ES2114629T3 - Preparacion de haluros de acidos carboxilicos y sales carboxilato. - Google Patents
Preparacion de haluros de acidos carboxilicos y sales carboxilato.Info
- Publication number
- ES2114629T3 ES2114629T3 ES94106032T ES94106032T ES2114629T3 ES 2114629 T3 ES2114629 T3 ES 2114629T3 ES 94106032 T ES94106032 T ES 94106032T ES 94106032 T ES94106032 T ES 94106032T ES 2114629 T3 ES2114629 T3 ES 2114629T3
- Authority
- ES
- Spain
- Prior art keywords
- halide
- carboxylic acid
- halides
- preparation
- salt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000002360 preparation method Methods 0.000 title abstract 3
- -1 CARBOXYLIC ACID HALIDES Chemical class 0.000 title 2
- 150000004820 halides Chemical class 0.000 abstract 5
- 238000000034 method Methods 0.000 abstract 3
- 150000003839 salts Chemical class 0.000 abstract 3
- 150000001244 carboxylic acid anhydrides Chemical class 0.000 abstract 2
- 150000001732 carboxylic acid derivatives Chemical class 0.000 abstract 2
- 239000003153 chemical reaction reagent Substances 0.000 abstract 2
- 229910001507 metal halide Inorganic materials 0.000 abstract 2
- 150000005309 metal halides Chemical class 0.000 abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 230000010933 acylation Effects 0.000 abstract 1
- 238000005917 acylation reaction Methods 0.000 abstract 1
- 230000002152 alkylating effect Effects 0.000 abstract 1
- 230000029936 alkylation Effects 0.000 abstract 1
- 238000005804 alkylation reaction Methods 0.000 abstract 1
- 150000001735 carboxylic acids Chemical class 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- 238000011065 in-situ storage Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000002699 waste material Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/14—Preparation of carboxylic acid esters from carboxylic acid halides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/58—Preparation of carboxylic acid halides
- C07C51/60—Preparation of carboxylic acid halides by conversion of carboxylic acids or their anhydrides or esters, lactones, salts into halides with the same carboxylic acid part
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
SE DESCRIBE UN PROCESO PARA LA ELABORACION DE HALOGENUROS DE ACIDO CARBOXILICO Y SALES DE CARBOXILATO A TRAVES DE LA TRANSFORMACION DE HALOGENUROS METALICOS O HALOGENUROS "ONIUM" CON ANHIDRIDOS DE ACIDO CARBOXILICO. EL PROCESO SE CARACTERIZA POR UNA ELABORACION MUY BUENA DE PREPARACIONES DE CATALIZADOR UTILIZADAS, LIBRES DE AGUA. EL HALOGENURO DE ACIDO CARBOXILICO ELABORADO O LA SAL DE CARBOXILATO PUEDEN SER UTILIZADOS COMO REACTIVO DE ACILIRACION O REACTIVO DE ALQUILIZACION. CON ELLO EL HALOGENURO METALICO O HALOGENURO "ONIUM" LIBERADO PUEDE RENOVARSE CON ANHIDRIDO DE ACIDO CARBOXILICO TRANSFORMADO Y CON ELLO SER REGENERADO. DE ESTA FORMA ES POSIBLE UNA ALQULIZACION LIBRE DE HIDROLISIS O ACILIRACION SIN LA EXISTENCIA DE PRODUCTOS DE DESECHO DEL TIPO DE SALES. SE REACCIONA LA MEZCLA DEL HALOGENURO DE ACIDO CARBOXILICO Y SAL DE CARBOXILATO, CON PREFERENCIA IN SITU CON UN ALCOHOL, SIENDO POSIBLE EL AISLAMIENTO DEL ESTER GENERADO SIN HIDROLISIS.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4313793A DE4313793A1 (de) | 1993-04-27 | 1993-04-27 | Herstellung von Carbonsäurehalogeniden und Carboxylat-Salzen |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2114629T3 true ES2114629T3 (es) | 1998-06-01 |
Family
ID=6486521
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES94106032T Expired - Lifetime ES2114629T3 (es) | 1993-04-27 | 1994-04-19 | Preparacion de haluros de acidos carboxilicos y sales carboxilato. |
Country Status (6)
Country | Link |
---|---|
US (1) | US5532411A (es) |
EP (1) | EP0623577B1 (es) |
JP (1) | JPH06306008A (es) |
AT (1) | ATE165077T1 (es) |
DE (2) | DE4313793A1 (es) |
ES (1) | ES2114629T3 (es) |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19732031C1 (de) * | 1997-07-25 | 1999-04-22 | Solvay Fluor & Derivate | 2-Phasen-Herstellung von Carbonsäureestern |
JP4621352B2 (ja) * | 1998-07-06 | 2011-01-26 | ゾルファイ フルーオル ゲゼルシャフト ミット ベシュレンクテル ハフツング | 弗化物の少ない有機化合物の製法 |
DE10143178A1 (de) * | 2001-09-04 | 2003-03-20 | Solvay Fluor & Derivate | Verfahren zur Herstellung von Carbonsäureestern |
US6969576B2 (en) * | 2001-11-30 | 2005-11-29 | Sandia National Laboratories | Photosensitive dissolution inhibitors and resists based on onium salt carboxylates |
DE102004060076A1 (de) * | 2004-12-14 | 2006-07-06 | Merck Patent Gmbh | Verfahren zur Herstellung von Onium-Salzen mit Alkyl- oder Arylsulfonat-Anionen oder Alkyl- oder Arylcarboxylat-Anionen mit geringem Halogenid-Gehalt |
FR2933693B1 (fr) * | 2008-07-10 | 2010-09-03 | Rhodia Operations | Procede de separation d'un acide carboxylique sous forme salifiee porteur d'au moins un atome d'halogene |
EP2987782A1 (en) | 2014-08-22 | 2016-02-24 | Solvay SA | Distillation process comprising at least two distillation steps to obtain purified halogenated carboxylic acid halide, and use of the purified halogenated carboxylic acid halide |
WO2016079126A1 (en) | 2014-11-17 | 2016-05-26 | Solvay Sa | Distillation process comprising at least two distillation steps to obtain purified halogenated carboxylic acid halide, and use of the purified halogenated carboxylic acid halide |
KR20210036985A (ko) | 2018-08-24 | 2021-04-05 | 허니웰 인터내셔날 인코포레이티드 | 트라이플루오로요오도메탄 및 트라이플루오로아세틸 요오다이드의 제조 방법 |
MX2021002101A (es) | 2018-08-24 | 2021-04-28 | Honeywell Int Inc | Procesos para producir trifluoroyodometano. |
US11554956B2 (en) | 2019-04-16 | 2023-01-17 | Honeywell International Inc. | Integrated process and catalysts for manufacturing hydrogen iodide from hydrogen and iodine |
WO2021031431A1 (en) | 2019-08-22 | 2021-02-25 | Fujian Yongjing Technology Co., Ltd | Process for preparing fluorobenzene by direct fluorination |
US20220112226A1 (en) * | 2020-10-14 | 2022-04-14 | Honeywell International Inc. | Trifluoroacetyl iodide compositions useful for making trifluoroiodomethane |
CN112159438B (zh) * | 2020-10-28 | 2024-02-09 | 浩宇康宁健康科技(湖北)有限公司 | 1-氯-2,3,5-三乙酰基-d-核糖的制备方法及其应用 |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2647933A (en) * | 1951-02-19 | 1953-08-04 | Minnesota Mining & Mfg | Making of rfbr from rfcooh |
CH313549A (de) * | 1952-05-23 | 1956-04-30 | Lonza Ag | Verfahren zur Herstellung von Carbonsäurehalogeniden |
US2704776A (en) * | 1953-02-24 | 1955-03-22 | Minnesota Mining & Mfg | Process for making of fluorocarbon derivatives |
US4136113A (en) * | 1977-12-28 | 1979-01-23 | Ethyl Corporation | Process for preparation of organic acid halide |
DE2947376A1 (de) * | 1979-11-24 | 1981-06-11 | Wolfgang Dipl.-Chem. Dr. Bobo-Dioulasso Hirsch | Verfahren zur herstellung von trifluoressigsaeurederivaten |
JPS577438A (en) * | 1980-06-17 | 1982-01-14 | Japan Tobacco Inc | Production of acid chloride |
US4382897A (en) * | 1981-07-23 | 1983-05-10 | Kali Chemie Ag | Process for the preparation of trifluoracetic acid derivatives |
IT1201435B (it) * | 1985-07-19 | 1989-02-02 | Montefluos Spa | Procedimento per la produzione di alchil trifluracetati |
CA1274539A (en) * | 1985-07-29 | 1990-09-25 | Eastman Chemical Company | Carbonylation process for the production of aromatic acids |
US4649216A (en) * | 1985-07-29 | 1987-03-10 | Eastman Kodak Company | Carbonylation process for the production of aromatic acids |
SU1694567A1 (ru) * | 1989-08-15 | 1991-11-30 | Предприятие П/Я Г-4567 | Способ получени галогенангидридов насыщенных полифторкарбоновых кислот |
-
1993
- 1993-04-27 DE DE4313793A patent/DE4313793A1/de not_active Withdrawn
-
1994
- 1994-04-19 DE DE59405676T patent/DE59405676D1/de not_active Expired - Fee Related
- 1994-04-19 AT AT94106032T patent/ATE165077T1/de active
- 1994-04-19 ES ES94106032T patent/ES2114629T3/es not_active Expired - Lifetime
- 1994-04-19 EP EP94106032A patent/EP0623577B1/de not_active Expired - Lifetime
- 1994-04-25 JP JP6086349A patent/JPH06306008A/ja active Pending
- 1994-04-26 US US08/233,624 patent/US5532411A/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
DE4313793A1 (de) | 1994-11-03 |
JPH06306008A (ja) | 1994-11-01 |
EP0623577A1 (de) | 1994-11-09 |
US5532411A (en) | 1996-07-02 |
EP0623577B1 (de) | 1998-04-15 |
ATE165077T1 (de) | 1998-05-15 |
DE59405676D1 (de) | 1998-05-20 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG2A | Definitive protection |
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