ES2108527T3 - Procedimiento para la obtencion de 3-aminometil-3,5,5-trimetilciclohexilamina. - Google Patents

Procedimiento para la obtencion de 3-aminometil-3,5,5-trimetilciclohexilamina.

Info

Publication number
ES2108527T3
ES2108527T3 ES95112482T ES95112482T ES2108527T3 ES 2108527 T3 ES2108527 T3 ES 2108527T3 ES 95112482 T ES95112482 T ES 95112482T ES 95112482 T ES95112482 T ES 95112482T ES 2108527 T3 ES2108527 T3 ES 2108527T3
Authority
ES
Spain
Prior art keywords
aminometil
procedure
obtaining
trimetilciclohexilamina
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES95112482T
Other languages
English (en)
Inventor
Tom Dr Witzel
Guido Dr Voit
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of ES2108527T3 publication Critical patent/ES2108527T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/33—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of rings other than six-membered aromatic rings
    • C07C211/34—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of rings other than six-membered aromatic rings of a saturated carbon skeleton
    • C07C211/36—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of rings other than six-membered aromatic rings of a saturated carbon skeleton containing at least two amino groups bound to the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
    • C07C209/26—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds by reduction with hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
    • C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
    • C07C209/52—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of imines or imino-ethers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PROCEDIMIENTO PARA LA OBTENCION DE 3-AMINOMETIL-3,5,5-TRIMETILCICLOHEXIL-AMINA POR REACCION DE 3-CIANO-3,5,5-TRIMETILCICLOHEXANONA CON 3-AMINOMETIL-3,5,5-TRIMETIL-CICLOHEXIL-AMINA Y A CONTINUACION O SIMULTANEAMENTE ADICION DE AMONIACO A UNA PRESION DE HIDROGENO DE 50 A 300 BAR Y EN PRESENCIA DE UN CATALIZADOR DE HIDROGENACION A TEMPERATURAS DE 20 A 150 C, REALIZANDOSE LA REACCION SIN SEPARACION DEL AGUA DE LA REACCION.
ES95112482T 1994-03-04 1995-08-09 Procedimiento para la obtencion de 3-aminometil-3,5,5-trimetilciclohexilamina. Expired - Lifetime ES2108527T3 (es)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DE4407325A DE4407325B4 (de) 1994-03-04 1994-03-04 Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin
EP95112482A EP0757980B1 (de) 1994-03-04 1995-08-09 Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin
JP21085695A JP3811202B2 (ja) 1994-03-04 1995-08-18 ３−アミノメチル３，５，５−トリメチルシクロヘキシルアミンの製造方法
CA002156576A CA2156576C (en) 1994-03-04 1995-08-21 Preparation of 3-aminomethyl-3, 5, 5-trimethylcyclohexylamine

Publications (1)

Publication Number Publication Date
ES2108527T3 true ES2108527T3 (es) 1997-12-16

Family

ID=27427251

Family Applications (1)

Application Number Title Priority Date Filing Date
ES95112482T Expired - Lifetime ES2108527T3 (es) 1994-03-04 1995-08-09 Procedimiento para la obtencion de 3-aminometil-3,5,5-trimetilciclohexilamina.

Country Status (6)

Country Link
US (1) US5705699A (es)
EP (1) EP0757980B1 (es)
JP (1) JP3811202B2 (es)
CA (1) CA2156576C (es)
DE (2) DE4407325B4 (es)
ES (1) ES2108527T3 (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19627265A1 (de) * 1996-07-06 1998-01-08 Degussa Verfahren zur Herstellung primärer und/oder sekundärer Amine aus Oxoverbindungen
US7544354B2 (en) * 2000-10-27 2009-06-09 Novartis Vaccines And Diagnostics Methods of protein purification and recovery
EP2279164B1 (de) * 2008-05-13 2012-03-28 Basf Se Verfahren zur herstellung von n,n-substituierten-1,3-propandiaminen
EP2459514B1 (en) 2009-07-31 2017-07-19 Dow Global Technologies LLC Cycloaliphatic diamines and method of making the same
RU2616616C2 (ru) * 2012-12-07 2017-04-18 Ваньхуа Кемикал Груп Ко., Лтд. Способ получения 3-аминометил-3,5,5-триметилциклогексиламина
CN107857704B (zh) * 2017-11-21 2020-04-10 万华化学集团股份有限公司 一种制备3-氨甲基-3,5,5-三甲基环己胺的方法及用于该方法的催化剂

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1229078B (de) 1961-10-18 1966-11-24 Hibernia Chemie Ges Mit Beschr Verfahren zur Herstellung von 3-(Aminomethyl)-3, 5, 5-trimethylcyclohexylderivaten
DE1240854B (de) 1964-10-24 1967-05-24 Scholven Chemie Ag Verfahren zur Herstellung von 3-Cyan-3, 5, 5-trimethylcyclohexanon aus Isophoron undBlausaeure
US4248799A (en) * 1978-12-27 1981-02-03 Phillips Petroleum Company Hydrogenation of nitriles in ammonia and water
DE3011656A1 (de) * 1980-03-26 1981-10-01 Chemische Werke Hüls AG, 4370 Marl Verfahren zur herstellung von 3-aminomethyl-3-5-5-trimethyl-cyclohexylamin
DE3021955A1 (de) 1980-06-12 1981-12-24 Chemische Werke Hüls AG, 4370 Marl Verfahren zur herstellung primaerer mono- und diamine aus oxoverbindungen
CN1047856A (zh) * 1989-04-25 1990-12-19 联合碳化化学品及塑料有限公司 羰基腈和类似化合物的还原胺化
US5011968A (en) * 1990-02-06 1991-04-30 W. R. Grace & Co.-Conn. Process for the preparation of 3-cyano-3,5,5-trimethylcyclohexanone
DE4010227A1 (de) * 1990-03-30 1991-10-02 Basf Ag Verfahren zur herstellung von 3-aminomethyl-3,5,5-trimethyl-cyclohexylamin
DE4106882C2 (de) * 1991-03-05 1994-02-03 Degussa Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethyl-cyclohexylamin durch reduktive Aminierung von 1,3,3-Trimethyl-5-oxocyclohexan-carbonitril
EP0534449A3 (en) * 1991-09-25 1993-06-02 Mitsubishi Kasei Corporation Process for the preparation of 3-aminomethyl-3,5,5-trialkylcyclohexylamine
DE4232424A1 (de) * 1992-09-28 1994-03-31 Basf Ag Verfahren zur Herstellung von ungesättigten Aminen
US5406000A (en) * 1993-01-12 1995-04-11 Elf/Atochem North America, Inc. Process for the production of 3-aminomethyl-3,5,5-trialkylcyclohexylamine
DE4426472A1 (de) * 1993-07-27 1995-02-02 Du Pont Herstellung von Isophorondiamin

Also Published As

Publication number Publication date
DE4407325A1 (de) 1995-09-07
EP0757980B1 (de) 1997-10-29
CA2156576C (en) 2004-10-05
CA2156576A1 (en) 1997-02-22
JPH0959226A (ja) 1997-03-04
EP0757980A1 (de) 1997-02-12
DE4407325B4 (de) 2006-06-29
DE59500920D1 (de) 1997-12-04
JP3811202B2 (ja) 2006-08-16
US5705699A (en) 1998-01-06

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