alkoxyamines from nitroxyl radicals |
| AUPO460797A0 (en) * | 1997-01-15 | 1997-02-06 | University Of Melbourne, The | Polymerisation process |
| BR9913416A (pt) * | 1998-09-03 | 2001-05-22 | Ciba Sc Holding Ag | Enxerto de monÈmeros etilenicamente insaturados em polìmeros |
-
2001
- 2001-05-22 ES ES01981920T patent/ES2259677T3/es not_active Expired - Lifetime
- 2001-05-22 DE DE60118235T patent/DE60118235T2/de not_active Expired - Lifetime
- 2001-05-22 US US10/296,346 patent/US6949594B2/en not_active Expired - Lifetime
- 2001-05-22 WO PCT/EP2001/005863 patent/WO2001092397A1/en not_active Ceased
- 2001-05-22 CA CA002405108A patent/CA2405108C/en not_active Expired - Lifetime
- 2001-05-22 AT AT01981920T patent/ATE321095T1/de active
- 2001-05-22 JP JP2002500600A patent/JP5042435B2/ja not_active Expired - Lifetime
- 2001-05-22 AU AU10134/02A patent/AU1013402A/en not_active Abandoned
- 2001-05-22 EP EP01981920A patent/EP1287064B1/en not_active Expired - Lifetime
- 2001-05-28 TW TW090112766A patent/TWI255279B/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| DE60118235D1 (de) | 2006-05-11 |
| US6949594B2 (en) | 2005-09-27 |
| EP1287064A1 (en) | 2003-03-05 |
| JP5042435B2 (ja) | 2012-10-03 |
| DE60118235T2 (de) | 2006-08-17 |
| CA2405108A1 (en) | 2001-12-06 |
| JP2003535171A (ja) | 2003-11-25 |
| AU1013402A (en) | 2001-12-11 |
| EP1287064B1 (en) | 2006-03-22 |
| CA2405108C (en) | 2009-10-13 |
| WO2001092397A1 (en) | 2001-12-06 |
| ATE321095T1 (de) | 2006-04-15 |
| US20030176588A1 (en) | 2003-09-18 |
| TWI255279B (en) | 2006-05-21 |
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