ES2013588A4 - Purificacion de glioxilato de alquilo. - Google Patents
Purificacion de glioxilato de alquilo.Info
- Publication number
- ES2013588A4 ES2013588A4 ES89870115T ES89870115T ES2013588A4 ES 2013588 A4 ES2013588 A4 ES 2013588A4 ES 89870115 T ES89870115 T ES 89870115T ES 89870115 T ES89870115 T ES 89870115T ES 2013588 A4 ES2013588 A4 ES 2013588A4
- Authority
- ES
- Spain
- Prior art keywords
- alkyl
- glioxylate
- purification
- streams
- oxidation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/22—Evaporating by bringing a thin layer of the liquid into contact with a heated surface
- B01D1/222—In rotating vessels; vessels with movable parts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
- B01D3/146—Multiple effect distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/36—Azeotropic distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0078—Condensation of vapours; Recovering volatile solvents by condensation characterised by auxiliary systems or arrangements
- B01D5/0093—Removing and treatment of non condensable gases
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/20—Power plant
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/90—Particular type of heating
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/224,045 US4867849A (en) | 1988-07-25 | 1988-07-25 | Purification of alkyl glyoxylate |
Publications (2)
Publication Number | Publication Date |
---|---|
ES2013588A4 true ES2013588A4 (es) | 1990-05-16 |
ES2013588T3 ES2013588T3 (es) | 1994-08-01 |
Family
ID=22839075
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES89870115T Expired - Lifetime ES2013588T3 (es) | 1988-07-25 | 1989-07-24 | Purificacion de glioxilatos de alquilo. |
Country Status (7)
Country | Link |
---|---|
US (1) | US4867849A (es) |
EP (1) | EP0353215B1 (es) |
JP (1) | JPH0745435B2 (es) |
AT (1) | ATE107272T1 (es) |
CA (1) | CA1324103C (es) |
DE (1) | DE68916123T2 (es) |
ES (1) | ES2013588T3 (es) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AT392638B (de) * | 1989-06-05 | 1991-05-10 | Chemie Linz Gmbh | Verfahren zur kontinuierlichen herstellung einer konzentrierten waessrigen loesung von glyoxylsaeure |
US5217582A (en) * | 1990-06-20 | 1993-06-08 | E. I. Du Pont De Nemours And Company | Process for the isolation of alkyl glyoxylate |
JP3150909B2 (ja) * | 1996-09-05 | 2001-03-26 | 株式会社日本触媒 | グリオキシル酸エステル類の精製方法 |
US6286335B1 (en) * | 1999-09-03 | 2001-09-11 | Air Products And Chemicals, Inc. | Processes for multicomponent separation |
NL1013682C2 (nl) * | 1999-11-26 | 2001-05-30 | Purac Biochem Bv | Werkwijze en inrichting voor het zuiveren van een waterige oplossing van melkzuur. |
US9114328B2 (en) | 2012-05-16 | 2015-08-25 | Eastman Chemical Company | Reactive distillation of a carboxylic acid and a glycol |
US9040748B2 (en) | 2012-06-08 | 2015-05-26 | Eastman Chemical Company | Hydrocarboxylation of aqueous formaldehyde using a dehydrating recycle stream to decrease water concentration |
DE102013222343A1 (de) | 2013-11-04 | 2015-05-07 | Matthias Enzenhofer | Vorrichtung und Verfahren für den Kontakt einer Gasphase mit einem flüssigen Medium |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1627091A (en) * | 1923-03-05 | 1927-05-03 | Boehringer Sohn Ingelheim | Making keto and aldo aliphatic carboxylic acids |
US3476656A (en) * | 1968-06-07 | 1969-11-04 | Universal Oil Prod Co | Fractional distillation and recovery of styrene containing sulfur with subsequent bottoms separation |
FR2383911A1 (fr) * | 1977-03-17 | 1978-10-13 | Hoechst France | Procede permettant d'augmenter les rendements en hemiacetal-esters de l'acide glyoxylique au cours de leur obtention ou leurs taux de recuperation dans les milieux les contenant |
US4144226A (en) * | 1977-08-22 | 1979-03-13 | Monsanto Company | Polymeric acetal carboxylates |
US4234739A (en) * | 1978-12-05 | 1980-11-18 | Stauffer Chemical Company | Method for preparing glyoxylic acids and derivatives thereof |
DE2904775C2 (de) * | 1979-02-08 | 1985-03-21 | Hoechst Ag, 6230 Frankfurt | Verfahren zur Herstellung von Glyoxylsäureestern |
JPS57176929A (en) * | 1981-04-24 | 1982-10-30 | Nippon Synthetic Chem Ind Co Ltd:The | Preparation of glyoxylic ester |
DE3323372A1 (de) * | 1983-06-29 | 1985-01-10 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung eines glyoxylsaeureesters |
US4502923A (en) * | 1983-10-06 | 1985-03-05 | Monsanto Company | Production of high purity alkyl glyoxylate by plural stage distillation |
JPS61109221A (ja) * | 1984-10-31 | 1986-05-27 | 田中貴金属工業株式会社 | 孔あき型クラツドボタン接点の製造方法 |
DE3446528A1 (de) * | 1984-12-20 | 1986-06-26 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung von glyoxylsaeurehemiacetalestern |
DE3602274A1 (de) * | 1986-01-25 | 1987-07-30 | Hoechst Ag | Halbacetale von glyoxylsaeureestern sowie verfahren zur isolierung von glyoxylsaeureestern |
-
1988
- 1988-07-25 US US07/224,045 patent/US4867849A/en not_active Expired - Lifetime
-
1989
- 1989-07-24 DE DE68916123T patent/DE68916123T2/de not_active Expired - Fee Related
- 1989-07-24 AT AT89870115T patent/ATE107272T1/de not_active IP Right Cessation
- 1989-07-24 JP JP1189028A patent/JPH0745435B2/ja not_active Expired - Lifetime
- 1989-07-24 CA CA000606487A patent/CA1324103C/en not_active Expired - Fee Related
- 1989-07-24 ES ES89870115T patent/ES2013588T3/es not_active Expired - Lifetime
- 1989-07-24 EP EP89870115A patent/EP0353215B1/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
DE68916123T2 (de) | 1994-12-01 |
JPH0745435B2 (ja) | 1995-05-17 |
ATE107272T1 (de) | 1994-07-15 |
ES2013588T3 (es) | 1994-08-01 |
EP0353215B1 (en) | 1994-06-15 |
CA1324103C (en) | 1993-11-09 |
EP0353215A2 (en) | 1990-01-31 |
EP0353215A3 (en) | 1990-08-08 |
DE68916123D1 (de) | 1994-07-21 |
US4867849A (en) | 1989-09-19 |
JPH0273040A (ja) | 1990-03-13 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG2A | Definitive protection |
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