ES2139691T3 - Procedimiento para la preparacion de cloruros de acidos polifluorocarboxilicos y perfluorocarboxilicos. - Google Patents
Procedimiento para la preparacion de cloruros de acidos polifluorocarboxilicos y perfluorocarboxilicos.Info
- Publication number
- ES2139691T3 ES2139691T3 ES94112316T ES94112316T ES2139691T3 ES 2139691 T3 ES2139691 T3 ES 2139691T3 ES 94112316 T ES94112316 T ES 94112316T ES 94112316 T ES94112316 T ES 94112316T ES 2139691 T3 ES2139691 T3 ES 2139691T3
- Authority
- ES
- Spain
- Prior art keywords
- preparation
- chloride
- polyfluorocarboxyllic
- procedure
- perfluorocarboxylic acids
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 title 1
- 239000002253 acid Substances 0.000 title 1
- 150000007513 acids Chemical class 0.000 title 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 3
- 239000000460 chlorine Substances 0.000 abstract 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical group [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 2
- 239000011737 fluorine Substances 0.000 abstract 2
- 229910052731 fluorine Inorganic materials 0.000 abstract 2
- 125000001153 fluoro group Chemical group F* 0.000 abstract 2
- 230000003647 oxidation Effects 0.000 abstract 2
- 238000007254 oxidation reaction Methods 0.000 abstract 2
- OHMHBGPWCHTMQE-UHFFFAOYSA-N 2,2-dichloro-1,1,1-trifluoroethane Chemical compound FC(F)(F)C(Cl)Cl OHMHBGPWCHTMQE-UHFFFAOYSA-N 0.000 abstract 1
- AZPWOLJQERBBBM-UHFFFAOYSA-N 2-chloro-2,2-difluoroacetyl chloride Chemical compound FC(F)(Cl)C(Cl)=O AZPWOLJQERBBBM-UHFFFAOYSA-N 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- PNQBEPDZQUOCNY-UHFFFAOYSA-N trifluoroacetyl chloride Chemical compound FC(F)(F)C(Cl)=O PNQBEPDZQUOCNY-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/58—Preparation of carboxylic acid halides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
Abstract
SE DESCRIBE LA ELABORACION DE COMPUESTOS DE LA FORMULA RCFX(O)CL, DONDE X ES FLUOR O CLORO Y R ES FLUOR O UN C1 ESTO ALQUIL PERFLUORADO, CON PREFERENCIA A PARTIR DE CLORO DIFLUOR ACETIL CLORURO MEDIANTE OXIDACION FOTOQUIMICA DE R122 (CF2 CLCHCL2) Y LA ELABORACION DE TRIFLUOR ACETIL CLORURO MEDIANTE OXIDACION DE R123 (CF3CHCL2) CON OXIGENO BAJO RADIACION. LA TRANSFORMACION SE REALIZA PREFERENTEMENTE SIN PRESION Y SIN ADICION DE CLORO ELEMENTAL.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE4327195 | 1993-08-13 | ||
| DE4342601A DE4342601A1 (de) | 1993-08-13 | 1993-12-14 | Verfahren zur Herstellung von Poly- und Perfluorcarbonsäurechloriden |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2139691T3 true ES2139691T3 (es) | 2000-02-16 |
Family
ID=25928594
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES94112316T Expired - Lifetime ES2139691T3 (es) | 1993-08-13 | 1994-08-06 | Procedimiento para la preparacion de cloruros de acidos polifluorocarboxilicos y perfluorocarboxilicos. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US5545298A (es) |
| EP (1) | EP0638539B1 (es) |
| JP (1) | JPH0753446A (es) |
| AT (1) | ATE186291T1 (es) |
| DE (2) | DE4342601A1 (es) |
| DK (1) | DK0638539T3 (es) |
| ES (1) | ES2139691T3 (es) |
| GR (1) | GR3032296T3 (es) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5905169A (en) * | 1995-03-20 | 1999-05-18 | E. I. Du Pont De Nemours And Company | Process for producing polyfluoroacyl compositions |
| DE19650212A1 (de) * | 1996-12-04 | 1998-06-18 | Solvay Fluor & Derivate | Herstellung von Carbonsäurefluoriden |
| FR2807752A1 (fr) * | 2000-04-12 | 2001-10-19 | Solvay | Procede pour la preparation d'un hydrochlorofluoroalcane et catalyseur |
| FR2807751B1 (fr) * | 2000-04-12 | 2005-05-20 | Solvay | Procede pour la preparation d'un hydro (chloro) fluoroalcane et catalyseur |
| DE10033255A1 (de) * | 2000-07-10 | 2002-01-24 | Clariant Gmbh | Verfahren zur Herstellung von Perfluorcarbonsäuren |
| US20050113606A1 (en) * | 2003-11-20 | 2005-05-26 | Bell Robert L. | Continuous production of chlorodifluoroacetyl fluoride via chlorotrifluoroethylene oxidation |
| EP2170789A1 (en) * | 2007-07-20 | 2010-04-07 | Solvay Fluor GmbH | Process for obtaining a purified hydrofluoroalkane |
| CN101801906A (zh) * | 2007-08-16 | 2010-08-11 | 索尔维公司 | 制备4-氟取代的3-氧代-烷酸酯的方法 |
| CN102317252A (zh) | 2009-02-19 | 2012-01-11 | 苏威氟有限公司 | 氟取代的链烷酸的酯类的组合物 |
| CN101747176B (zh) * | 2009-12-24 | 2013-04-03 | 杭州原正化学工程技术装备有限公司 | 一种由三氟乙烷氯化混合物制备三氟乙酰氯的方法 |
| EP2987782A1 (en) * | 2014-08-22 | 2016-02-24 | Solvay SA | Distillation process comprising at least two distillation steps to obtain purified halogenated carboxylic acid halide, and use of the purified halogenated carboxylic acid halide |
| CA2966702A1 (en) | 2014-11-17 | 2016-05-26 | Solvay Sa | Distillation process comprising at least two distillation steps to obtain purified halogenated carboxylic acid halide, and use of the purified halogenated carboxylic acid halide |
| WO2016079122A1 (en) | 2014-11-17 | 2016-05-26 | Solvay Sa | A method for producing a chemical compound and apparatus therefor |
| EP3031791A1 (en) * | 2014-12-10 | 2016-06-15 | Solvay SA | Halogenation process of 1,1-dihaloethene |
| JP2019504840A (ja) | 2016-01-28 | 2019-02-21 | ソルヴェイ(ソシエテ アノニム) | ハロゲン置換ジケトン、ピラゾール化合物およびピラゾール化合物の製造方法 |
| EP3494107A1 (en) | 2016-08-02 | 2019-06-12 | Solvay Sa | Manufacture of hydrazinyl compounds useful in the manufacture of pyrazole carboxylic acid and derivatives, hydrazinyl compounds and their use |
| US20210171468A1 (en) | 2017-12-22 | 2021-06-10 | Solvay Sa | Process for the manufacture of pyrazole carboxylic derivatives and precursors thereof |
| CN109096087A (zh) * | 2018-09-11 | 2018-12-28 | 淄博飞源化工有限公司 | 一种三氟乙酸的制备方法 |
| EP3632855A1 (en) | 2018-10-02 | 2020-04-08 | Solvay Sa | A method for providing aqueous compositions with reduced content of organic fluorinated compounds |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1069137B (de) * | 1959-11-19 | Farbwerke Hoechst Aktiengesellschaft vormals Meister Lucius &. Bruning, Framkfurtl/M | Verfahren zur Herstellung von Fluor und Chlor enthaltenden Essigsaurtechloriden | |
| US2736695A (en) * | 1951-06-05 | 1956-02-28 | Allied Chem & Dye Corp | Process for preparing trichloroacetyl chloride |
| US3151051A (en) * | 1957-03-14 | 1964-09-29 | Pennsalt Chemicals Corp | Synthesis of fluorine compounds |
| DE1254616B (de) * | 1965-08-13 | 1967-11-23 | Hoechst Ag | Verfahren zur Herstellung von Trifluoracetylchlorid |
| DE1917630C3 (de) * | 1969-04-05 | 1979-04-12 | Kali-Chemie Ag, 3000 Hannover | Verfahren zur Herstellung von fluorhaltigen Perhalogencarbonsäurefluoriden oder -Chloriden |
| US3674664A (en) * | 1970-03-06 | 1972-07-04 | Dow Chemical Co | Method of preparing chloroacetyl chloride |
| USRE29044E (en) * | 1972-08-19 | 1976-11-23 | Kureha Kagaku Kogyo Kabushiki Kaisha | Method for the preparation of acetyl chloride |
| US3883407A (en) * | 1973-04-20 | 1975-05-13 | Halocarbon Prod Corp | Production of 2,2,2-trifluoroacetyl chloride |
| DE3564257D1 (en) * | 1984-05-15 | 1988-09-15 | Asahi Glass Co Ltd | Process for producing trifluoroacetic acid and trifluoroacetyl chloride |
| DE3513041A1 (de) * | 1985-04-09 | 1986-10-16 | Schering AG, Berlin und Bergkamen, 1000 Berlin | Difluorcyclopropanderivate, schaedlingsbekaempfungsmittel enthaltend diese verbindungen sowie verfahren zu ihrer herstellung |
| US5259938A (en) * | 1992-09-15 | 1993-11-09 | E. I. Du Pont De Nemours And Company | Process for omega-halo-perfluoro acid chlorides |
-
1993
- 1993-12-14 DE DE4342601A patent/DE4342601A1/de not_active Withdrawn
-
1994
- 1994-08-06 DK DK94112316T patent/DK0638539T3/da active
- 1994-08-06 ES ES94112316T patent/ES2139691T3/es not_active Expired - Lifetime
- 1994-08-06 EP EP94112316A patent/EP0638539B1/de not_active Expired - Lifetime
- 1994-08-06 AT AT94112316T patent/ATE186291T1/de not_active IP Right Cessation
- 1994-08-06 DE DE59408873T patent/DE59408873D1/de not_active Expired - Fee Related
- 1994-08-10 US US08/288,070 patent/US5545298A/en not_active Expired - Fee Related
- 1994-08-12 JP JP6190538A patent/JPH0753446A/ja not_active Ceased
-
1999
- 1999-12-30 GR GR990403384T patent/GR3032296T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE59408873D1 (de) | 1999-12-09 |
| DK0638539T3 (da) | 2000-01-03 |
| ATE186291T1 (de) | 1999-11-15 |
| EP0638539A2 (de) | 1995-02-15 |
| GR3032296T3 (en) | 2000-04-27 |
| DE4342601A1 (de) | 1995-02-16 |
| EP0638539A3 (de) | 1995-04-12 |
| US5545298A (en) | 1996-08-13 |
| JPH0753446A (ja) | 1995-02-28 |
| EP0638539B1 (de) | 1999-11-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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