ES2042120T3 - Procedimiento para la separacion de fluoruro de hidrogeno, 1,1-dicloro-1-fluoroetano y 1-cloro-1,1-difluoroetano de sus mezclas liquidas. - Google Patents
Procedimiento para la separacion de fluoruro de hidrogeno, 1,1-dicloro-1-fluoroetano y 1-cloro-1,1-difluoroetano de sus mezclas liquidas.Info
- Publication number
- ES2042120T3 ES2042120T3 ES199090106409T ES90106409T ES2042120T3 ES 2042120 T3 ES2042120 T3 ES 2042120T3 ES 199090106409 T ES199090106409 T ES 199090106409T ES 90106409 T ES90106409 T ES 90106409T ES 2042120 T3 ES2042120 T3 ES 2042120T3
- Authority
- ES
- Spain
- Prior art keywords
- separation
- fluoroethane
- difluoroethane
- dichloro
- chlorine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000926 separation method Methods 0.000 title abstract 3
- 239000000203 mixture Substances 0.000 title abstract 2
- FRCHKSNAZZFGCA-UHFFFAOYSA-N 1,1-dichloro-1-fluoroethane Chemical compound CC(F)(Cl)Cl FRCHKSNAZZFGCA-UHFFFAOYSA-N 0.000 title 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 title 1
- 229910000040 hydrogen fluoride Inorganic materials 0.000 title 1
- 239000007788 liquid Substances 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical class [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
- 239000012071 phase Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
- C01B7/191—Hydrogen fluoride
- C01B7/195—Separation; Purification
- C01B7/196—Separation; Purification by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/90—Particular type of heating
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
LA SEPARACION RESULTA DE LA HIDROFLUORINACION CON 1,1,1,-TRICLOROETAO O CLORURO VINILEDENO. LOS COMPONENES A SEPARAR SE DESTILAN PRIMERO EN SUS RESPECTIVAS MEZCLAS, LUEGO SE SUJETAN A UNO FASE DE SEPARACION RESULTANTE DE DOS FASES LIQUIDAS DE HIDROGENO ENRIQUECIDO CON FLUORIDO.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/347,606 US4975156A (en) | 1989-05-04 | 1989-05-04 | Process for the separation of hydrogen fluoride, 1,1-dichloro-1-fluoroethane and 1-chloro-1,1-difluoroethane from liquid mixtures thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2042120T3 true ES2042120T3 (es) | 1993-12-01 |
Family
ID=23364444
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES199090106409T Expired - Lifetime ES2042120T3 (es) | 1989-05-04 | 1990-04-04 | Procedimiento para la separacion de fluoruro de hidrogeno, 1,1-dicloro-1-fluoroetano y 1-cloro-1,1-difluoroetano de sus mezclas liquidas. |
Country Status (7)
Country | Link |
---|---|
US (1) | US4975156A (es) |
EP (1) | EP0395898B1 (es) |
JP (1) | JPH02295938A (es) |
AT (1) | ATE91277T1 (es) |
CA (1) | CA2013822A1 (es) |
DE (1) | DE69002123D1 (es) |
ES (1) | ES2042120T3 (es) |
Families Citing this family (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5087329A (en) * | 1991-05-16 | 1992-02-11 | E. I. Du Pont De Nemours And Company | Process for separating pentafluoroethane from a mixture of halogenated hydrocarbons containing chloropentafluoroethane |
JP2661441B2 (ja) * | 1991-11-27 | 1997-10-08 | ダイキン工業株式会社 | 1,1,1−トリフルオロ−2−クロロエタンおよび/または1,1,1,2−テトラフルオロエタンの製法 |
US6676809B1 (en) | 1992-02-07 | 2004-01-13 | Daikin Industries Ltd. | Process for removal of hydrogen fluoride |
FR2689503B1 (fr) * | 1992-04-03 | 1994-06-10 | Solvay | Procede d'epuration d'un hydrofluoroalcane. |
DE69319711T2 (de) | 1992-04-13 | 1999-01-07 | Daikin Industries, Ltd., Osaka | Verfahren zur entfernung von fluorwasserstoff |
FR2689885B1 (fr) * | 1992-04-14 | 1994-10-21 | Atochem North America Elf | Procédé pour inhiber la décomposition du 1,1-dichloro-1-fluoréthane. |
TW227550B (es) * | 1992-08-05 | 1994-08-01 | Showa Denko Kk | |
TW228512B (es) * | 1992-08-10 | 1994-08-21 | Showa Denko Kk | |
US5336816A (en) * | 1992-12-17 | 1994-08-09 | Laroche Chemicals, Inc. | Method for preparing 1,1-dichloro-1-fluoroethane |
DE69417024T2 (de) * | 1993-04-30 | 1999-11-04 | E.I. Du Pont De Nemours And Co., Wilmington | AZEOTROPE UND AZEOTROPARTIGE ZUSAMMENSETZUNGEN UND VERFAHREN ZUR TRENNUNG VON HCl UND HALOGENKOHLENWASSERSTOFFEN |
US5656137A (en) * | 1994-03-25 | 1997-08-12 | Elf Atochem North America, Inc. | F141B crude stabilization |
GB2297380A (en) * | 1995-01-30 | 1996-07-31 | Grace W R & Co | Analysing chloride content of a liquid |
JP4443921B2 (ja) * | 2001-06-01 | 2010-03-31 | ハネウェル・インターナショナル・インコーポレーテッド | ペンタフルオロブタンの共沸混合物様組成物 |
JP4689084B2 (ja) * | 2001-06-13 | 2011-05-25 | 新オオツカ株式会社 | 溶剤分離装置 |
RU2476416C2 (ru) * | 2008-02-21 | 2013-02-27 | Е.И.Дюпон Де Немур Энд Компани | Способы отделения 2,3,3,3-тетрафторпропена от фтористого водорода способом азеотропной дистилляции |
BRPI0906015A2 (pt) * | 2008-02-21 | 2015-06-30 | Du Pont | "processo de separação de uma mistura que compreende o hf e hfc-1234ze, processo para a separação de um e-hfc-1234ze a partir de uma mistura que inclui o fluoreto de hidrogênio e dito e-hfc-1234ze, processo para a separação do fluoreto de hidrogênio a partir de uma mistura contendo fluoreto de hidrogênio e e-hfc-1234ze, processo para a purificação de um e-hfc-1234ze a partir de uma mistura de e-hfc-1234ze e hf, processo para a purificação do hf a partir de uma mistura que compreende e-hfc-1234ze e hf, processo para a separação do e-hfc-1234ze de uma mistura de e-hfc-1234ze, hf e pelo menos um dos hfc-245fa ou hfc-245eb e processo para a separação do hfc-1234yf do hfc-1234ze" |
CN111099961A (zh) * | 2018-10-26 | 2020-05-05 | 中昊晨光化工研究院有限公司 | 一种二氟乙烷和二氟一氯乙烷生产合用的精馏方法及系统 |
JP6904374B2 (ja) * | 2019-03-28 | 2021-07-14 | ダイキン工業株式会社 | 1,1,2−トリクロロエタン、トランス−1,2−ジクロロエチレン又はシス−1,2−ジクロロエチレンと、フッ化水素とを含む共沸又は共沸様組成物 |
KR102690745B1 (ko) * | 2019-04-10 | 2024-08-05 | 다이킨 고교 가부시키가이샤 | 1,1,2-트리플루오로에탄, 1-클로로-2,2-디플루오로에탄 또는 1,2-디클로로-1-플루오로에탄과, 불화수소를 포함하는 공비 또는 유사 공비 조성물 |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2549609A (en) * | 1944-10-27 | 1951-04-17 | Kenneth C Johnson | Separation of fluorinated hydrocarbons by distillation with hydrogen fluoride |
US2478362A (en) * | 1948-06-15 | 1949-08-09 | Kinetic Chemicals Inc | Distillation process for separating products of perchloro-ethylene fluorination |
JPS505681B1 (es) * | 1970-07-28 | 1975-03-06 | ||
JPS4832449A (es) * | 1971-08-31 | 1973-04-28 | ||
US3947558A (en) * | 1973-08-16 | 1976-03-30 | Dow Chemical (Nederland) B.V. | Method of recovering HF from mixtures containing C1 -C3 halocarbon compounds |
JPS5946211B2 (ja) * | 1975-12-29 | 1984-11-10 | ダイキン工業株式会社 | 1− クロロ −1,1− ジフルオロエタンマタハ / オヨビ 1,1,1− トリフルオロエタンオセイゾウスルホウホウ |
LU75857A1 (es) * | 1976-09-22 | 1978-05-12 | ||
US4199409A (en) * | 1977-02-22 | 1980-04-22 | Phillips Petroleum Company | Recovery of HF from an alkylation unit acid stream containing acid soluble oil |
FR2414475A1 (fr) * | 1978-01-13 | 1979-08-10 | Solvay | Procede pour la separation du fluorure d'hydrogene de ses melanges avec le 1-chloro-1, 1-difluorethane |
FR2617475B1 (fr) * | 1987-07-03 | 1989-12-01 | Atochem | Synthese du chloro-1 difluoro-1,1 ethane |
-
1989
- 1989-05-04 US US07/347,606 patent/US4975156A/en not_active Expired - Fee Related
-
1990
- 1990-04-04 AT AT90106409T patent/ATE91277T1/de not_active IP Right Cessation
- 1990-04-04 DE DE9090106409T patent/DE69002123D1/de not_active Expired - Lifetime
- 1990-04-04 CA CA002013822A patent/CA2013822A1/en not_active Abandoned
- 1990-04-04 EP EP90106409A patent/EP0395898B1/en not_active Expired - Lifetime
- 1990-04-04 ES ES199090106409T patent/ES2042120T3/es not_active Expired - Lifetime
- 1990-04-18 JP JP2100564A patent/JPH02295938A/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
DE69002123D1 (de) | 1993-08-12 |
CA2013822A1 (en) | 1990-11-04 |
JPH02295938A (ja) | 1990-12-06 |
EP0395898A1 (en) | 1990-11-07 |
EP0395898B1 (en) | 1993-07-07 |
US4975156A (en) | 1990-12-04 |
ATE91277T1 (de) | 1993-07-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG2A | Definitive protection |
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